Indole

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30100.1255.9Tudor, 199740. m/0.35 mm/0.35 μm
CapillaryOV-101140.1281.1Gerasimenko, Kirilenko, et al., 1981N2; Column length: 50. m; Column diameter: 0.3 mm
PackedSE-30170.1296.Tibor and Anna, 1971N2, Chromosorb W-AW; Column length: 2. m
PackedSE-30190.1310.Tibor and Anna, 1971N2, Chromosorb W-AW; Column length: 2. m

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-11303.Raina, Lal, et al., 200260. m/0.32 mm/0.25 μm, N2, 5. K/min; Tstart: 60. C; Tend: 220. C
CapillaryDB-51292.Dickens, 199930. m/0.25 mm/0.25 μm, 50. C @ 2. min, 15. K/min, 235. C @ 2. min
CapillarySE-301260.Greenberg, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C
CapillarySE-301263.Greenberg, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C
CapillaryOV-1011273.Yamaguchi and Shibamoto, 1981N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011274.Yamaguchi and Shibamoto, 1981N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySPB-11291.Borse, Jagan Mohan Rao, et al., 200230. m/0.32 mm/0.25 μm, He; Program: 40C(3min) => 2C/min => 100C => 4C/min => 220C (7min)
CapillaryDB-51292.Dickens J.C., 2000Program: not specified
PackedSE-301276.Ramsey, Lee, et al., 1980He, Chromosorb G HP (80-100 mesh); Column length: 1.5 m; Program: not specified

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedCarbowax 20M220.2449.Sellier, Tersac, et al., 1981Column length: 2. m
PackedPEG-20M190.2420.Tibor and Anna, 1971N2, Chromosorb W-AW; Column length: 2. m

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP-Sil PONA GB1265.Cunicao, Lopes, et al., 2007100. m/0.25 mm/0.25 μm, He, 140. C @ 10. min, 5. K/min, 230. C @ 25. min
CapillaryHP-51289.Flamini, Tebano, et al., 200730. m/0.25 mm/0.25 μm, N2, 50. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51320.Rout, Rao, et al., 200725. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 60. min; Tstart: 60. C
CapillaryCP Sil 8 CB1287.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryBPX-51319.Dickschat J.S., Wagner-Dobler I., et al., 200525. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 5. K/min; Tend: 300. C
CapillarySPB-51288.Píno, Marbot, et al., 200430. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillarySPB-51288.Pino, Marbot, et al., 200430. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillarySPB-51288.Pino, Marbot, et al., 2004, 230. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillaryDB-51295.Reis, Pansarim, et al., 200430. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 290. C
CapillaryHP-51295.Flamini, Luigi Cioni, et al., 200330. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-5MS1290.Karagül-Yüceer, Vlahovich, et al., 200330. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 10. K/min, 200. C @ 30. min
CapillaryDB-11244.3Sun and Stremple, 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 325. C
CapillaryMega 5MS1290.Verzera, Trozzi, et al., 200330. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryDB-11257.Kim, 200160. m/0.32 mm/1. μm, He, 40. C @ 5. min, 2. K/min; Tend: 220. C
CapillaryDB-51288.Nogueira, Bittrich, et al., 200130. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillarySE-541291.Li, Wang, et al., 1998H2, 35. C @ 3. min, 4. K/min; Column length: 25. m; Column diameter: 0.31 mm; Tend: 250. C
CapillarySE-541294.Li, Wang, et al., 1998H2, 35. C @ 3. min, 4. K/min; Column length: 25. m; Column diameter: 0.31 mm; Tend: 250. C
