Fenchone


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSVF-5 MSVF-5 MSCP-Sil 5 CBDB-1-MS
Column length (m) 30.60.60.30.60.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.250.250.250.260.25
Tstart (C) 35.30.30.45.30.
Tend (C) 300.260.260.280.200.
Heat rate (K/min) 3.2.2.3.2.
Initial hold (min) 5.   4.
Final hold (min) 15.28.28.22.35.
I 1084.1090.1091.1069.1063.
ReferenceKotowska, Zalikowski, et al., 2012Leffingwell and Alford, 2011Leffingwell and Alford, 2011Mothana, Hasson, et al., 2011Takeoka, Hobbs, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-5 MSZB-5DB-1
Column length (m) 25.30.30.30.50.
Carrier gas HeliumHeliumHelium He
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 60.50.60.60.95.
Tend (C) 240.230.200.220.240.
Heat rate (K/min) 3.3.4.4.4.
Initial hold (min)  10. 5. 
Final hold (min) 7.10.20.20. 
I 1088.1088.1085.1090.1074.
ReferenceMaridass, 2009Adams, Beauchamp, et al., 2007Araque, Rojas, et al., 2007Mohottalage, Tabacchi, et al., 2007Pala-Paul, Brophy, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-52DB-1HP-5MSHP-5MS
Column length (m) 60.50.50.30.30.
Carrier gas  HeliumN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.50.95.60.60.
Tend (C) 250.240.240.280.280.
Heat rate (K/min) 5.3.4.3.4.
Initial hold (min)      
Final hold (min)      
I 1075.1087.1081.1052.1089.
ReferenceSalehi, Asghari, et al., 2007Ozcan, Chalchat, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pitarokili, Tzakou, et al., 2006Sajjadi, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1HP-1DB-1HP-5MS
Column length (m) 60.30.50.50.30.
Carrier gas HeliumHeHe He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.50.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 250.250.250.240.280.
Heat rate (K/min) 5.4.2.3.3.
Initial hold (min)  1.   
Final hold (min) 10.10.60.  
I 1073.1057.1075.1060.1087.
ReferenceSonboli, Mirjalili, et al., 2006Wong, Sivasothy, et al., 2006Bendimerad and Bendiab, 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005Malencic, Couladis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5RSL-200RSL-200CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas  HeH2H2He
Substrate      
Column diameter (mm) 0.320.2490.320.320.25
Phase thickness (μm) 0.250.250.250.250.39
Tstart (C) 50.60.40.40.60.
Tend (C) 200.300.280.280.220.
Heat rate (K/min) 5.3.6.6.5.
Initial hold (min) 5. 5.5. 
Final hold (min)   5.5. 
I 1093.1085.1078.1080.1071.
ReferenceWang, Guo, et al., 2004Woerdenbag, Windono, et al., 2004Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Khanavi, Hadjiakhoondi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-5HP-5HP-5
Column length (m) 30.50.25.30.30.
Carrier gas HeliumN2N2He 
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm)  0.250.250.25 
Tstart (C) 70.95.50.60.50.
Tend (C) 210.240.250.275.200.
Heat rate (K/min) 2.4.4.4.3.
Initial hold (min)      
Final hold (min) 60. 10.  
I 1087.1076.1088.1087.1090.
ReferenceMookdasanit, Tamura, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Zrira, Elamrani, et al., 2003Ghannadi, Sajjadi, et al., 2002Isidorov and Jdanova, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5OV-101DB-1DB-5MSDB-5MS
Column length (m) 60.50.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.50.250.250.25
Tstart (C) 50.50.50.60.60.
Tend (C) 240.250.250.270.240.
Heat rate (K/min) 5.2.4.3.3.
Initial hold (min) 3. 5.  
Final hold (min) 10.    
I 1099.1066.1070.1086.1086.
ReferenceKim and Lee, 2002Orav, Kailas, et al., 2002Yamini, Sefidkon, et al., 2002Zoghbi, Andrade, et al., 2002Cherchi, Deidda, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101HP-5 MSSPB-1HP-5DB-1
Column length (m) 50.30.30.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.20.250.20.250.25
Phase thickness (μm)  0.250.2 0.25
Tstart (C) 50.50.80.80.40.
Tend (C) 250.250.300.200.260.
Heat rate (K/min) 2.5.5.9.2.
Initial hold (min)  2.3. 5.
Final hold (min)  5. 10.2.
I 1064.1078.1088.1083.1067.
ReferenceOrav and Kann, 2001Shang, Hu, et al., 2001Fraternale, Giamperi, et al., 2000Lis-Balchin and Roth, 2000Senatore, Napolitano, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5HP-1OV-101DB-1
Column length (m) 25.30.60.25.60.
Carrier gas H2HeHe He
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm) 0.170.250.25 0.25
Tstart (C) 40.40.50.50.50.
Tend (C) 260.250.280.200.250.
Heat rate (K/min) 3.2.4.5.2.5
Initial hold (min) 5.5.5. 5.
Final hold (min)  60.   
I 1058.1069.1086.1080.1076.
ReferenceLopes, Koketsu, et al., 1999Porta, Porcedda, et al., 1999Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998Stashenko, Puertas, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1Methyl SiliconeOV-101OV-101SE-54
Column length (m) 50.25.50.50.30.
Carrier gas N2   Hydrogen
Substrate      
Column diameter (mm) 0.270.500.250.250.25
Phase thickness (μm) 0.2   0.25
Tstart (C) 80.60.80.80.60.
Tend (C) 240.220.200.200.250.
Heat rate (K/min) 3.5.2.2.2.
Initial hold (min)     5.
Final hold (min)     2.
I 1072.1075.1072.1072.1083.
ReferenceRamanoelina, Viano, et al., 1994Mallavarapu, Ramesh, et al., 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase BP-1
Column length (m) 25.
Carrier gas  
Substrate  
Column diameter (mm) 0.33
Phase thickness (μm)  
Tstart (C) 45.
Tend (C) 180.
Heat rate (K/min) 3.
Initial hold (min) 3.
Final hold (min)  
I 1067.
ReferenceWyllie, Brophy, et al., 1990
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Lis-Balchin and Roth, 2000
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Senatore, Napolitano, et al., 2000
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Lopes, Koketsu, et al., 1999
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Porta, Porcedda, et al., 1999
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Stashenko, Cervantes, et al., 1998
Stashenko, E.E.; Cervantes, M.; Combariza, Y.; Martínez, J.R., HRGC-FID-MSD Analysis of the Secondary Metabolites Obtained by Different Extraction Methods from Lepechinia schiedeana, and Evaluation of its Antioxidant Activity in vitro in 20th International Symposium on Capillary Chromatography, 1998, 1-11. [all data]

