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Cyclohexanol, 5-methyl-2-(1-methylethyl)-, (1«alpha»,2«beta»,5«alpha»)-

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30100.1166.6Tudor, 199740. m/0.35 mm/0.35 «mu»m
CapillaryPB-1130.1174.Engewald, Knobloch, et al., 1991Column length: 42. m; Column diameter: 0.32 mm
PackedSE-30150.1180.Tiess, 1984Ar, Gas Chrom Q (80-100 mesh); Column length: 3. m

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51185.Baranauskiene, Venskutonis, et al., 200350. m/0.32 mm/0.25 «mu»m, He, 50. C @ 2. min, 5. K/min, 280. C @ 10. min
CapillaryBP-11169.Rajeswara Rao, 200225. m/0.5 mm/0.25 «mu»m, N2, 5. K/min, 220. C @ 10. min; Tstart: 60. C
CapillaryBP-11169.Rao B.R.R., 200225. m/0.5 mm/0.25 «mu»m, 5. K/min, 220. C @ 10. min; Tstart: 60. C
CapillaryBP-11173.Jain, Aggarwal, et al., 200125. m/0.55 mm/0.25 «mu»m, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryHP-51173.Kitic, Palic, et al., 200125. m/0.32 mm/0.52 «mu»m, H2, 4. K/min; Tstart: 40. C; Tend: 240. C
CapillaryDB-51141.de Feo, Porta, et al., 199830. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min
CapillaryBPX-51172.Fournier, Hadjiakhoondi, et al., 199750. m/0.22 mm/0.25 «mu»m, N2, 60. C @ 10. min, 2. K/min; Tend: 185. C
CapillaryDB-51174.Loayza, Abujder, et al., 199540. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m
CapillaryOV-11162.Bicchi, Frattini, et al., 198823. m/0.32 mm/0.3 «mu»m, H2, 3. K/min; Tstart: 50. C; Tend: 200. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-11163.Dwivedi, Khan, et al., 200425. m/0.25 mm/0.25 «mu»m, N2; Program: 60C => 5C/min => 220C(5min) => 3C/min => 245C(5min)
CapillaryBP-11161.Rao, Kaul, et al., 200330. m/0.32 mm/0.25 «mu»m, N2; Program: 60C => 5.5C/min => 220C => 3.5C/min => 245C
CapillarySF-961168.Malingré and Maarse, 1974Column length: 150. m; Column diameter: 0.75 mm; Program: not specified

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryCarbowax 20M130.1640.Malingré and Maarse, 1974Column length: 150. m; Column diameter: 0.75 mm