CapillaryDB-51288.Nogueira, Marsaioli, et al., 199830. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51328.Moio L., Rillo L., et al., 199630. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryDB-51329.Moio L., Rillo L., et al., 199630. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryDB-51340.Moio L., Rillo L., et al., 199630. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryDB-11305.Stashenko, Prada, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 3.5 K/min; Tend: 250. C
CapillarySE-301263.de Frutos, Sanz, et al., 199122. m/0.30 mm/1.0 μm, N2, 2. K/min; Tstart: 60. C; Tend: 250. C
PackedSE-301273.Peng, Ding, et al., 1988He, Supelcoport and Chromosorb, 40. C @ 4. min, 10. K/min, 250. C @ 60. min; Column length: 3.05 m
CapillaryDB-51295.Rostad and Pereira, 198630. m/0.26 mm/0.25 μm, He, 50. C @ 4. min, 6. K/min, 300. C @ 20. min

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11276.Place, Imhof, et al., 200360. m/0.32 mm/1. μm, He; Program: 35C(5min) => 10C/min => 45C (5min) => 5C/min => 250C (10min)
CapillaryDB-51300.Jezussek, Juliano, et al., 200230. m/0.32 mm/0.25 μm, He; Program: 40C(1min) => 40C/min => 50C(2min) => 6C/min => 240C
CapillaryDB-51293.Rychlik and Bosset, 200130. m/0.32 mm/0.25 μm, He; Program: 35C(2min) => 40C/min => 60C (2min) => 4C/min => 240C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP-Wax 52CB2420.Mahadevan and Farmer, 200660. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillarySupelcowax-102405.Chung, Fung, et al., 200560. m/0.25 mm/0.25 μm, 35. C @ 5. min, 6. K/min, 195. C @ 60. min
CapillaryDB-FFAP2446.Karagül-Yüceer, Vlahovich, et al., 200330. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 10. K/min, 200. C @ 30. min
CapillarySupelcowax-102444.Chung, Yung, et al., 200260. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 2. K/min, 195. C @ 90. min
CapillarySupelcowax-102444.Chung, Yung, et al., 200160. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 2. K/min, 195. C @ 90. min
CapillarySupelcowax-102444.Chung, 200060. m/0.25 mm/0.25 μm, He, 2. K/min, 195. C @ 90. min; Tstart: 35. C
CapillaryHP-Innowax2465.Christensen, Jakobsen, et al., 1999He, 32. C @ 1. min, 2. K/min, 220. C @ 40. min; Column length: 60. m; Column diameter: 0.25 mm
CapillarySupelcowax-102445.Chung, 199960. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 2. K/min, 195. C @ 90. min
CapillarySupelcowax-102444.Chung, 1999, 260. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 2. K/min, 195. C @ 90. min
CapillaryDB-Wax2441.Shimoda, Shigematsu, et al., 199560. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 230. C
CapillaryDB-Wax2435.Shiratsuchi, Shimoda, et al., 199460. m/0.25 mm/0.25 μm, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillaryDB-Wax2435.Shiratsuchi, Shimoda, et al., 1994, 260. m/0.25 mm/0.25 μm, He, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillarySupelcowax-102444.Chung and Cadwallader, 199360. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 195. C @ 40. min

Van Den Dool and Kratz RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryFFAP2456.Jezussek, Juliano, et al., 200230. m/0.25 mm/0.25 μm, He; Program: 40C(1min) => 40C/min => 50C(2min) => 6C/min => 240C
CapillaryDB-Wax2412.Cantergiani, Brevard, et al., 200130. m/0.25 mm/0.25 μm; Program: 20C(30s) => fast => 60C => 4C/min => 220C (20min)
CapillaryFFAP2446.Yasuhara, 198750. m/0.25 mm/0.25 μm, He; Program: 20C (5min) => 2C/min => 70C => 4C/min => 210C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5 MS1293.Fanaro, Duarte, et al., 201230. m/0.25 mm/0.25 μm, Helium, 50. C @ 0.5 min, 5. K/min, 250. C @ 0.5 min
