Cyclohexanol, 5-methyl-2-(1-methylethyl)-, (1α,2β,5α)-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5VF-5 MSVF-5 MS
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 100.35.60.30.30.
Tend (C) 260.300.240.260.260.
Heat rate (K/min) 10.3.3.2.2.
Initial hold (min) 1.5.   
Final hold (min) 10.15. 28.28.
I 1186.1170.1172.1180.1182.
ReferenceBoukhris, Bouaziz, et al., 2012Kotowska, Zalikowski, et al., 2012Bertoli, Lepnardi, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1HP-5 MSDB-1DB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.50.50.30.50.
Tend (C) 290.220.280.210.280.
Heat rate (K/min) 5.4.4.5.5.
Initial hold (min)  2.  2.
Final hold (min)  2.  10.
I 1172.1154.1178.1171.1194.
ReferenceLazarevic, Radulovic, et al., 2010Xu, Tang, et al., 2010Zhao, Zeng, et al., 2009Kumazawa, Itobe, et al., 2008Baranauskiene R., Bylaite E., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSSPB-5SPB-5HP-5MSHP-5
Column length (m) 30.60.60.30.30.
Carrier gas Helium  HeHelium
Substrate      
Column diameter (mm) 0.250.320.320.250.32
Phase thickness (μm) 0.251.1.0.250.25
Tstart (C) 60.40.40.60.40.
Tend (C) 280.230.230.280.240.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min)  5.5.  
Final hold (min)  5.5. 5.
I 1172.1185.1185.1172.1175.
ReferenceVagionas, Graikou, et al., 2007Vasta, Ratel, et al., 2007Vasta, Ratel, et al., 2007Bozin, Mimicá-Dukic, et al., 2006Miyazawa and Kawata, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeDB-5SPB-5BPX5HP-5
Column length (m) 25.30.60.25.25.
Carrier gas N2HeHeHeliumHe
Substrate      
Column diameter (mm) 0.30.250.320.220.2
Phase thickness (μm) 0.150.251.0.250.33
Tstart (C) 50.40.40.50.60.
Tend (C) 210.250.230.320.240.
Heat rate (K/min) 2.4.3.5.3.
Initial hold (min) 5. 5.5. 
Final hold (min)     7.
I 1191.1149.1186.1188.1179.
ReferenceTonzibo, Coffy, et al., 2006Yadegarinia, Gachkar, et al., 2006Cornu, Kondjoyan, et al., 2005Dickschat, Bode, et al., 2005Duarte, Figueira, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200HP-5DB-1PE-5HP-5
Column length (m) 30.60.60.30.30.
Carrier gas  HeHeH2Helium
Substrate      
Column diameter (mm) 0.250.320.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.30.60.60.40.
Tend (C) 280.260.250.230.250.
Heat rate (K/min) 6.2.5.5.5.
Initial hold (min) 2.2. 2.2.
Final hold (min) 10.28.10.4.5.
I 1172.1173.71166.1191.1160.
ReferenceJirovetz, Buchbauer, et al., 2005Leffingwell and Alford, 2005Salehi, Sonboli, et al., 2005Singh, Raina, et al., 2005N/A
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSDB-1DB-1
Column length (m) 30.60.30.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 90.40.60.35.35.
Tend (C) 220.280.280.230.230.
Heat rate (K/min) 7.4.3.2.2.
Initial hold (min) 2.4. 4.4.
Final hold (min) 5.  25.25.
I 1174.1171.1172.1151.1152.
ReferenceAgnihotri, Thappa, et al., 2004Kalvandi, Sefidkon, et al., 2004Mimica-Dukic, Bozin, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1Methyl SiliconeDB-5DB-5
Column length (m) 60.60.12.560.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.320.32
Phase thickness (μm) 0.250.25   
Tstart (C) 35.35.50.50.50.
Tend (C) 230.230.270.220.220.
Heat rate (K/min) 2.2.4.3.3.
Initial hold (min) 4.4.   
Final hold (min) 25.25.   
I 1153.1155.1168.1186.1186.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Curini, Bianchi, et al., 2003Edris and Farrag, 2003Edris, Shalaby, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5OV-101BP-1
Column length (m) 30.60.30.25.30.
Carrier gas He HeNitrogenN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.40.70.60.60.
Tend (C) 280.250.250.240.220.
Heat rate (K/min) 4.5.3.4.5.
Initial hold (min)  15.3.0. 
Final hold (min)   2.0. 
I 1173.1173.1150.1165.1163.
ReferenceGhasemi, Asghari, et al., 2003Stashenko, Jaramillo, et al., 2003Phatak and Heble, 2002Zenkevich and Rodin, 2002Gupta, Mallavarapu, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-1BP-1
Column length (m) 50.52.50.25.25.
Carrier gas HeHeliumN2H2N2
Substrate      
Column diameter (mm) 0.20.260.20.250.5
Phase thickness (μm)  0.13 0.25 
Tstart (C) 50.50.80.40.60.
Tend (C) 250.220.200.220.220.
Heat rate (K/min) 2.3.1.3.5.
Initial hold (min)  0. 5. 
Final hold (min)  0.20.5.10.
I 1163.1156.1169.1169.1171.
ReferenceOrav and Kann, 2001Dzumayev, Tkachenko, et al., 1999Menon, Chacko, et al., 1999Oberhofer, Nikiforov, et al., 1999Rao, Bhattacharya, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB-1
Column length (m) 60.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (μm) 1.2
Tstart (C) 30.
Tend (C) 240.
Heat rate (K/min) 3.
Initial hold (min) 10.
Final hold (min)  
I 1175.
ReferenceCiccioli, Cecinato, et al., 1992
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Boukhris, Bouaziz, et al., 2012
Boukhris, M.; Bouaziz, M.; Feki, I.; Jemai, H.; El Feki, A.; Sayadi, S., Hypoglycemic and antioxidant effects of leaf essential oil of Pelargonium graveolens L'Her. in alloxan induced diabetic rats, Lipids in Health and Disease, 2012, 11, 1, 1-10, https://doi.org/10.1186/1476-511X-11-81 . [all data]

