Androst-5-ene-3,17-diol, (3«beta»,17«alpha»)-, 2TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1235.2600.Smith, Joannou, et al., 1978N2, Gas-Chrom Q (100-120 mesh); Column length: 2.5 m
PackedOV-101207.2582.Berthou, Picart, et al., 1976Column length: 2.1 m
CapillaryOV-101252.2598.Berthou, Picart, et al., 1976Column length: 55. m; Column diameter: 0.37 mm
CapillaryOV-101252.2600.Berthou, Picart, et al., 1976Column length: 55. m; Column diameter: 0.37 mm

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-12593.Bowers, 199630. m/0.25 mm/0.25 «mu»m, Helium; Program: 170 0C 20 0C/min -> 260 0C 2.7 0C/min -> 305 0C 20 0C/min -> 320 0C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Smith, Joannou, et al., 1978
Smith, A.G.; Joannou, G.E.; Mák, M.; Uwajima, T.; Terada, O.; Brooks, C.J.W., Oxidation of 3«beta»-hydroxyandrostenes by the 3«beta»-hydroxysteroid oxidase (cholesterol oxidase) from Brevibacterium sterolicum prior to their analysis by gas-liquid chromatography-mass spectrometry, J. Chromatogr., 1978, 152, 2, 467-474, https://doi.org/10.1016/S0021-9673(00)85083-9 . [all data]

Berthou, Picart, et al., 1976
Berthou, F.; Picart, D.; Bardou, L.; Floch, H.H., Separation of C19 and C21 dihydroxysteroids by open-hole tubular glass columns and lipophilic gel chromatography, J. Chromatogr., 1976, 118, 2, 135-155, https://doi.org/10.1016/S0021-9673(00)81203-0 . [all data]

Bowers, 1996
Bowers, L.D., Separation and confirmation of anabolic steroids with quadrupole ion trap tandem mass spectrometry, J. Chromatogr. B, 1996, 687, 1, 69-78, https://doi.org/10.1016/S0378-4347(96)00231-9 . [all data]


Notes

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