1,3-Dimethyldibenzothiophene
- Formula: C14H12S
- Molecular weight: 212.310
- IUPAC Standard InChI: InChI=1S/C14H12S/c1-9-7-10(2)14-11-5-3-4-6-12(11)15-13(14)8-9/h3-8H,1-2H3
- IUPAC Standard InChIKey: IPMMDFNYBNKMQS-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Dibenzothiophene, 1,3-dimethyl
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | PONA | 2079. | Xiaolan, Jun, et al., 2006 | 50. m/0.20 mm/0.50 μm, Helium, 1.5 K/min, 300. C @ 20. min; Tstart: 120. C |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | PONA | 2079. | Xiaolan, Jun, et al., 2006, 2 | 50. m/0.20 mm/0.50 μm, 1.5 K/min; Tstart: 120. C; Tend: 300. C |
| Capillary | DB-Petro | 2081. | Lu, Wu, et al., 2004 | 50. m/0.20 mm/0.50 μm, He, 35. C @ 5. min, 2. K/min, 300. C @ 5. min |
| Capillary | PONA | 2079. | Yang, Wang, et al., 2002 | 50. m/0.20 mm/0.50 μm, 1.5 K/min, 270. C @ 10. min; Tstart: 120. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-Petro | 2079. | Lu, Wu, et al., 2004 | 50. m/0.20 mm/0.50 μm, He; Program: not specified |
Lee's RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5MS | 336.65 | Schade and Andersson, 2006 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 1. min, 10. K/min; Tend: 300. C |
Lee's RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 334.73 | Mössner, de Alda, et al., 1999 | 60. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 45 C/min => 150C (2 min) => 2 C/min => 300 C (25 min) |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Xiaolan, Jun, et al., 2006
Xiaolan, Z.; Jun, L.; Jianhua, L.; Yongtan, Y.,
Speciation distribution of polycyclic aromatic sulfur heterocycles in crude oil,
Chinese J. Anal. Chem., 2006, 34, 11, 1546-1550, https://doi.org/10.1016/S1872-2040(07)60014-0
. [all data]
Xiaolan, Jun, et al., 2006, 2
Xiaolan, Z.; Jun, L.; Jianhua, L.; Yongtan, Y.,
Speciation distribution of polycyclic aromatic sulfur heterocycles in crude oil,
Fenxi Huaxue, 2006, 34, 11, 1546-1551. [all data]
Lu, Wu, et al., 2004
Lu, X.; Wu, J.; Wu, J.; Kong, H.; Hua, R.; Tao, W.; Gu, J.; Xu, G.,
Characterization and quantitative determination of diesel fractions by comprehensive two-dimensional gas chromatography/time of flight mass spectrometry,
Chin. J. Chromatogr., 2004, 22, 1, 5-11. [all data]
Yang, Wang, et al., 2002
Yang, Y.-T.; Wang, H.-Y.; Lu, W.-Z.,
Determination od sulfur compounds in catalytic diesel oil by gas chromatography with atomic emission detector and its application,
Chin. J. Chromatogr., 2002, 20, 6, 493-497. [all data]
Schade and Andersson, 2006
Schade, T.; Andersson, J.T.,
Speciation of alkylated dibenzothiophenes through correlation of structure and gas chromatographic retention indexes,
J. Chromatogr. A, 2006, 1117, 2, 206-213, https://doi.org/10.1016/j.chroma.2006.03.079
. [all data]
Mössner, de Alda, et al., 1999
Mössner, S.G.; de Alda, M.J.L.; Sander, L.C.; Lee, M.L.; Wise, S.A.,
Gas chromatographic retention behavior of polycyclic aromatic sulfur heterocyclic compounds, (dibenzothiophene, naphtho[b]thiophenes, benzo[b]naphthothiophenes and alkyl-substituted derivatives) on stationary phases of different selectivity,
J. Chromatogr. A, 1999, 841, 2, 207-228, https://doi.org/10.1016/S0021-9673(99)00363-5
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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