CapillaryOptima-5 MS1297.Goeminne, Vandendriessche, et al., 201230. m/0.25 mm/0.25 μm, Helium, 35. C @ 3. min, 10. K/min, 250. C @ 5. min
CapillaryHP-5 MS1294.Kotowska, Zalikowski, et al., 201230. m/0.25 mm/0.25 μm, Helium, 35. C @ 5. min, 3. K/min, 300. C @ 15. min
CapillaryHP-5 MS1289.Nawrath, Mgode, et al., 201230. m/0.25 mm/0.25 μm, Helium, 50. C @ 5. min, 5. K/min; Tend: 320. C
CapillaryHP-5 MS1299.Miyazawa, Marumoto, et al., 201130. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C
CapillaryHP-5 MS1300.Radulovic, Blagojevic, et al., 201030. m/0.25 mm/0.25 μm, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C
CapillaryZB-51303.Harrison and Priest, 200930. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 6. K/min, 280. C @ 9. min
CapillaryHP-5 MS1287.Kim and Chung, 200930. m/0.25 mm/0.25 μm, Helium, 35. C @ 5. min, 2. K/min, 195. C @ 30. min
CapillarySLB-5MS1316.Risticevic, Carasek, et al., 200810. m/0.18 mm/0.18 μm, Helium, 40. C @ 1.5 min, 10. K/min; Tend: 295. C
CapillaryRTX-5 MS1297.Edris, Chizzola, et al., 200730. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 2. K/min, 200. C @ 10. min
CapillaryZP-51254.Füssel, Dötterl, et al., 200760. m/0.25 mm/0.25 μm, He, 40. C @ 7. min, 6. K/min, 260. C @ 1. min
CapillaryElite-5MS1282.Tava, Pecetti, et al., 200730. m/0.32 mm/0.5 μm, He, 40. C @ 5. min, 4. K/min, 280. C @ 10. min
CapillaryHP-51300.Bertrand, Comte, et al., 200660. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 250. C
CapillaryBPX-51320.Fons, Rapior, et al., 200625. m/0.20 mm/0.13 μm, Helium, 50. C @ 2. min, 3. K/min; Tend: 230. C
CapillaryCP Sil 8 CB1297.Li, Lee, et al., 200630. m/0.25 mm/0.25 μm, 40. C @ 5. min, 3. K/min, 250. C @ 20. min
CapillaryDB-51295.Morteza-Semnani, Saeedi, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 4. min, 4. K/min; Tend: 260. C
CapillarySPB-51288.Pino, Marquez, et al., 200630. m/0.25 mm/0.25 μm, Helium, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillaryDB-51303.Rout, Naik, et al., 200630. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 60. min; Tstart: 60. C
CapillaryDB-51303.Rout, Naik, et al., 200630. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 60. min; Tstart: 60. C
CapillaryDB-51301.Senatore, Landolfi, et al., 200630. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min
CapillaryHP-11278.Valette, Fernandez, et al., 200650. m/0.2 mm/0.5 μm, He, 2. K/min, 250. C @ 40. min; Tstart: 60. C
CapillaryHP-11256.Bendimerad and Bendiab, 200550. m/0.2 mm/0.5 μm, He, 2. K/min, 250. C @ 60. min; Tstart: 60. C
CapillaryPolymethylsiloxane, (PMS-20000)1260.Dohou, Yamni, et al., 2005He, 50. C @ 3. min, 3. K/min; Column length: 25. m; Column diameter: 0.20 mm; Tend: 250. C
CapillaryZB-51307.Dötterl and Jürgens, 200560. m/0.25 mm/0.25 μm, He, 40. C @ 7. min, 6. K/min, 250. C @ 1. min
CapillaryZB-51307.Dötterl, Wolfe, et al., 200560. m/0.25 mm/0.25 μm, He, 40. C @ 7. min, 6. K/min, 250. C @ 1. min
CapillaryHP-51329.6Leffingwell and Alford, 200560. m/0.32 mm/0.25 μm, He, 30. C @ 2. min, 2. K/min, 260. C @ 28. min
CapillaryDB-51283.Miyazawa, Nishiguchi, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillarySPB-51288.Pino, Marbot, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillaryDB-51301.Senatore, Apostolides Arnold, et al., 200530. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min