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Stashenko, Puertas, et al., 1996
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Ramanoelina, Viano, et al., 1994
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Mallavarapu, Ramesh, et al., 1993
Mallavarapu, G.R.; Ramesh, S.; Kaul, P.N.; Battacharya, A.K.; Rao, B.R.R., The essential oil of Hyptis suaveolens (L.) Poit., J. Essent. Oil Res., 1993, 5, 3, 321-323, https://doi.org/10.1080/10412905.1993.9698230 . [all data]

Tamura, Yang, et al., 1993
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Kollmannsberger, Nitz, et al., 1992
Kollmannsberger, H.; Nitz, S.; Drawert, F., UBer die Aromastoffzusammensetzung von Hochdruckextrakten. I. Pfeffer (Piper nigrum, Var. muntok), Z. Lebensm. Unters Forsch., 1992, 194, 6, 545-551, https://doi.org/10.1007/BF01185481 . [all data]

Wyllie, Brophy, et al., 1990
Wyllie, S.G.; Brophy, J.J.; Sarafis, V.; Hobbs, M., Volatile Components of the Fruit of Pistacia Lentiscus, J. Food. Sci., 1990, 55, 5, 1325-1326, https://doi.org/10.1111/j.1365-2621.1990.tb03926.x . [all data]


Notes

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