Cyclohexanol, 5-methyl-2-(1-methylethyl)-, (1α,2β,5α)-
- Formula: C10H20O
- Molecular weight: 156.2652
- IUPAC Standard InChIKey: NOOLISFMXDJSKH-KXUCPTDWSA-N
- CAS Registry Number: 89-78-1
- Chemical structure:
This structure is also available as a 2d Mol file - Species with the same structure:
- Stereoisomers:
- Cyclohexanol, 5-methyl-2-(1-methylethyl)-
- Cyclohexanol, 5-methyl-2-(1-methylethyl)-, [1R-(1α,2α,5β)]-
- Levomenthol
- Cyclohexanol, 5-methyl-2-(1-methylethyl)-, [1S-(1α,2α,5β)]-
- Cyclohexanol, 5-methyl-2-(1-methylethyl)-, [1S-(1α,2β,5β)]-
- Cyclohexanol, 5-methyl-2-(1-methylethyl)-, (1α,2β,5β)-
- Cyclohexanol, 5-methyl-2-(1-methylethyl)-, (1α,2α,5β)-
- Cyclohexanol, 5-methyl-2-(1-methylethyl)-, (1α,2α,5α)-
- Other names: Menthol, cis-1,3,trans-1,4-; Hexahydrothymol; Menthacamphor; Menthol; Menthomenthol; Peppermint camphor; dl-Menthol; p-Menthan-3-ol; Cyclohexanol, 2-isopropyl-5-methyl-; NCI-C50000; 5-Methyl-2-(1-methylethyl)cyclohexanol; 2-Isopropyl-5-methylcyclohexanol; l-Menthol; 3-p-Menthanol; 5α-Methyl-2β-(1α-methylethyl)cyclohexanol; component of Dermoplast; Fancol menthol; Fisherman's friend lozenges; Menthol terpine hydrate; component of Minut-rub; Racemic menthol; component of Robitussin cough drops; component of Sarna; component of Theragesic; Therapeutic mineral ice; Cyclohexanol, 2-isopropyl-5-methyl-, (1α,2β,5α)-; 2-Isopropyl-5-methylcyclohexanol, (1α,2β,5α)-; 5-Methyl-2-(1-methylethyl)cyclohexanol, (1α,2β,5α)-; (.+/-.)-Menthol; Cyclohexanol, 5-methyl-2-(1-methylethyl)-, (1R,2S,5R)-rel-; NSC 2603; Racementhol; rac-Menthol; Diterpene
- Information on this page:
- Other data available:
- Options:
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Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-5 MS | HP-5 | VF-5 MS | VF-5 MS |
Column length (m) | 30. | 30. | 30. | 60. | 60. |
Carrier gas | Helium | Helium | Helium | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 100. | 35. | 60. | 30. | 30. |
Tend (C) | 260. | 300. | 240. | 260. | 260. |
Heat rate (K/min) | 10. | 3. | 3. | 2. | 2. |
Initial hold (min) | 1. | 5. | |||
Final hold (min) | 10. | 15. | 28. | 28. | |
I | 1186. | 1170. | 1172. | 1180. | 1182. |
Reference | Boukhris, Bouaziz, et al., 2012 | Kotowska, Zalikowski, et al., 2012 | Bertoli, Lepnardi, et al., 2011 | Leffingwell and Alford, 2011 | Leffingwell and Alford, 2011 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 MS | DB-1 | HP-5 MS | DB-1 | DB-5 |
Column length (m) | 30. | 30. | 30. | 30. | 50. |
Carrier gas | Helium | Helium | Helium | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 70. | 50. | 50. | 30. | 50. |
Tend (C) | 290. | 220. | 280. | 210. | 280. |
Heat rate (K/min) | 5. | 4. | 4. | 5. | 5. |
Initial hold (min) | 2. | 2. | |||
Final hold (min) | 2. | 10. | |||
I | 1172. | 1154. | 1178. | 1171. | 1194. |
Reference | Lazarevic, Radulovic, et al., 2010 | Xu, Tang, et al., 2010 | Zhao, Zeng, et al., 2009 | Kumazawa, Itobe, et al., 2008 | Baranauskiene R., Bylaite E., et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 MS | SPB-5 | SPB-5 | HP-5MS | HP-5 |
Column length (m) | 30. | 60. | 60. | 30. | 30. |
Carrier gas | Helium | He | Helium | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 1. | 1. | 0.25 | 0.25 |
Tstart (C) | 60. | 40. | 40. | 60. | 40. |
Tend (C) | 280. | 230. | 230. | 280. | 240. |
Heat rate (K/min) | 3. | 3. | 3. | 3. | 4. |
Initial hold (min) | 5. | 5. | |||
Final hold (min) | 5. | 5. | 5. | ||
I | 1172. | 1185. | 1185. | 1172. | 1175. |
Reference | Vagionas, Graikou, et al., 2007 | Vasta, Ratel, et al., 2007 | Vasta, Ratel, et al., 2007 | Bozin, Mimicá-Dukic, et al., 2006 | Miyazawa and Kawata, 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Methyl Silicone | DB-5 | SPB-5 | BPX5 | HP-5 |
Column length (m) | 25. | 30. | 60. | 25. | 25. |
Carrier gas | N2 | He | He | Helium | He |
Substrate | |||||
Column diameter (mm) | 0.3 | 0.25 | 0.32 | 0.22 | 0.2 |
Phase thickness (μm) | 0.15 | 0.25 | 1. | 0.25 | 0.33 |
Tstart (C) | 50. | 40. | 40. | 50. | 60. |
Tend (C) | 210. | 250. | 230. | 320. | 240. |
