Octanal
- Formula: C8H16O
- Molecular weight: 128.2120
- IUPAC Standard InChIKey: NUJGJRNETVAIRJ-UHFFFAOYSA-N
- CAS Registry Number: 124-13-0
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: n-Caprylaldehyde; n-Octaldehyde; n-Octanal; n-Octylal; Antifoam-LF; Caprylaldehyde; Caprylic aldehyde; Octaldehyde; Octanaldehyde; Octanoic aldehyde; Octylaldehyde; 1-Octanal; n-Octyl aldehyde; Aldehyde C-8; C-8 Aldehyde; NSC 1508
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Equity-5MS | Equity-5MS | HP-5 | SPB-5 | HP-5 |
Column length (m) | 30. | 30. | 25. | 60. | 30. |
Carrier gas | He | He | He | N2 | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 1. | 0.25 |
Tstart (C) | 50. | 50. | 60. | 40. | 50. |
Tend (C) | 250. | 250. | 240. | 230. | 220. |
Heat rate (K/min) | 3. | 3. | 4. | 3. | 5. |
Initial hold (min) | 2. | 2. | 10. | ||
Final hold (min) | 10. | 10. | 10. | ||
I | 1007. | 1007. | 1007. | 1003. | 1002. |
Reference | Belsito E.L., Carbone C., et al., 2007 | Belsito E.L., Carbone C., et al., 2007 | Dehghan, Solaimanian, et al., 2007 | Engel and Ratel, 2007 | Flamini, Tebano, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | DB-5 | ZB-5 | DB-1 |
Column length (m) | 30. | 30. | 60. | 30. | 60. |
Carrier gas | He | He | He | N2 | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 0.5 | 1. | 0.5 | 0.25 |
Tstart (C) | 60. | 40. | 40. | 40. | 60. |
Tend (C) | 240. | 265. | 260. | 265. | 250. |
Heat rate (K/min) | 3. | 7. | 4. | 7. | 5. |
Initial hold (min) | 2. | ||||
Final hold (min) | 5. | 10. | 5. | 10. | |
I | 1003. | 1002. | 1005. | 1003. | 982. |
Reference | Maccioni, Baldini, et al., 2007 | Mahattanatawee K., Perez-Cacho P.R., et al., 2007 | Methven L., Tsoukka M., et al., 2007 | Ruiz Perez-Cacho, Mahattanatawee, et al., 2007 | Sonboli, Azizian, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | DB-5 | HP-5 | HP-5 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | N2 | He | ||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 1. | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 50. | 60. | 60. |
Tend (C) | 250. | 220. | 290. | 220. | 260. |
Heat rate (K/min) | 5. | 3. | 10. | 5. | 3. |
Initial hold (min) | 2. | 1. | 10. | ||
Final hold (min) | 5. | 10. | |||
I | 1004. | 1001. | 1003. | 1003. | 1002. |
Reference | Wu, Zorn, et al., 2007 | Bastos, Ishimoto, et al., 2006 | Bylaite and Meyer, 2006 | Flamini, Tebano, et al., 2006 | Javidnia K., Miri R., et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5MS | HP-5MS | HP-5MS | HP-5MS | HP-5MS |
Column length (m) | 20. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | He | H2 | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 60. | 60. | 60. | 50. |
Tend (C) | 240. | 280. | 280. | 280. | 285. |
Heat rate (K/min) | 5. | 3. | 3. | 4. | 4.3 |
Initial hold (min) | 4. | 5. | |||
Final hold (min) | 15. | ||||
I | 1005. | 996. | 981. | 1002. | 993. |
Reference | Kallio, Jussila, et al., 2006 | Kukic J., Petrovic S., et al., 2006 | Pavlovic, Kovacevic, et al., 2006 | Saroglou, Dorizas, et al., 2006 | Vujisic L., Vuckovic I., et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | DB-5MS | HP-5 | HP-5MS | CP Sil 5 CB |
Column length (m) | 30. | 30. | 30. | 30. | 25. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.4 |
Tstart (C) | 40. | 40. | 50. | 80. | 80. |
Tend (C) | 300. | 200. | 220. | 300. | 270. |
Heat rate (K/min) | 4. | 5. | 3. | 4. | 10. |
Initial hold (min) | 5. | 5. | |||
Final hold (min) | 45. | 20. | |||