Kovats' RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySupelcowax-101642.Loayza, Abujder, et al., 199540. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m
CapillaryCarbowax 20M1619.Nishimura, Yamaguchi, et al., 19892. K/min; Column length: 50. m; Column diameter: 0.22 mm; Tstart: 80. C; Tend: 200. C
CapillarySupelcowax-20M1632.Bicchi, Frattini, et al., 198823. m/0.32 mm/0.30 «mu»m, H2, 50. C @ 1. min, 3. K/min; Tend: 200. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51173.Benzo, Gilardoni, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 40. C @ 1. min, 5. K/min, 250. C @ 10. min
CapillaryDB-51178.Mahattanatawee K., Perez-Cacho P.R., et al., 200730. m/0.32 mm/0.5 «mu»m, He, 7. K/min, 265. C @ 5. min; Tstart: 40. C
CapillaryDB-51160.Wu, Zorn, et al., 200730. m/0.32 mm/0.25 «mu»m, He, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryDB-51160.Wu, Zorn, et al., 200730. m/0.32 mm/0.25 «mu»m, He, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryDB-11160.Dob, Dahmane, et al., 200530. m/0.32 mm/0.25 «mu»m, 50. C @ 8. min, 2. K/min; Tend: 250. C
CapillaryDB-11141.de Feo, Urrunaga Soria, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min
CapillaryHP-5MS1173.Pino, Mesa, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillarySPB-11165.Antunes, Sevinate-Pinto, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryHP-51170.Flach A., Dondon R.C., et al., 200430. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 50. C; Tend: 290. C
CapillaryDB-11150.2Sun and Stremple, 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 40. C; Tend: 325. C
CapillaryDB-51175.Tampieri, Galuppi, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5MS1173.Demetzos, Angelopoulou, et al., 200230. m/0.25 mm/0.25 «mu»m, 50. C @ 5. min, 3. K/min; Tend: 280. C
CapillarySE-521140.Duru, Cakir, et al., 200225. m/0.32 mm/0.15 «mu»m, N2, 45. C @ 5. min, 3. K/min, 200. C @ 20. min
CapillaryHP-51181.Flamini, Cioni, et al., 200230. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillarySE-541180.78Yin, Xiu, et al., 200135. C @ 3. min, 4. K/min, 230. C @ 10. min; Column length: 25. m; Column diameter: 0.31 mm
CapillarySE-541180.91Yin, Xiu, et al., 200135. C @ 3. min, 4. K/min, 230. C @ 10. min; Column length: 25. m; Column diameter: 0.31 mm
CapillaryBP-11156.Baldovini, Ristorcelli, et al., 200050. m/0.22 mm/0.25 «mu»m, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryMethyl Silicone1167.Píry, Príbela, et al., 199525. m/0.2 mm/0.3 «mu»m, He, 2. K/min; Tstart: 40. C; Tend: 200. C
CapillaryUltra-11153.3Farkas, Le Quere, et al., 199450. m/0.32 mm/0.52 «mu»m, H2, 2. K/min; Tstart: 35. C; Tend: 259. C
CapillaryUltra-11153.3Farkas, Le Quere, et al., 199450. m/0.32 mm/0.52 «mu»m, H2, 2. K/min; Tstart: 35. C; Tend: 259. C
CapillaryUltra-11153.3Farkas, Le Quere, et al., 199450. m/0.32 mm/0.52 «mu»m, H2, 2. K/min; Tstart: 35. C; Tend: 259. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1169.Pérez, Navarro, et al., 200730. m/0.25 mm/0.25 «mu»m, He; Program: 50C(4min) => 10C/min => 200C(0.5min) => 20C/min => 260C(5min)
CapillarySE-521175.Mondello, Dugo, et al., 199560. m/0.32 mm/0.40 «mu»m, He; Program: 45 C (6 min) 3 C/min -> 111 0C 2 C/min -> 160 C 3 C/min -> 300 C (15 min)
PackedSE-301172.Peng, Ding, et al., 1988Supelcoport; Chromosorb; Column length: 3.05 m; Program: 40C(5min) => 10C/min => 200C or 250C (60min)

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryZB-Wax1631.Wu, Zorn, et al., 200730. m/0.32 mm/0.25 «mu»m, He, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryZB-Wax1631.Wu, Zorn, et al., 200730. m/0.32 mm/0.25 «mu»m, He, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryDB-Wax1618.Varming, Andersen, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 40. C @ 10. min, 6. K/min, 240. C @ 25. min
CapillaryDB-Wax1651.Choi, 200560. m/0.25 mm/0.25 «mu»m, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillarySupelcowax-101632.Riu-Aumatell, Lopez-Tamames, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 3. K/min, 240. C @ 10. min
CapillaryOV-3511612.Bonvehi and Coll, 200350. m/0.32 mm/0.2 «mu»m, He, 5. K/min; Tstart: 60. C; Tend: 220. C
CapillarySupelcowax-101630.Moreira, Trugo, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 230. C @ 30. min; Tstart: 50. C
CapillaryBP-201637.Baldovini, Ristorcelli, et al., 200050. m/0.22 mm/0.25 «mu»m, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1636.Kim, Thuy, et al., 200030. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 2. K/min, 200. C @ 20. min
CapillaryDB-FFAP1642.Guillard, le Quere, et al., 1997H2, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 40. C; Tend: 220. C
CapillaryDB-FFAP1646.Guillard, le Quere, et al., 1997H2, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 40. C; Tend: 220. C
CapillaryCarbowax 20M1627.Mondello, Dugo, et al., 199560. m/0.32 mm/0.425 «mu»m, He, 45. C @ 3. min, 3. K/min, 300. C @ 20. min
CapillaryCarbowax 20M1615.Píry, Príbela, et al., 199550. m/0.2 mm/0.2 «mu»m, He, 30. C @ 2. min, 4. K/min, 170. C @ 20. min
CapillarySupelcowax-101644.Chung and Cadwallader, 199360. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 2. K/min, 195. C @ 40. min
CapillaryDB-Wax1637.Umano, Hagi, et al., 1992He, 40. C @ 10. min, 2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 200. C

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedPolydimethyl siloxane150.1178.Maume, 1968 

