5β-Androstan-3β-ol-17-one, TMS derivative
- Formula: C22H38O2Si
- Molecular weight: 362.6214
- IUPAC Standard InChI: InChI=1S/C22H38O2Si/c1-21-12-10-16(24-25(3,4)5)14-15(21)6-7-17-18-8-9-20(23)22(18,2)13-11-19(17)21/h15-19H,6-14H2,1-5H3/t15-,16+,17+,18+,19+,21+,22+/m0/s1
- IUPAC Standard InChIKey: RKALSSDGCWGKHQ-SSLWXMMXSA-N
- CAS Registry Number: 10426-96-7
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Stereoisomers:
- Other names: Androstan-17-one, 3-[(trimethylsilyl)oxy]-, (3β,5β)-; Etiocholan-3α-ol-17-one, trimethylsilyl ether; 5β-Androstan-17-one, 3β-(trimethylsiloxy)-; 3β-Trimethylsilyloxy-5β-androstan-17-one; 3-[(Trimethylsilyl)oxy]androstan-17-one, (3β,5β)-; 3β-Hydroxy-5β-androstan-17-one, TMS; Ethiocholan-3.alpha.-ol-17-one, trimethylsilyl ether; 3B-Hydroxy-5B-androstan-17-one, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 2495. | Ludwig-Koehn and Henning, 1986 | 30. m/0.25 mm/0.25 μm, H2, 2. K/min; Tstart: 120. C; Tend: 280. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 2574.5 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Ludwig-Koehn and Henning, 1986
Ludwig-Koehn, H.; Henning, H.V.,
Some aspects of quantification of neutral steroid metabolites in body fluids of healthy and uremic subjects by capillary gas chromatography,
J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 1, 35-38, https://doi.org/10.1002/jhrc.1240090106
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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