I | 1000. | 1005. | 991. | 1002.5 | 981. |
Reference | Vundac, Pfeifhofer, et al., 2006 | Whetstine M.E.C., Drake M.A., et al., 2006 | Xian Q., Chen H., et al., 2006 | Zhao C.X., Li, et al., 2006 | Ziegenbein, Hanssen, et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5MS | DB-5MS | MDN-5 | CP-Sil 8CB-MS |
Column length (m) | 30. | 30. | 30. | 30. | 0. |
Carrier gas | H2 | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 35. | 40. | 40. | 50. | 40. |
Tend (C) | 270. | 200. | 200. | 250. | 280. |
Heat rate (K/min) | 5. | 5. | 10. | 3. | 4. |
Initial hold (min) | 5. | 3. | 2. | ||
Final hold (min) | 20. | 45. | 20. | 5. | |
I | 1001. | 1005. | 1005. | 1002. | 1007. |
Reference | Alves, Pinto, et al., 2005 | Carunchia Whetstine, Croissant, et al., 2005 | Carunchia Whetstine, Croissant, et al., 2005 | Dugo, Mondello, et al., 2005 | Elmore, Cooper, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | 5 % Phenyl methyl siloxane | BP-1 | HP-5 | HP-5 | DB-1 |
Column length (m) | 30. | 50. | 30. | 30. | 30. |
Carrier gas | He | He | N2 | N2 | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.22 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 1. | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 60. | 60. | 40. |
Tend (C) | 250. | 220. | 220. | 220. | 250. |
Heat rate (K/min) | 7. | 2. | 5. | 5. | 3. |
Initial hold (min) | 10. | 10. | 10. | ||
Final hold (min) | 5. | 20. | 20. | ||
I | 1018. | 980. | 1003. | 1002. | 984. |
Reference | Estevez, Ventanas, et al., 2005 | Ferrari, Tomi, et al., 2005 | Flamini, Luigi Cioni, et al., 2005 | Flamini, Luigi Cioni, et al., 2005, 2 | Gancel, Ollitrault, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | HP-5 | HP-5 | HP-5MS | HP-5MS |
Column length (m) | 50. | 30. | 30. | 30. | 60. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.2 |
Phase thickness (μm) | 1.05 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 35. | 60. | 50. | 60. | 60. |
Tend (C) | 220. | 260. | 250. | 250. | 200. |
Heat rate (K/min) | 8. | 3. | 4. | 4. | 2. |
Initial hold (min) | 15. | 5. | 2. | ||
Final hold (min) | 5. | 15. | 20. | 10. | |
I | 1002. | 1001. | 1007. | 1001. | 1004. |
Reference | Insausti, Goñi, et al., 2005 | Javidnia, Miri, et al., 2005 | Mahattanatawee, Goodner, et al., 2005 | Pino, Mesa, et al., 2005 | Smadja, Rondeau, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | HP-5 | HP-5 | Mega 5MS | DB-5MS |
Column length (m) | 25. | 25. | 25. | 30. | 30. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.2 | 0.2 | 0.2 | 0.25 | 0.25 |
Phase thickness (μm) | 1. | 1. | 1. | 0.25 | 0.25 |
Tstart (C) | 40. | 40. | 40. | 40. | 40. |
Tend (C) | 280. | 280. | 280. | 240. | 200. |
Heat rate (K/min) | 5. | 5. | 5. | 3. | 10. |
Initial hold (min) | 2. | 3. | |||
Final hold (min) | 5. | 5. | 5. | 20. | |
I | 1008. | 1008. | 1008. | 997. | 1008. |
Reference | Solina, Baumgartner, et al., 2005 | Solina, Baumgartner, et al., 2005 | Solina, Baumgartner, et al., 2005 | Verzera, Trozzi, et al., 2005 | Whetstine, Cadwallader, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-5MS | ZB-5 | HP-5 | HP-5 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | Helium | N2 | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.50 | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 40. | 60. | 50. |
Tend (C) | 250. | 280. | 265. | 220. | 290. |
Heat rate (K/min) | 5. | 3. | 7. | 5. | 4. |
Initial hold (min) | 2. | 10. | |||
Final hold (min) | 5. | 5. | |||