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51186.Boukhris, Bouaziz, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium, 100. C @ 1. min, 10. K/min, 260. C @ 10. min
CapillaryHP-5 MS1170.Kotowska, Zalikowski, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium, 35. C @ 5. min, 3. K/min, 300. C @ 15. min
CapillaryHP-51172.Bertoli, Lepnardi, et al., 201130. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryVF-5 MS1180.Leffingwell and Alford, 201160. m/0.32 mm/0.25 «mu»m, Helium, 2. K/min, 260. C @ 28. min; Tstart: 30. C
CapillaryVF-5 MS1182.Leffingwell and Alford, 201160. m/0.32 mm/0.25 «mu»m, Helium, 2. K/min, 260. C @ 28. min; Tstart: 30. C
CapillaryHP-5 MS1172.Lazarevic, Radulovic, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium, 5. K/min; Tstart: 70. C; Tend: 290. C
CapillaryDB-11154.Xu, Tang, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 2. min, 4. K/min, 220. C @ 2. min
CapillaryHP-5 MS1178.Zhao, Zeng, et al., 200930. m/0.25 mm/0.25 «mu»m, Helium, 4. K/min; Tstart: 50. C; Tend: 280. C
CapillaryDB-11171.Kumazawa, Itobe, et al., 200830. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 30. C; Tend: 210. C
CapillaryDB-51194.Baranauskiene R., Bylaite E., et al., 200750. m/0.32 mm/0.25 «mu»m, He, 50. C @ 2. min, 5. K/min, 280. C @ 10. min
CapillaryHP-5 MS1172.Vagionas, Graikou, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillarySPB-51185.Vasta, Ratel, et al., 200760. m/0.32 mm/1. «mu»m, 40. C @ 5. min, 3. K/min, 230. C @ 5. min
CapillarySPB-51185.Vasta, Ratel, et al., 200760. m/0.32 mm/1. «mu»m, 40. C @ 5. min, 3. K/min, 230. C @ 5. min
CapillaryHP-5MS1172.Bozin, Mimicá-Dukic, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51175.Miyazawa and Kawata, 200630. m/0.32 mm/0.25 «mu»m, Helium, 4. K/min, 240. C @ 5. min; Tstart: 40. C
CapillaryMethyl Silicone1191.Tonzibo, Coffy, et al., 200625. m/0.3 mm/0.15 «mu»m, N2, 50. C @ 5. min, 2. K/min; Tend: 210. C
CapillaryDB-51149.Yadegarinia, Gachkar, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 40. C; Tend: 250. C
CapillarySPB-51186.Cornu, Kondjoyan, et al., 200560. m/0.32 mm/1. «mu»m, He, 40. C @ 5. min, 3. K/min; Tend: 230. C
CapillaryBPX51188.Dickschat, Bode, et al., 200525. m/0.22 mm/0.25 «mu»m, Helium, 50. C @ 5. min, 5. K/min; Tend: 320. C
CapillaryHP-51179.Duarte, Figueira, et al., 200525. m/0.2 mm/0.33 «mu»m, He, 3. K/min, 240. C @ 7. min; Tstart: 60. C
CapillaryRSL-2001172.Jirovetz, Buchbauer, et al., 200530. m/0.25 mm/0.25 «mu»m, 40. C @ 2. min, 6. K/min, 280. C @ 10. min
CapillaryHP-51173.7Leffingwell and Alford, 200560. m/0.32 mm/0.25 «mu»m, He, 30. C @ 2. min, 2. K/min, 260. C @ 28. min
CapillaryDB-11166.Salehi, Sonboli, et al., 200560. m/0.25 mm/0.25 «mu»m, He, 5. K/min, 250. C @ 10. min; Tstart: 60. C
CapillaryPE-51191.Singh, Raina, et al., 200530. m/0.32 mm/0.25 «mu»m, H2, 60. C @ 2. min, 5. K/min, 230. C @ 4. min
CapillaryHP-51160.N/A30. m/0.32 mm/0.25 «mu»m, Helium, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryDB-51174.Agnihotri, Thappa, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 90. C @ 2. min, 7. K/min, 220. C @ 5. min
CapillaryDB-51171.Kalvandi, Sefidkon, et al., 200460. m/0.25 mm/0.25 «mu»m, He, 40. C @ 4. min, 4. K/min; Tend: 280. C
CapillaryHP-5MS1172.Mimica-Dukic, Bozin, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-11151.Park, Lee, et al., 200460. m/0.32 mm/0.25 «mu»m, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min
CapillaryDB-11152.Park, Lee, et al., 200460. m/0.32 mm/0.25 «mu»m, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min
CapillaryDB-11153.Park, Lee, et al., 200460. m/0.32 mm/0.25 «mu»m, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min
CapillaryDB-11155.Park, Lee, et al., 200460. m/0.32 mm/0.25 «mu»m, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min
CapillaryMethyl Silicone1168.Curini, Bianchi, et al., 2003He, 4. K/min; Column length: 12.5 m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 270. C
CapillaryDB-51186.Edris and Farrag, 2003He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 220. C
CapillaryDB-51186.Edris, Shalaby, et al., 2003He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 220. C