Heat rate (K/min) | 2. | 4. | 3. | 5. | 3. |
Initial hold (min) | 5. | 5. | 5. | ||
Final hold (min) | 7. | ||||
I | 1191. | 1149. | 1186. | 1188. | 1179. |
Reference | Tonzibo, Coffy, et al., 2006 | Yadegarinia, Gachkar, et al., 2006 | Cornu, Kondjoyan, et al., 2005 | Dickschat, Bode, et al., 2005 | Duarte, Figueira, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | RSL-200 | HP-5 | DB-1 | PE-5 | HP-5 |
Column length (m) | 30. | 60. | 60. | 30. | 30. |
Carrier gas | He | He | H2 | Helium | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 30. | 60. | 60. | 40. |
Tend (C) | 280. | 260. | 250. | 230. | 250. |
Heat rate (K/min) | 6. | 2. | 5. | 5. | 5. |
Initial hold (min) | 2. | 2. | 2. | 2. | |
Final hold (min) | 10. | 28. | 10. | 4. | 5. |
I | 1172. | 1173.7 | 1166. | 1191. | 1160. |
Reference | Jirovetz, Buchbauer, et al., 2005 | Leffingwell and Alford, 2005 | Salehi, Sonboli, et al., 2005 | Singh, Raina, et al., 2005 | N/A |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | HP-5MS | DB-1 | DB-1 |
Column length (m) | 30. | 60. | 30. | 60. | 60. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 90. | 40. | 60. | 35. | 35. |
Tend (C) | 220. | 280. | 280. | 230. | 230. |
Heat rate (K/min) | 7. | 4. | 3. | 2. | 2. |
Initial hold (min) | 2. | 4. | 4. | 4. | |
Final hold (min) | 5. | 25. | 25. | ||
I | 1174. | 1171. | 1172. | 1151. | 1152. |
Reference | Agnihotri, Thappa, et al., 2004 | Kalvandi, Sefidkon, et al., 2004 | Mimica-Dukic, Bozin, et al., 2004 | Park, Lee, et al., 2004 | Park, Lee, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | DB-1 | Methyl Silicone | DB-5 | DB-5 |
Column length (m) | 60. | 60. | 12.5 | 60. | 60. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | |||
Tstart (C) | 35. | 35. | 50. | 50. | 50. |
Tend (C) | 230. | 230. | 270. | 220. | 220. |
Heat rate (K/min) | 2. | 2. | 4. | 3. | 3. |
Initial hold (min) | 4. | 4. | |||
Final hold (min) | 25. | 25. | |||
I | 1153. | 1155. | 1168. | 1186. | 1186. |
Reference | Park, Lee, et al., 2004 | Park, Lee, et al., 2004 | Curini, Bianchi, et al., 2003 | Edris and Farrag, 2003 | Edris, Shalaby, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5MS | HP-5 | DB-5 | OV-101 | BP-1 |
Column length (m) | 30. | 60. | 30. | 25. | 30. |
Carrier gas | He | He | Nitrogen | N2 | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 60. | 40. | 70. | 60. | 60. |
Tend (C) | 280. | 250. | 250. | 240. | 220. |
Heat rate (K/min) | 4. | 5. | 3. | 4. | 5. |
Initial hold (min) | 15. | 3. | 0. | ||
Final hold (min) | 2. | 0. | |||
I | 1173. | 1173. | 1150. | 1165. | 1163. |
Reference | Ghasemi, Asghari, et al., 2003 | Stashenko, Jaramillo, et al., 2003 | Phatak and Heble, 2002 | Zenkevich and Rodin, 2002 | Gupta, Mallavarapu, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | OV-101 | OV-101 | OV-1 | BP-1 |
Column length (m) | 50. | 52. | 50. | 25. | 25. |
Carrier gas | He | Helium | N2 | H2 | N2 |
Substrate | |||||
Column diameter (mm) | 0.2 | 0.26 | 0.2 | 0.25 | 0.5 |
Phase thickness (μm) | 0.13 | 0.25 | |||
Tstart (C) | 50. | 50. | 80. | 40. | 60. |
Tend (C) | 250. | 220. | 200. | 220. | 220. |
Heat rate (K/min) | 2. | 3. | 1. | 3. | 5. |
Initial hold (min) | 0. | 5. | |||
Final hold (min) | 0. | 20. | 5. | 10. | |
I | 1163. | 1156. | 1169. | 1169. | 1171. |
Reference | Orav and Kann, 2001 | Dzumayev, Tkachenko, et al., 1999 | Menon, Chacko, et al., 1999 | Oberhofer, Nikiforov, et al., 1999 | Rao, Bhattacharya, et al., 1999 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary |
---|---|
Active phase | DB-1 |
Column length (m) | 60. |
Carrier gas | He |
Substrate | |
Column diameter (mm) | 0.32 |
Phase thickness (μm) | 1.2 |
Tstart (C) | 30. |
Tend (C) | 240. |
Heat rate (K/min) | 3. |
Initial hold (min) | 10. |
Final hold (min) | |
I | 1175. |
Reference | Ciccioli, Cecinato, et al., 1992 |
Comment | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Boukhris, Bouaziz, et al., 2012
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Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
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