I | 986. | 1002. | 1003. | 1005. | 1005. |
Reference | Wu, Zorn, et al., 2005 | Aligiannis, Kalpoutzakis, et al., 2004 | Bell, 2004 | Bertoli, Pistelli, et al., 2004 | Flach A., Dondon R.C., et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | ZB-5 | CP-Sil 8CB-MS | HP-5 | SPB-5 |
Column length (m) | 30. | 0. | 60. | 30. | 30. |
Carrier gas | N2 | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.5 | 0.25 | 0.25 | |
Tstart (C) | 60. | 40. | 40. | 60. | 60. |
Tend (C) | 220. | 265. | 280. | 260. | 250. |
Heat rate (K/min) | 5. | 7. | 4. | 3. | 4. |
Initial hold (min) | 10. | 2. | 2. | ||
Final hold (min) | 5. | 5. | 20. | ||
I | 1003. | 1003. | 1005. | 1002. | 1000. |
Reference | Flamini, Luigi Cioni, et al., 2004 | Gocmen, Gurbuz, et al., 2004 | Hierro, de la Hoz, et al., 2004 | Javidnia, Miri, et al., 2004 | Pino, Marbot, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SPB-5 | HP-5 | HP-5 | HP-5MS | DB-1 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 1. | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | -30. | 50. | 50. | 40. |
Tend (C) | 250. | 250. | 310. | 200. | 250. |
Heat rate (K/min) | 4. | 10. | 4. | 6. | 3. |
Initial hold (min) | 2. | 1. | 1.5 | ||
Final hold (min) | 20. | 5. | 20. | ||
I | 1000. | 1003. | 999. | 1006. | 980. |
Reference | Pino, Marbot, et al., 2004, 2 | Siegmund, Derler, et al., 2004 | Singer, Flach, et al., 2004 | Weissbecker, Holighaus, et al., 2004 | Brat, Rega, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP-Sil 8CB-MS | HP-5 | HP-5 | SPB-1 | SPB-1 |
Column length (m) | 60. | 30. | 30. | 30. | 30. |
Carrier gas | N2 | N2 | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 60. | 35. | 35. |
Tend (C) | 280. | 220. | 220. | 225. | 225. |
Heat rate (K/min) | 4. | 5. | 5. | 4. | 4. |
Initial hold (min) | 2. | 10. | 10. | 5. | 5. |
Final hold (min) | 5. | 20. | 20. | ||
I | 1006. | 1002. | 1002. | 982. | 982. |
Reference | Bruna, Hierro, et al., 2003 | Campeol, Flamini, et al., 2003 | Campeol, Flamini, et al., 2003 | Chisholm, Jell, et al., 2003 | Chisholm, Jell, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SPB-1 | SPB-1 | HP-5 | HP-5 | DB-5 |
Column length (m) | 25. | 25. | 30. | 30. | 30. |
Carrier gas | N2 | N2 | He | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 35. | 35. | 60. | 60. | 60. |
Tend (C) | 225. | 225. | 220. | 220. | 240. |
Heat rate (K/min) | 4. | 4. | 5. | 5. | 3. |
Initial hold (min) | 10. | 10. | 10. | 10. | |
Final hold (min) | |||||
I | 988. | 988. | 1002. | 1002. | 1003. |
Reference | Chisholm, Wilson, et al., 2003 | Chisholm, Wilson, et al., 2003 | Dural, Bagci, et al., 2003 | Ertugrul, Dural, et al., 2003 | Flamini, Cioni, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-5 | HP-5 | DB-1 | DB-5 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | N2 | N2 | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.5 |
Tstart (C) | 60. | 60. | 60. | 40. | 40. |
Tend (C) | 240. | 220. | 220. | 250. | 265. |
Heat rate (K/min) | 3. | 5. | 5. | 3. | 7. |
Initial hold (min) | 10. | 10. | |||
Final hold (min) | 20. | 5. | |||
I | 1003. | 1004. | 1003. | 984. | 1004. |
Reference | Flamini, Luigi Cioni, et al., 2003 | Flamini, Luigi Cioni, et al., 2003, 2 | Flamini, Luigi Cioni, et al., 2003, 3 | Gancel, Ollitrault, et al., 2003 | Högnadóttir and Rouseff, 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | Mega 5MS | DB-5 | BPX-5 | DB-5 |
Column length (m) | 30. | 30. | 30. | 50. | 30. |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.32 | 0.25 |
