Histamine, 3TMS derivative
- Formula: C14H33N3Si3
- Molecular weight: 327.6884
- IUPAC Standard InChI: InChI=1S/C14H33N3Si3/c1-18(2,3)16-12-14(15-13-16)10-11-17(19(4,5)6)20(7,8)9/h12-13H,10-11H2,1-9H3
- IUPAC Standard InChIKey: JHBJMCFUYLNCSZ-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Histamine, N,N,N'-tris(trimethylsilyl)-; Bis(trimethylsilyl)pyrrol2-[1-(trimethylsilyl)-1H-imidazol-4-yl]ethylmorphoamine; Histamine, tris-TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-1 | 190. | 1870. | Cashaw, Walsh, et al., 1971 | N2, GasChrom Q; Column length: 2. m |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 1873. | Butts, 1972 | He, Chromosorb W HP (80-100 mesh), 10. K/min; Column length: 2. m; Tstart: 100. C; Tend: 325. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 1880.3 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Cashaw, Walsh, et al., 1971
Cashaw, J.L.; Walsh, M.J.; Yamanaka, Y.; Davis, V.E.,
Simultaneous determination of biogenic amines and narcotic alkaloids by gas-liquid chromatography,
J. Chromatogr. Sci., 1971, 9, 2, 98-104, https://doi.org/10.1093/chromsci/9.2.98
. [all data]
Butts, 1972
Butts, W.C.,
Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds,
Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Notes
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