Diisopropyl methanephosphonate

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-541073.Kostiainen, 200025. m/0.32 mm/0.25 μm, He, 40. C @ 1. min, 10. K/min, 280. C @ 10. min

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-541066.Budiman, 200730. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 10. K/min, 280. C @ 5. min
CapillarySE-541075.Budiman, 200730. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 10. K/min, 280. C @ 5. min
CapillarySE-541085.Budiman, 200730. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 10. K/min, 280. C @ 5. min
CapillaryDB-51067.Savel'eva, Zenkevich, et al., 200225. m/0.20 mm/0.33 μm, Helium, 40. C @ 1. min, 5. K/min, 270. C @ 15. min
CapillarySE-541072.7Söderström, Ketola, et al., 199525. m/0.32 mm/0.25 μm, He, 40. C @ 2. min, 10. K/min, 250. C @ 10. min

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySE-541073.Budiman, 200730. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryDB-5 MS1059.Tsunoda, 200530. m/0.25 mm/0.25 μm, Helium; Program: 45 0C (2 min) 8 0C/min -> 125 0C 15 0C/min -> 280 0C
CapillaryDB-5 MS1058.Tsunoda, 200530. m/0.25 mm/0.25 μm, Helium; Program: 45 0C (2 min) 8 0C/min -> 125 0C 15 0C/min -> 280 0C
CapillaryDB-51067.Saveljeva, Zenkevich, et al., 2003He; Program: not specified
Capillary5 % Phenyl methyl siloxane1073.OPCW, 1997Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kostiainen, 2000
Kostiainen, O., Gas Chromatography in Screening of Chemicals Related to the Chemical Weapons Convention in Encyclopedia of Analytical Chemistry, Meyers, R.A., ed(s)., John Wiley Sons Ltd, Chichester, 2000, 963-979. [all data]

Budiman, 2007
Budiman, H., Analysis and identification spiking chemical compounds related to chemical weapon convention in unknown water samples using gas chromatography and gas chromatography electron ionization mass spectrometry, Indo. J. Chem., 2007, 7, 3, 297-302. [all data]

Savel'eva, Zenkevich, et al., 2002
Savel'eva, E.I.; Zenkevich, I.G.; Kuznetsova, T.A.; Radilov, A.S.; Pshenichnaya, G.V., Investigation of Products of Transformation of Phosphororganic Toxic Substances with Gas Chromatography - Mass Spectrometry, Rus. Khim. Zh. (Rus.), 2002, 56, 6, 82-91. [all data]

Söderström, Ketola, et al., 1995
Söderström, M.T.; Ketola, R.A.; Kostiainen, O., Identification of some nerve agent homologues and dialkyl methylphosphonates by gas chromatography/Fourier transform infrared spectrometry. Part II. Spectral search with the help of retention indices, Fresenius J. Anal. Chem., 1995, 352, 6, 550-556, https://doi.org/10.1007/BF00323072 . [all data]

Tsunoda, 2005
Tsunoda, N., The sarin incidents in Japan and mass spectrometry, J. MAss Spectrom. Soc. Japan, 2005, 53, 3, 157-163, https://doi.org/10.5702/massspec.53.157 . [all data]

Saveljeva, Zenkevich, et al., 2003
Saveljeva, E.; Zenkevich, I.; Radilov, A., Identification of chemical neutralization and products of organophosphorus chemical warfare agents, 2003, retrieved from http://www.shimadzu.com/apps/form.cfm. [all data]

OPCW, 1997
OPCW, Conference of the States Parties C-I/DEC.64 (22 May 1997), 1997, retrieved from http://www.opcw.org/html/global/cseries/csp1/CIDEC64.html. [all data]


Notes

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