Phase thickness (μm) | 0.5 | 0.25 | 1. | 0.5 | 0.25 |
Tstart (C) | 40. | 40. | 50. | 60. | 60. |
Tend (C) | 265. | 240. | 200. | 250. | 240. |
Heat rate (K/min) | 7. | 3. | 2.5 | 4. | 3. |
Initial hold (min) | 2. | 5. | |||
Final hold (min) | 5. | 20. | |||
I | 1006. | 997. | 1003.0 | 1016. | 1004. |
Reference | Högnadóttir and Rouseff, 2003 | Verzera, Trozzi, et al., 2003 | Xu, van Stee, et al., 2003 | Bredie, Mottram, et al., 2002 | Flamini, Cioni, et al., 2002 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | CP Sil 5 CB | BP-1 | RTX-5 | HP-1 |
Column length (m) | 30. | 50. | 50. | 30. | 24. |
Carrier gas | N2 | H2 | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.22 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 0.15 | 0.25 | 0.25 | 0.17 |
Tstart (C) | 60. | 40. | 60. | 45. | 60. |
Tend (C) | 220. | 300. | 220. | 300. | 250. |
Heat rate (K/min) | 5. | 4. | 2. | 3. | 4. |
Initial hold (min) | 10. | 3. | 6. | 2. | |
Final hold (min) | 20. | 10. | 20. | ||
I | 1003. | 1003. | 978. | 1004. | 980. |
Reference | Flamini, Cioni, et al., 2002, 2 | Heinrich, Pfeifhofer, et al., 2002 | Lota, de Rocca Serra, et al., 2002 | Mondello, Zappia, et al., 2002 | Nath, Sarma, et al., 2002 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 8 CB | CP Sil 5 CB | DB-5 | CP-Sil 8CB-MS | SPB-1 |
Column length (m) | 60. | 50. | 30. | 60. | 15. |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.4 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 40. | 40. | 35. |
Tend (C) | 250. | 280. | 220. | 280. | 225. |
Heat rate (K/min) | 4. | 3. | 10. | 4. | 6. |
Initial hold (min) | 8. | 10. | 5. | 2. | 3. |
Final hold (min) | 10. | 60. | 30. | 10. | |
I | 1003. | 985. | 1007. | 1006. | 988. |
Reference | Oruna-Concha, Ames, et al., 2002 | Pino, Marbot, et al., 2002 | Wu and Cadwallader, 2002 | Bruna, Hierro, et al., 2001 | Chisholm, Wilson, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | DB-1 | DB-5MS | DB-1 | BP-1 |
Column length (m) | 30. | 60. | 60. | 30. | 50. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.32 | 0.22 |
Phase thickness (μm) | 0.25 | 1. | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 40. | 40. | 40. | 60. |
Tend (C) | 380. | 220. | 200. | 240. | 220. |
Heat rate (K/min) | 3. | 2. | 2. | 7. | 2. |
Initial hold (min) | 5. | 5. | |||
Final hold (min) | 30. | 5. | |||
I | 1002. | 981. | 1005. | 977. | 978. |
Reference | Couladis, Tsortanidou, et al., 2001 | Kim, 2001 | Lee, Suriyaphan, et al., 2001 | Lin and Rouseff, 2001 | Lota, Serra, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | BP-1 | DB-5 | CP Sil 5 CB | CP Sil 5 CB | HP-5MS |
Column length (m) | 50. | 30. | 50. | 50. | 30. |
Carrier gas | He | H2 | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.22 | 0.25 | 0.32 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.4 | 0.4 | 0.25 |
Tstart (C) | 60. | 60. | 60. | 60. | 60. |
Tend (C) | 220. | 240. | 280. | 280. | 280. |
Heat rate (K/min) | 2. | 3. | 3. | 3. | 4. |
Initial hold (min) | 10. | 10. | 5. | ||
Final hold (min) | 60. | 60. | |||
I | 978. | 968. | 981. | 981. | 1001. |
Reference | Lota, Serra, et al., 2001 | Nogueira, Bittrich, et al., 2001 | Pino and Marbot, 2001 | Pino, Marbot, et al., 2001 | Skaltsa, Mavrommati, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-5 | CP Sil 8 CB | HP-5 | HP-5 |
Column length (m) | 60. | 50. | 60. | 30. | 30. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 1.05 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 50. | 40. | 50. | 50. |