CapillaryZB-51310.Jürgens and Dötterl, 200460. m/0.25 mm/0.25 μm, He, 40. C @ 4.6 min, 6. K/min, 260. C @ 1. min
CapillaryDB-5MS1327.Robledo and Arzuffi, 200430. m/0.25 mm/0.25 μm, 30. K/min, 200. C @ 10. min; Tstart: 90. C
CapillaryDB-11277.Perez-Alonso, Velasco-Negueruela, et al., 200350. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryHP-11248.Valette, Fernandez, et al., 200350. m/0.2 mm/0.5 μm, He, 2. K/min, 220. C @ 40. min; Tstart: 60. C
CapillaryBPX-51301.Diaz and Kite, 20025. K/min; Tstart: 40. C; Tend: 260. C
CapillaryDB-51287.Kobaisy, Tellez, et al., 200230. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51289.Tellez, Khan, et al., 200230. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-5MS1296.Fernando and Grün, 200160. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 3. K/min; Tend: 250. C
CapillaryDB-5MS1296.Fernando and Grün, 200160. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 3. K/min; Tend: 250. C
CapillaryAT-11282.Kelling, 2001He, 50. C @ 2. min, 10. K/min; Tend: 300. C
CapillaryDB-51288.Tellez, Canel, et al., 199930. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51286.El-Sakhawy, El-Tantawy, et al., 199830. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-11260.Boatright and Crum, 199730. m/0.25 mm/0.1 μm, He, 50. C @ 2. min, 5. K/min, 300. C @ 3. min
CapillaryHP-11260.Boatright and Crum, 199730. m/0.25 mm/0.1 μm, He, 50. C @ 2. min, 5. K/min, 300. C @ 3. min
CapillaryOV-1011304.Egolf and Jurs, 19932. K/min; Column length: 50. m; Column diameter: 0.22 mm; Tstart: 80. C; Tend: 200. C
CapillaryDB-51328.Moio, Dekimpe, et al., 199330. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryDB-51329.Moio, Dekimpe, et al., 199330. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryDB-51340.Moio, Langlois, et al., 199330. m/0.32 mm/1. μm, H2, 40. C @ 5. min, 5. K/min; Tend: 220. C
CapillarySE-301270.4Bur'yan and Nabivach, 19921.7 K/min; Tstart: 82. C; Tend: 177. C
CapillarySE-301275.2Bur'yan and Nabivach, 19921.7 K/min; Tstart: 82. C; Tend: 177. C
CapillaryUltra-11248.Okumura, 199125. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 80. C; Tend: 260. C
CapillaryDB-11250.Buttery, Takeoka, et al., 199030. C @ 25. min, 4. K/min, 200. C @ 30. min; Column length: 60. m
CapillaryHP-51303.Spadone, Takeoka, et al., 1990H2, 16. K/min; Column length: 50. m; Column diameter: 0.3 mm; Tstart: 80. C; Tend: 250. C
CapillaryOV-1011277.Wu, Zhao, et al., 1987He, 3. K/min; Column length: 45. m; Column diameter: 0.25 mm; Tstart: 100. C; Tend: 180. C
CapillaryDB-11248.Flath, Mon, et al., 198350. C @ 0.1 min, 4. K/min, 250. C @ 5. min; Column length: 60. m; Column diameter: 0.32 mm

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5 MS1292.Kotowska, Zalikowski, et al., 201230. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryHP-5 MS1290.Mancini, Arnold, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
CapillaryDB-11255.Mendes, Trindade, et al., 200930. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)
CapillaryDB-11255.Mendes, Trindade, et al., 2009, 230. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)
CapillaryCP-Sil 8CB-MS1298.Profitt, Schatz, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 50 0C(3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 260 0C
CapillarySLB-5MS1297.Risticevic, Carasek, et al., 200810. m/0.18 mm/0.18 μm, Helium; Program: not specified
CapillaryDB-5 MS1251.Zhu, Li, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (2.8 min) 5.5 0C/min -> 140 0C (1 min) 4.5 oC/min -> 220 0C -> 225 0C (2 min) 3.4 0C/min -> 265 0C (5 min)
