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Androstane-3,17-diol, (3«alpha»,5«alpha»,17«alpha»)-, 2TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, isothermal

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Column typeActive phaseTemperature (C)IReferenceComment
PackedOV-101207.2464.Berthou, Picart, et al., 1976Column length: 2.1 m
CapillaryOV-101252.2476.Berthou, Picart, et al., 1976Column length: 55. m; Column diameter: 0.37 mm

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryBP-12474.Houghton, Ginn, et al., 1989H2, 5. K/min; Column length: 25. m; Column diameter: 0.3 mm; Tstart: 150. C; Tend: 300. C
CapillaryBP-52489.Houghton, Ginn, et al., 1989H2, 5. K/min; Column length: 25. m; Column diameter: 0.3 mm; Tstart: 150. C; Tend: 300. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Berthou, Picart, et al., 1976
Berthou, F.; Picart, D.; Bardou, L.; Floch, H.H., Separation of C19 and C21 dihydroxysteroids by open-hole tubular glass columns and lipophilic gel chromatography, J. Chromatogr., 1976, 118, 2, 135-155. [doi:10.1016/S0021-9673(00)81203-0] [all data]

Houghton, Ginn, et al., 1989
Houghton, E.; Ginn, A.; Teale, P.; Dumasia, M.C.; Copsey, J., Comparison of the use of mass spectrometry and methylene unit values in the determination of the stereochemistry of estranediol, the major urinary metabolite of 19-nortestosterone in the horse, J. Chromatogr., 1989, 479, 73-83. [doi:10.1016/S0021-9673(01)83318-5] [all data]


Notes

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