Kotowska, Zalikowski, et al., 2012
Kotowska, U.; Zalikowski, M.; Isidorov, V.A., HS-SPME/GC-MS analysis of volatile and semi-volatile organic compounds emitted from municipal sewage sludge, Environ. Monit. Asses., 2012, 184, 5, 2893-2907, https://doi.org/10.1007/s10661-011-2158-8 . [all data]

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Lazarevic, Radulovic, et al., 2010
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Vagionas, Graikou, et al., 2007
Vagionas, K.; Graikou, K.; Ngassapa, O.; Runyoro, D.; Chinou, I., Composition and antimicrobial activity of the essential oils of three Satureja species growing in Tansania, Food Chem., 2007, 103, 2, 319-324, https://doi.org/10.1016/j.foodchem.2006.07.051 . [all data]

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Miyazawa, M.; Kawata, J., Identification of the Key Aroma Compounds in Dried Roots of Rubia cordifolia, L. Oleo Sci., 2006, 55, 1, 37-39, https://doi.org/10.5650/jos.55.37 . [all data]

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Cornu, Kondjoyan, et al., 2005
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Leffingwell and Alford, 2005
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Salehi, Sonboli, et al., 2005
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Singh, Raina, et al., 2005
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Agnihotri, Thappa, et al., 2004
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Gupta, Mallavarapu, et al., 2001
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Orav and Kann, 2001
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Dzumayev, Tkachenko, et al., 1999
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Menon, Chacko, et al., 1999
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Oberhofer, Nikiforov, et al., 1999
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Rao, Bhattacharya, et al., 1999
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Ciccioli, Cecinato, et al., 1992
Ciccioli, P.; Cecinato, A.; Brancaleoni, E.; Frattoni, M.; Liberti, A., Use of carbon adsorption traps combined with high resolution gas chromatography - mass spectrometry for the analysis of polar and non-polar C4-C14 hydrocarbons involved in photochemical smog formation, J. Hi. Res. Chromatogr., 1992, 15, 2, 75-84, https://doi.org/10.1002/jhrc.1240150205 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References