3α,16α-dihydroxy-5β-androstan-17-one, TMS
- Formula: C25H46O3Si2
- Molecular weight: 450.8019
- IUPAC Standard InChI: InChI=1S/C25H46O3Si2/c1-24-13-11-18(27-29(3,4)5)15-17(24)9-10-19-20(24)12-14-25(2)21(19)16-22(23(25)26)28-30(6,7)8/h17-22H,9-16H2,1-8H3/t17-,18-,19?,20?,21?,22-,24+,25+/m0/s1
- IUPAC Standard InChIKey: JTMVSMLYJSJYTE-KAVSHOJGSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | OV-1 | 2604. | Bègue, Dumas, et al., 1979 | He, 1. K/min; Tstart: 180. C; Tend: 250. C |
| Capillary | SE-30 | 2556. | Bègue, Dumas, et al., 1979 | N2, 1. K/min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 210. C; Tend: 260. C |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Bègue, Dumas, et al., 1979
Bègue, R.-J.; Dumas, M.; Morinière, M.; Nivois, C.; Padieu, P.,
Steroids and hypertension. 1-Gas-liquid chromatography and gas chromatography mass spectrometry of 3,15- and 3,16-dihydroxy-17-oxosteroids,
Biomed. Mass Spectrom., 1979, 6, 11, 476-481, https://doi.org/10.1002/bms.1200061104
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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