Hippuric acid, TMS derivative
- Formula: C12H17NO3Si
- Molecular weight: 251.3538
- IUPAC Standard InChI: InChI=1S/C12H17NO3Si/c1-17(2,3)16-11(14)9-13-12(15)10-7-5-4-6-8-10/h4-8H,9H2,1-3H3,(H,13,15)
- IUPAC Standard InChIKey: BKKRGGOJGSDXNW-UHFFFAOYSA-N
- CAS Registry Number: 2078-24-2
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: Glycine, N-benzoyl-, trimethylsilyl ester; Hippuric acid, trimethylsilyl ester; Hippuric acid, mono-TMS; Hippuric acid, TMS # 2
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Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | HP-5MS | HP-5 |
| Column length (m) | 30. | 25. |
| Carrier gas | He | He |
| Substrate | ||
| Column diameter (mm) | 0.25 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.52 |
| Tstart (C) | 70. | 70. |
| Tend (C) | 280. | 280. |
| Heat rate (K/min) | 4. | 5. |
| Initial hold (min) | 3. | 10. |
| Final hold (min) | 3. | |
| I | 1822. | 1844. |
| Reference | Lee, Yanamandra, et al., 2002 | Richards, Wong, et al., 1992 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Lee, Yanamandra, et al., 2002
Lee, B.Y.; Yanamandra, K.; Thurmon, T.F.,
Quantitative estimation of organic analytes with a capillary column,
Am. Clin. Lab., 2002, May, 30-34. [all data]
Richards, Wong, et al., 1992
Richards, M.; Wong, Y.S.; Tan, W.C.; Tan, I.K.; Ng, T.L.,
Profiling urinary organic acids for the diagnosis of inborn errors of metabolism by GC/MS,
Bull. Sing. N.I. Chem., 1992, 20, 135-143. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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