CapillaryDB-5 MS1289.Zhu, Li, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (2.8 min) 5.5 0C/min -> 140 0C (1 min) 4.5 oC/min -> 220 0C -> 225 0C (2 min) 3.4 0C/min -> 265 0C (5 min)
CapillaryHP-5 MS1340.Chuang, Lee, et al., 200730. m/0.25 mm/0.25 μm, Hydrogen; Program: 50 0C (15 min) 2 0C/min -> 150 0C (10 min) 2 0C/min -> 220 0C (20 min)
CapillaryDB-5 MS1293.Liu, Xu, et al., 200760. m/0.32 mm/1.0 μm, Helium; Program: 40 0C (2 min) 6 0C/min -> 100 0C 4 0C/min -> 180 0C 8 0C/min -> 250 0C (12 min)
CapillaryCP Sil 8 CB1293.Meekijjaroenroj, Bessière, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 50C(3min) => 3C/min => 100C => 2.7C/min => 140C => 2.4C/min => 180C => 6C/min => 250C
CapillaryCP-Sil1279.Proffit, 200730. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C
CapillaryCP-Sil1292.Proffit, 200730. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C
CapillaryCP-Sil1298.Proffit, 200730. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C
CapillaryCP-Sil1298.Proffit, 200730. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C
CapillaryHP-5MS1290.Senatore, Apostolides Arnold, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillaryVF-5MS1283.Xie, Sun, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 40C(1min) => 15C/min => 100C => 4C/min => 250C (1min)
CapillaryDB-11255.Belhattab, Larous, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 300C(10min)
CapillaryPolydimethyl siloxane with 5 % Ph groups1288.Pino, Marbot, et al., 2005, 2Program: not specified
CapillarySE-541293.Buettner, 200430. m/0.32 mm/0.25 μm, He; Program: 40C(2min) => 40C/min => 50C(2min) => 6C/min => 180C => 15C/min => 230C (10min)
CapillarySE-301304.Vinogradov, 2004Program: not specified
CapillarySPB-51305.Begnaud, Pérès, et al., 200360. m/0.32 mm/1. μm; Program: not specified
CapillaryBPX-51304.Machiels, van Ruth, et al., 200360. m/0.32 mm/1. μm, He; Program: 40C (4min) => 2C/min => 90C => 4C/min => 130C => 8C/min => 250 C (10min)
CapillaryDB-5MS1303.Young, Lane, et al., 200330. m/0.25 mm/1. μm; Program: 50C => 3C/min => 160C => 6C/min => 250C => 25C/min => 325C
CapillaryCP Sil 5 CB1276.Counet, Callemien, et al., 200250. m/0.32 mm/1.2 μm; Program: 36C => 20C/min => 85C => 1C/min => 145C=3C/min => 250C(30min)
CapillaryHP-5MS1294.Ansorena, Gimeno, et al., 200130. m/0.25 mm/0.25 μm, He; Program: 40C (10min) => 3C/min => 120C => 10C/min => 250C (5min)
CapillaryCP Sil 5 CB1269.Guyot, Scheirman, et al., 1999He; Column length: 50. m; Column diameter: 0.32 mm; Program: 30C => 55C/min => 85C => 1C/min => 145C => 3C/min => 250C
CapillaryDB-51305.Young and Baumeister, 199930. m/0.53 mm/1. μm; Program: -40C(10min) => 70C/min => 40C(5min) => 3C/min => 180C => 6C/min => 280C(5min)
CapillaryDB-51292.Schieberle, 1996Column length: 30. m; Column diameter: 0.32 mm; Program: not specified
CapillaryDB-11264.Kawai, Ishida, et al., 199160. m/0.25 mm/0.25 μm; Program: not specified
CapillaryDB-11265.Kawai, Ishida, et al., 199160. m/0.25 mm/0.25 μm; Program: not specified
CapillaryOV-1011304.Shibamoto, 1987Program: not specified
CapillaryOV-1011304.Wu, Zhao, et al., 1987He; Column length: 45. m; Column diameter: 0.25 mm; Program: not specified
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.1276.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
OtherMethyl Silicone1276.Ardrey and Moffat, 1981Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryTC-Wax2454.Miyazawa, Fujita, et al., 2010Helium, 40. C @ 3. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 230. C