CapillaryHP-5MS1173.Ghasemi, Asghari, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51173.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 «mu»m, 40. C @ 15. min, 5. K/min; Tend: 250. C
CapillaryDB-51150.Phatak and Heble, 200230. m/0.25 mm/0.25 «mu»m, He, 70. C @ 3. min, 3. K/min, 250. C @ 2. min
CapillaryOV-1011165.Zenkevich and Rodin, 2002Nitrogen, 60. C @ 0. min, 4. K/min, 240. C @ 0. min; Column length: 25. m; Column diameter: 0.25 mm
CapillaryBP-11163.Gupta, Mallavarapu, et al., 200130. m/0.25 mm/0.25 «mu»m, N2, 5. K/min; Tstart: 60. C; Tend: 220. C
CapillaryOV-1011163.Orav and Kann, 2001He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 50. C; Tend: 250. C
CapillaryOV-1011156.Dzumayev, Tkachenko, et al., 199952. m/0.26 mm/0.13 «mu»m, Helium, 50. C @ 0. min, 3. K/min, 220. C @ 0. min
CapillaryOV-1011169.Menon, Chacko, et al., 1999N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C
CapillaryOV-11169.Oberhofer, Nikiforov, et al., 199925. m/0.25 mm/0.25 «mu»m, H2, 40. C @ 5. min, 3. K/min, 220. C @ 5. min
CapillaryBP-11171.Rao, Bhattacharya, et al., 1999N2, 5. K/min, 220. C @ 10. min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 60. C
CapillaryDB-11175.Ciccioli, Cecinato, et al., 199260. m/0.32 mm/1.2 «mu»m, He, 30. C @ 10. min, 3. K/min; Tend: 240. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5 MS1173.Kotowska, Zalikowski, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillarySLB-5 MS1184.Mondello, 201230. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillarySLB-5 MS1184.Mondello, 201230. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryDB-11150.Xu, Tang, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryHP-5 MS1178.Fan, Lu, et al., 200930. m/0.25 mm/0.25 «mu»m, Helium; Program: 40 0C (3 min) 3 0C/min -> 160 0C (2 min) 8 0C/min -> 220 0C (3 min)
CapillaryHP-51175.Zhao, Li, et al., 200830. m/0.25 mm/0.25 «mu»m; Program: 40 0C (2 min) 5 0C/min -> 80 0C 7 oC/min -> 160 0C 9 0C/min -> 200 0C 20 0C/min -> 280 0C (10 min)
CapillaryHP-51172.Zhao, Li, et al., 200830. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryHP-11151.Barra, Baldovini, et al., 200750. m/0.2 mm/0.33 «mu»m, He; Program: 40C(2min) => 2C/min => 200C => 15C/min => 250C (30min)
CapillarySPB-11160.Díaz-Maroto, Castillo, et al., 200750. m/0.25 mm/0.25 «mu»m; Program: 70C(3min) => 4C/min => 120C => 8C/min => 250C(5min)
CapillaryHP-5 MS1182.Formisano, Rigano, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium; Program: 40 0C (5 min) 2 0C/min -> 250 0C (15 min) 10 0C/min -> 270 0C
CapillaryHP-5MS1182.Senatore, Apostolides Arnold, et al., 200630. m/0.25 mm/0.25 «mu»m, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillarySE-521172.Tognolini, Barocelli, et al., 200630. m/0.32 mm/0.15 «mu»m, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min)
CapillaryCP Sil 8 CB1173.Nivinskienë, Butkienë, et al., 200550. m/0.32 mm/0.25 «mu»m, He; Program: 60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)
CapillaryCP Sil 8 CB1172.Radudienë, Judpintienë, et al., 200550. m/0.32 mm/0.25 «mu»m, He; Program: 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min)
CapillaryHP-51171.Riu-Aumatell, Lopez-Tamames, et al., 2005Program: not specified
CapillarySE-301171.Vinogradov, 2004Program: not specified
CapillaryDB-5 MS1182.Luo and Agnew, 200130. m/0.25 mm/1.0 «mu»m, Helium; Program: not specified
CapillaryDB-11148.Baratta, Dorman, et al., 199830. m/0.25 mm/0.25 «mu»m, He; Program: 45C => 3C/min => 175C => 15C/min => 240C (10min)
CapillaryCP Sil 5 CB1166.Guyot, Bouseta, et al., 199850. m/0.32 mm/1.2 «mu»m, He; Program: 30C => 55C/min => 85C => 1C/min => 145C => 3C/min => 250C
CapillaryDB-51174.Anitescu, Doneanu, et al., 199715. m/0.25 mm/0.25 «mu»m, He; Program: 40C(5min) => 5C/min => 120C(10min) => 4C/min => 250C(4min) => 5C/min => 280C
CapillaryPolydimethyl siloxanes1165.Zenkevich, 1997Program: not specified
Capillary5 % Phenyl methyl siloxane1173.Sagrero-Nieves and Bartley, 1995Program: not specified
CapillaryMethyl Silicone1160.Grundschober, 1991Program: not specified
