3-Aminopropanol, 2TBDMS derivative
- Formula: C15H37NOSi2
- Molecular weight: 303.6314
- IUPAC Standard InChI: InChI=1S/C15H37NOSi2/c1-14(2,3)18(7,8)16-12-11-13-17-19(9,10)15(4,5)6/h16H,11-13H2,1-10H3
- IUPAC Standard InChIKey: DMESNZCHXSSLJJ-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 3-Amino-1-propanol, N-(tert-butyldimethylsilyl)-, tert-butyldimethylsilyl ether; 1-tert-Butyl-N-(3-pyrrol[tert-butyl(dimethyl)silyl]oxymorphopropyl)-1,1-dimethylsilanamine; 1-Propanol, 3-amino, TBDMS; 1-Propanol, 3-amino, O,N-bis-DMTBS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 1551.1 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
| Capillary | Methyl Silicone | 1560. | Peng, Yang, et al., 1991 | Program: not specified |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Peng, Yang, et al., 1991
Peng, C.T.; Yang, Z.C.; Maltby, D.,
Prediction of retention indexes. III. Silylated derivatives of polar compounds,
J. Chromatogr., 1991, 586, 1, 113-129, https://doi.org/10.1016/0021-9673(91)80029-G
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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