Naringenin, 3TMS derivative
- Formula: C24H36O5Si3
- Molecular weight: 488.7961
- IUPAC Standard InChI: InChI=1S/C24H36O5Si3/c1-30(2,3)27-18-12-10-17(11-13-18)21-16-20(25)24-22(26-21)14-19(28-31(4,5)6)15-23(24)29-32(7,8)9/h10-15,21H,16H2,1-9H3
- IUPAC Standard InChIKey: ZMEWYEXWOABPGS-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 4',5,7-Trihydroxyflavanone, tris(trimethylsilyl) ether; Naringenin, TMS; Flavanone, 5,7,4'-trihydroxy, tris-TMS; NARINGENIN 3TMS-1
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | DB-1 | 280. | 2861.8 | Stremple, 1996 | 30. m/0.25 mm/0.25 μm, H2 |
| Capillary | DB-5 | 280. | 2907.9 | Stremple, 1996 | 30. m/0.25 mm/0.25 μm, H2 |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Methyl Silicone | 2851. | Greenaway and Whatley, 1990 | 25. m/0.32 mm/0.5 μm, He, 3. K/min; Tstart: 75. C; Tend: 300. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 2872.2 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
Normal alkane RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-1 | 210. | 2843. | Katagi, Horii, et al., 1973 | Nitrogen; Column length: 2. m |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Stremple, 1996
Stremple, P.,
Improved separation and identification of aglycon flavonoids by gas chromatography on phenylmethylsilicone copolymers,
J. Hi. Res. Chromatogr., 1996, 19, 10, 581-584, https://doi.org/10.1002/jhrc.1240191010
. [all data]
Greenaway and Whatley, 1990
Greenaway, W.; Whatley, F.R.,
Resolution of complex mixtures of phenolics in poplar bud exudate by analysis of gas chromatography-mass spectrometry data,
J. Chromatogr., 1990, 519, 1, 145-158, https://doi.org/10.1016/0021-9673(90)85143-J
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Katagi, Horii, et al., 1973
Katagi, T.; Horii, A.; Oomura, Y.; Miyakawa, H.; Kyu, T.; Ikeda, Y.; Isoi, K.,
Gas chromatography of flavonoids,
J. Chromatogr., 1973, 79, 45-56, https://doi.org/10.1016/S0021-9673(01)85272-9
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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