Met isoBOC TBDMS
- Formula: C16H33NO4SSi
- Molecular weight: 363.588
- IUPAC Standard InChI: InChI=1S/C16H33NO4SSi/c1-12(2)11-20-15(19)17-13(9-10-22-6)14(18)21-23(7,8)16(3,4)5/h12-13H,9-11H2,1-8H3,(H,17,19)
- IUPAC Standard InChIKey: GWYLUFZOASAFRB-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Met, N-isoBOC TBDMS
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Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | DB-5 | DB-5 |
| Column length (m) | 30. | 30. |
| Carrier gas | ||
| Substrate | ||
| Column diameter (mm) | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.24 |
| Tstart (C) | 150. | 150. |
| Tend (C) | 280. | 280. |
| Heat rate (K/min) | 3. | 3. |
| Initial hold (min) | 2. | 2. |
| Final hold (min) | ||
| I | 2135. | 2134. |
| Reference | Oh, Kim, et al., 1994 | Kim, Kim, et al., 1992 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Oh, Kim, et al., 1994
Oh, C.-H.; Kim, J.-H.; Kim, K.-R.; Brownson, D.M.; Mabry, T.J.,
Simultaneous gas chromatographic analysis of non-protein and protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives,
J. Chromatogr. A, 1994, 669, 1-2, 125-137, https://doi.org/10.1016/0021-9673(94)80344-7
. [all data]
Kim, Kim, et al., 1992
Kim, K.-R.; Kim, J.-H.; Oh, C.-H.; Mabry, T.J.,
Capillary gas chromatography of protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives in aqueous samples,
J. Chromatogr., 1992, 605, 2, 241-249, https://doi.org/10.1016/0021-9673(92)85242-L
. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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