Tend (C) | 290. | 290. | 280. | 280. | 280. |
Heat rate (K/min) | 4. | 2. | 4. | 4. | 4. |
Initial hold (min) | 2. | 2. | 5. | 5. | |
Final hold (min) | 5. | ||||
I | 997. | 1004. | 1006. | 1001. | 1002. |
Reference | Bartley and Jacobs, 2000 | David, Scanlan, et al., 2000 | Elmore, Mottram, et al., 2000 | Lazari, Skaltsa, et al., 2000 | Lazari, Skaltsa, et al., 2000, 2 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | BP-1 | HP-5 | DB-5 | Mega 5MS | Mega 5MS |
Column length (m) | 50. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | N2 | He | He |
Substrate | |||||
Column diameter (mm) | 0.22 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 70. | 70. | 40. | 40. |
Tend (C) | 230. | 230. | 230. | 240. | 240. |
Heat rate (K/min) | 2. | 2. | 2. | 3. | 3. |
Initial hold (min) | 2. | 2. | |||
Final hold (min) | 35. | ||||
I | 978. | 1002. | 1002. | 997. | 997. |
Reference | Lota, de Rocca Serra, et al., 2000 | Song, Sawamura, et al., 2000 | Song, Sawamura, et al., 2000, 2 | Verzera, la Rosa, et al., 2000 | Verzera, Trozzi, et al., 2000 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | BP-1 | OV-1 | OV-1 | BPX-5 |
Column length (m) | 60. | 50. | 20. | 20. | 50. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.22 | 0.32 | 0.32 | 0.32 |
Phase thickness (μm) | 1. | 0.25 | 0.3 | 0.3 | 0.50 |
Tstart (C) | -50. | 60. | 45. | 45. | 40. |
Tend (C) | 175. | 230. | 220. | 220. | 280. |
Heat rate (K/min) | 6. | 2. | 10. | 10. | 4. |
Initial hold (min) | 2. | 5. | 5. | ||
Final hold (min) | 35. | 10. | 10. | ||
I | 988.1 | 978. | 987. | 990. | 1016. |
Reference | Helmig, Klinger, et al., 1999 | Lota, Serra, et al., 1999 | Valero, Sanz, et al., 1999 | Valero, Sanz, et al., 1999 | Aaslyng, Elmore, et al., 1998 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SPB-1 | SPB-5 | BP-1 | DB-1 | DB-1 |
Column length (m) | 60. | 60. | 25. | 30. | 30. |
Carrier gas | N2 | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 1. | 5. | 1. | |
Tstart (C) | 40. | 40. | 5. | 35. | -50. |
Tend (C) | 200. | 200. | 250. | 270. | 180. |
Heat rate (K/min) | 4. | 3. | 5. | 10. | 6. |
Initial hold (min) | 5. | 5. | 1. | ||
Final hold (min) | 20. | 2. | 30. | ||
I | 976. | 1002. | 979. | 987. | 979.9 |
Reference | Chen, Huang, et al., 1998 | Verdier-Metz., Coulon, et al., 1998 | Sinyinda and Gramshaw, 1998 | Bartelt, 1997 | Helmig, Pollock, et al., 1996 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | SE-30 | DB-5 | DB-5 | DB-5 |
Column length (m) | 60. | 50. | 30. | 30. | 30. |
Carrier gas | H2 | H2 | H2 | ||
Substrate | |||||
Column diameter (mm) | 0.33 | 0.32 | 0.32 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 1. | 1. | 1. |
Tstart (C) | -50. | 50. | 40. | 40. | 40. |
Tend (C) | 180. | 250. | 220. | 220. | 220. |
Heat rate (K/min) | 6. | 4. | 3. | 3. | 3. |
Initial hold (min) | |||||
Final hold (min) | |||||
I | 1000.7 | 980. | 1004. | 1004. | 1004. |
Reference | Helmig, Pollock, et al., 1996 | Misharina and Golovnya, 1996 | Moio L., Rillo L., et al., 1996 | Moio L., Rillo L., et al., 1996 | Moio L., Rillo L., et al., 1996 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | OV-101 | OV-101 | OV-101 | OV-101 |
Column length (m) | 25. | 25. | 25. | 25. | 25. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.20 | 0.20 | 0.20 | 0.20 | 0.20 |
Phase thickness (μm) | |||||
Tstart (C) | 60. | 60. | 60. | 60. | 60. |
Tend (C) | 260. | 260. | 260. | 260. | 260. |
