6α-Methylprednisolone, bis-MO-tris-TMS
- Formula: C33H60N2O5Si3
- Molecular weight: 649.0964
- IUPAC Standard InChI: InChI=1S/C33H60N2O5Si3/c1-23-19-25-26-16-18-33(40-43(12,13)14,29(35-37-5)22-38-41(6,7)8)32(26,3)21-28(39-42(9,10)11)30(25)31(2)17-15-24(34-36-4)20-27(23)31/h15,17,20,23,25-26,28,30H,16,18-19,21-22H2,1-14H3/t23-,25-,26-,28-,30+,31-,32-,33-/m1/s1
- IUPAC Standard InChIKey: GNINHLKSWIXWMN-CIJFTMPRSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Normal alkane RI, non-polar column, custom temperature program
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | HP-1 | HP-1 |
| Column length (m) | 17. | 17. |
| Carrier gas | Helium | Helium |
| Substrate | ||
| Column diameter (mm) | 0.20 | 0.20 |
| Phase thickness (μm) | 0.11 | 0.11 |
| Program | 180 0C 3 0C/min -> 229 0C 40 0C/min -> 310 0C (5 min) | 180 0C 3 0C/min -> 229 0C 40 0C/min -> 310 0C (5 min) |
| I | 2972. | 2997. |
| Reference | Pereira, Marques, et al., 2001 | Pereira, Marques, et al., 2001 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Pereira, Marques, et al., 2001
Pereira, H.M.G.; Marques, M.A.S.; Cardoso, J.N.; Neto, F.R.A.,
Derivatization study of endogenous and synthetic corticosteroids by gas chromatography mass spectrometry
in Recent Advances in Doping Analysis, Schanzer, W.; Geyer, H.; Gotzmann, A.; Mareck-Engelke, U., ed(s)., Sport und Buch Strauss, Koln, 2001, 203-207. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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