CapillaryInnowax2451.Kaypak and Avsar, 200830. m/0.25 mm/0.25 μm, 40. C @ 5. min, 10. K/min, 200. C @ 15. min
CapillaryFFAP2476.Nebesny, Budryn, et al., 200730. m/0.32 mm/0.5 μm, N2, 35. C @ 5. min, 4. K/min, 320. C @ 45. min
CapillaryDB-Wax2414.Kishimoto, Wanikawa, et al., 200615. m/0.32 mm/0.25 μm, He, 6. K/min, 230. C @ 20. min; Tstart: 40. C
CapillaryInnowax2463.Joichi, Yomogida, et al., 200560. m/0.25 mm/0.25 μm, He, 5. K/min, 240. C @ 30. min; Tstart: 60. C
CapillaryDB-Wax2436.Ito, Sugimoto, et al., 200260. C @ 4. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 180. C
CapillaryDB-Wax2448.Kumazawa and Masuda, 200230. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax2451.Kumazawa and Masuda, 200260. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryTC-WAX FFS2431.Miyazawa, Maehara, et al., 2002He, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 240. C
CapillaryDB-Wax2444.Kumazawa and Masuda, 200130. m/0.53 mm/1. μm, He, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryPEG-20M2475.Hirose, Joichi, et al., 1999N2, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 220. C
CapillaryDB-Wax2478.Iwatsuki, Mizota, et al., 19994. K/min; Column length: 30. m; Column diameter: 0.53 mm; Tstart: 60. C; Tend: 210. C
CapillaryDB-Wax2460.Iwatsuki, Mizota, et al., 19994. K/min; Column length: 30. m; Column diameter: 0.53 mm; Tstart: 60. C; Tend: 210. C
CapillaryDB-Wax2444.Kumazawa and Masuda, 199930. m/0.53 mm/1. μm, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryDB-Wax2450.Kumazawa and Masuda, 199960. m/0.25 mm/0.25 μm, 5. K/min; Tstart: 40. C; Tend: 210. C
CapillaryPEG-20M2463.Awano, Ichikawa, et al., 19973. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 220. C
CapillaryTC-Wax2465.Shuichi, Masazumi, et al., 199680. C @ 5. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 240. C
CapillaryPEG-20M2398.Kubota, Nakamoto, et al., 1991N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 180. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-Wax2426.Kaprasob, Laohankunjit, et al., 2011Program: 55 0C (2 min) 5 0C/min -> 180 0C (5 min) 8 0C/min -> 230 0C (10 min)
CapillaryInnowax2471.Noorizadeh, Farmany, et al., 201160. m/0.25 mm/0.33 μm; Program: not specified
CapillaryPolyethylene glycol (Free Fatty Acid Phase)2455.Harraca, Syed, et al., 2009Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryPolyethylene glycol (Free Fatty Acid Phase)2455.Harraca, Syed, et al., 2009Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryHP Innowax2471.Mancini, Arnold, et al., 200950. m/0.20 mm/0.25 μm, Helium; Program: 40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
CapillaryHP-Innowax2471.Senatore, Apostolides Arnold, et al., 200650. m/0.2 mm/0.2 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillaryDB-FFAP2450.Buettner, 200430. m/0.32 mm/0.25 μm, He; Program: 40C(2min) => 40C/min => 60C(2min) => 6C/min => 180C => 15C/min => 230C (10min)

Lee's RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-5220.80Rostad and Pereira, 198630. m/0.26 mm/0.25 μm, He, 50. C @ 4. min, 6. K/min, 300. C @ 20. min
CapillarySE-52222.66Vassilaros, Kong, et al., 198220. m/0.30 mm/0.25 μm, H2, 40. C @ 2. min, 4. K/min; Tend: 265. C
CapillarySE-52205.26Lee, Vassilaros, et al., 197912. m/0.3 mm/0.34 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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