CapillaryOV-1011171.Shibamoto, 1987Column length: 60. m; Column diameter: 0.25 mm; Program: not specified
CapillaryOV-1011171.Shibamoto, 1987Program: not specified
CapillaryOV-1011171.Zenkevich and Malamakhov, 1987He; Column length: 50. m; Column diameter: 0.24 mm; Program: not specified
PackedOV-1011158.Swigar and Silverstein, 1981N2, Chromosorb G 60-80mesh DMCS; Column length: 2.5 m; Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryVF-Wax MS1641.Duarte, Dias, et al., 201060. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 5. min, 3. K/min, 220. C @ 25. min
CapillaryCP-Wax1639.Mo, Fan, et al., 200960. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 2. min, 6. K/min, 230. C @ 15. min
CapillaryDB-Wax1645.Kumazawa, Itobe, et al., 200830. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 30. C; Tend: 210. C
CapillaryHP-Innowax1652.Formisano, Rigano, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium, 40. C @ 5. min, 2. K/min; Tend: 250. C
CapillaryDB-Wax1636.Cai, Lin, et al., 200660. m/0.25 mm/0.5 «mu»m, He, 50. C @ 2. min, 3. K/min, 230. C @ 20. min
CapillaryCP-Wax1636.Ka, Choi, et al., 200530. m/0.32 mm/0.25 «mu»m, He, 40. C @ 2. min, 5. K/min; Tend: 180. C
CapillaryDB-Wax1589.Salehi, Sonboli, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 4. K/min, 250. C @ 10. min; Tstart: 40. C
CapillaryZB-Wax1631.N/A30. m/0.32 mm/0.25 «mu»m, Helium, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryDB-Wax1628.Agnihotri, Thappa, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 90. C @ 2. min, 7. K/min, 220. C @ 5. min
CapillaryDB-Wax1641.Lin, Cai, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 50. C @ 2. min, 3. K/min, 230. C @ 20. min
CapillaryTC-Wax1637.Miyazawa, Yamafuji, et al., 20033. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 240. C
CapillaryHP-Innowax1614.Stashenko, Jaramillo, et al., 200350. m/0.2 mm/0.2 «mu»m, 50. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryPEG-20M1637.Orav and Kann, 2001He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 70. C; Tend: 220. C
CapillaryDB-Wax1651.Tamura, Boonbumrung, et al., 2000Nitrogen, 40. C @ 10. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 200. C
CapillaryHP Innowax FSP1651.Kaya, Baser, et al., 199960. m/0.25 mm/0.25 «mu»m, He, 60. C @ 10. min, 220. C @ 10. min
CapillaryHP-Innowax1651.Kaya, Baser, et al., 1999, 260. m/0.25 mm/0.25 «mu»m, He, 60. C @ 10. min; Tend: 220. C
CapillaryCarbowax1612.Menon, Chacko, et al., 1999N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C
CapillaryBP-201640.Rao, Bhattacharya, et al., 1999N2, 5. K/min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 60. C; Tend: 200. C
CapillaryTC-Wax1642.Shuichi, Masazumi, et al., 199680. C @ 5. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 240. C
CapillaryCarbowax 20M1600.Shibamoto, 19872. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
PackedCarbowax 20M1631.Stancher and Pertoldi, 1967Hydrogen, Gas-Chrom Z (80-100 mesh), 4. K/min; Column length: 2. m; Tstart: 65. C; Tend: 220. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-FFAP1649.Toontom, Meenune, et al., 201225. m/0.32 mm/0.50 «mu»m, Helium; Program: 45 0C (2 min) 3 0C/min -> 130 0C (1 min) 20 0C/min -> 220 0C (3 min) 20 0C/min -> 230 0C (3 min)
CapillaryDB-Wax1635.Welke, Manfroi, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryDB-Wax1637.Welke, Manfroi, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryInnowax FSC1638.Demirci, Temel, et al., 201160. m/0.25 mm/0.25 «mu»m, Helium; Program: 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C
CapillaryDB-Wax1608.Krings, Zelena, et al., 200630. m/0.32 mm/0.25 «mu»m, He; Program: 45C(5min) => 5C/min => 150C => 10C/min => 240C (10min)
CapillaryHP-Innowax1652.Senatore, Apostolides Arnold, et al., 200650. m/0.2 mm/0.2 «mu»m, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillaryCarbowax 20M1612.Vinogradov, 2004Program: not specified
CapillaryInnowax FSC1638.Tabanca N., Demirci F., et al., 200160. m/0.25 mm/0.25 «mu»m, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryPolyethylene Glycol1636.Grundschober, 1991Program: not specified
CapillaryCarbowax 20M1612.Shibamoto, 1987Program: not specified