Heat rate (K/min) | 1. | 1. | 2. | 2. | 2. |
Initial hold (min) | 8. | 8. | 0. | 0. | 8. |
Final hold (min) | 30. | 30. | 30. | 30. | 30. |
I | 980. | 984. | 981. | 985. | 981. |
Reference | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | OV-101 | OV-101 | OV-101 | OV-101 |
Column length (m) | 25. | 25. | 25. | 25. | 25. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.20 | 0.20 | 0.20 | 0.20 | 0.20 |
Phase thickness (μm) | |||||
Tstart (C) | 60. | 60. | 60. | 60. | 60. |
Tend (C) | 260. | 260. | 260. | 260. | 260. |
Heat rate (K/min) | 2. | 2. | 2. | 4. | 4. |
Initial hold (min) | 8. | 8. | 8. | 8. | 8. |
Final hold (min) | 30. | 30. | 30. | 30. | 30. |
I | 983. | 985. | 987. | 983. | 986. |
Reference | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | OV-101 | OV-101 | OV-101 | CP Sil 5 CB |
Column length (m) | 25. | 25. | 25. | 25. | 25. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.20 | 0.20 | 0.20 | 0.20 | 0.22 |
Phase thickness (μm) | 0.11 | ||||
Tstart (C) | 70. | 70. | 80. | 80. | 80. |
Tend (C) | 260. | 260. | 260. | 260. | 230. |
Heat rate (K/min) | 2. | 2. | 2. | 2. | 1. |
Initial hold (min) | 8. | 8. | 8. | 8. | 8. |
Final hold (min) | 30. | 30. | 30. | 30. | 16. |
I | 981. | 985. | 980. | 985. | 991. |
Reference | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Baaliouamer, Boudarene, et al., 1993 | Chanegriha and Baaliouamer, 1993 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | OV-101 | OV-101 | OV-101 | DB-5 |
Column length (m) | 50. | 50. | 50. | 50. | 0.32 |
Carrier gas | He | N2 | N2 | He | H2 |
Substrate | |||||
Column diameter (mm) | 0.31 | 0.25 | 0.25 | 0.32 | 1. |
Phase thickness (μm) | 0.5 | 0.50 | |||
Tstart (C) | 50. | 80. | 80. | 50. | 30. |
Tend (C) | 250. | 200. | 200. | 250. | 180. |
Heat rate (K/min) | 4. | 2. | 2. | 2. | 1.5 |
Initial hold (min) | 5. | ||||
Final hold (min) | |||||
I | 980. | 980. | 981. | 989. | 1005. |
Reference | Misharina, Golovnya, et al., 1992 | Yang, Sugisawa, et al., 1992 | Yang, Sugisawa, et al., 1992 | Misharina, Aerove, et al., 1991 | Guichard and Souty, 1988 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Packed |
---|---|---|---|---|---|
Active phase | OV-1 | SPB-1 | SPB-1 | CP Sil 5 CB | Apiezon M |
Column length (m) | 60. | 60. | 60. | 25. | 1.5 |
Carrier gas | He | He | He | N2 | |
Substrate | Celite 545 | ||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.22 | |
Phase thickness (μm) | 0.25 | 0.25 | |||
Tstart (C) | 50. | 35. | 35. | 70. | 75. |
Tend (C) | 225. | 235. | 235. | 205. | 200. |
Heat rate (K/min) | 1.5 | 2. | 2. | 4. | 6. |
Initial hold (min) | 10. | 10. | |||
Final hold (min) | 50. | 40. | 40. | ||
I | 979. | 973. | 973. | 993. | 971. |
Reference | Chen and Ho, 1987 | Huang, Bruechert, et al., 1987 | Huang, Bruechert, et al., 1987 | Hendriks and Bruins, 1983 | Golovnya and Uraletz, 1971 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Packed | Packed |
---|---|---|
Active phase | Apiezon M | Apiezon M |
Column length (m) | 1.5 | 1.5 |
Carrier gas | N2 | N2 |
Substrate | Celite 545 | Celite 545 |
Column diameter (mm) | ||
Phase thickness (μm) | ||
Tstart (C) | 75. | 75. |
Tend (C) | 200. | 200. |
Heat rate (K/min) | 6. | 6. |
Initial hold (min) | ||
Final hold (min) | ||
I | 972. | 976. |
Reference | Golovnya and Uraletz, 1971 | Golovnya and Uraletz, 1971 |
Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
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