Pentanoic acid, 2-[(tert-butyldimethylsilyl)oxy]-, tert-butyldimethylsilyl ester, (DL)-
- Formula: C17H38O3Si2
- Molecular weight: 346.6528
- IUPAC Standard InChI: InChI=1S/C17H38O3Si2/c1-12-13-14(19-21(8,9)16(2,3)4)15(18)20-22(10,11)17(5,6)7/h14H,12-13H2,1-11H3
- IUPAC Standard InChIKey: MGAXIOLXSPMIGG-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Pentanoic acid, 2-hydroxy, TBDMS; 2-Hydroxyvaleric acid, TBDMS; 2-Hydroxyvaleric acid, DMTBS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1621. | Paik, Lee, et al., 2005 | 30. m/0.25 mm/0.25 μm, Helium, 60. C @ 2. min, 4. K/min; Tend: 290. C |
| Capillary | DB-5 | 1619.23 | Kim, Kim, et al., 1993 | 30. m/0.25 mm/0.241 μm, 4. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | DB-5 | 1621. | Kim, Kim, et al., 1990 | 30. m/0.25 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 280. C |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Paik, Lee, et al., 2005
Paik, M.-J.; Lee, H.-J.; Kim, K.-R.,
Simultaneous retention index analysis of urinary amino acids and carboxylic acids for graphic recognition of abnormal state,
J. Chromatogr. B, 2005, 821, 1, 94-104, https://doi.org/10.1016/j.jchromb.2005.04.011
. [all data]
Kim, Kim, et al., 1993
Kim, K.-R.; Kim, J.-H.; Park, H.-K.; Oh, C.-H.,
Dual capillary column system for the qualitative gas chromatography: 2. Comparison between splitless and on-column injection modes,
Bull. Korean Chem. Soc., 1993, 14, 2, 250-255. [all data]
Kim, Kim, et al., 1990
Kim, K.-R.; Kim, J.-H.; Park, H.-K.,
Trace analysis as TBDMS derivatives of organic acids in aqueous samples,
J. Korean Chem. Soc., 1990, 34, 4, 352-359. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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