Prednisolone, MO TMS
- Formula: C36H70N2O5Si5
- Molecular weight: 751.3789
- IUPAC Standard InChI: InChI=1S/C36H70N2O5Si5/c1-34-22-20-28(37-42-47(12,13)14)24-27(34)18-19-29-30-21-23-36(41-46(9,10)11,32(26-39-44(3,4)5)38-43-48(15,16)17)35(30,2)25-31(33(29)34)40-45(6,7)8/h20,22,24,29-31,33H,18-19,21,23,25-26H2,1-17H3/t29?,30?,31?,33?,34?,35?,36-/m1/s1
- IUPAC Standard InChIKey: REIKNJJJDMOPBV-HUGFTRFBSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Prednisolone (1-dehydrocortisol), MO-TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | ZB-1 | 3280. | Ebner, Corol, et al., 2006 | 30. m/0.25 mm/0.25 μm, He; Program: 70C(5min) => 20C/min => 220C(0.33min) => 5C/min => 315C (4min) |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Methyl Silicone | 3269. | Rodchenkov, Vedenin, et al., 1991 | 12.5 m/0.20 mm/0.33 μm, He; Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Ebner, Corol, et al., 2006
Ebner, M.J.; Corol, D.I.; Havlíková, H.; Honour, J.W.; Fry, J.P.,
Identification of neuroactive steroids and their precursors and metabolites in adult male rat brain,
Endocrinology, 2006, 147, 1, 179-190, https://doi.org/10.1210/en.2005-1065
. [all data]
Rodchenkov, Vedenin, et al., 1991
Rodchenkov, G.M.; Vedenin, A.N.; Uralets, V.P.; Semenov, V.A.,
Characterization of prednisone, prednisolone and their metabolites by gas chromatography-mass spectrometry,
J.Chromatography - Biomedical Applications, 1991, 565, 1-2, 45-51, https://doi.org/10.1016/0378-4347(91)80369-N
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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