Lee's RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryMethyl Silicone198.32Eckel, Ross, et al., 1993Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Leffingwell and Alford, 2011
Leffingwell, J.; Alford, E.D., Volatile constituents of the giant pufball mushroom (Calvatia gigantea), Leffingwell Rep., 2011, 4, 1-17. [all data]

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Lazarevic, J.; Radulovic, N.; Palic, R.; Zlatkovic, B., Chemical Analusis of volatile constituents of Berula erecta (Hudson) Coville subsp. erecta (Apiaceae) from Serbia, J. Essential Oil. Res., 2010, 22, 3, 153-156, https://doi.org/10.1080/10412905.2010.9700290 . [all data]

Xu, Tang, et al., 2010
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Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Kumazawa, Itobe, et al., 2008
Kumazawa, K.; Itobe, T.; Nishimura, O.; Hamaguchi, T., A new approach to estimate the in-mouth release characteristics of odorants in chewing gum, Food Science and Technology Research, 2008, 14, 3, 269-276, https://doi.org/10.3136/fstr.14.269 . [all data]

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Baranauskiene R.; Bylaite E.; Venskutonis R.P., Flavor retention of peppermint (Mentha piperita L.) essential oil spray-dried in modified starches during encapsulation and storage, J. Agric. Food Chem., 2007, 55, 8, 3027-3036, https://doi.org/10.1021/jf062508c . [all data]

Vagionas, Graikou, et al., 2007
Vagionas, K.; Graikou, K.; Ngassapa, O.; Runyoro, D.; Chinou, I., Composition and antimicrobial activity of the essential oils of three Satureja species growing in Tansania, Food Chem., 2007, 103, 2, 319-324, https://doi.org/10.1016/j.foodchem.2006.07.051 . [all data]

Vasta, Ratel, et al., 2007
Vasta, V.; Ratel, J.; Engel, E., Mass Spectrometry Analysis of Volatile Compounds in Raw Meat for the Authentication of the Feeding Background of Farm Animals, J. Agric. Food Chem., 2007, 55, 12, 4630-4639, https://doi.org/10.1021/jf063432n . [all data]

Bozin, Mimicá-Dukic, et al., 2006
Bozin, B.; Mimicá-Dukic, N.; Simin, N.; Anackov, G., Characterization of the volatile composition of essential oils of some lamiaceae spices and the antimicrobial and antioxidant activities of the entire oils, J. Agric. Food Chem., 2006, 54, 5, 1822-1828, https://doi.org/10.1021/jf051922u . [all data]

Miyazawa and Kawata, 2006
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Notes

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