3-Quinuclidinol, trimethylsilyl ether
- Formula: C10H21NOSi
- Molecular weight: 199.3653
- IUPAC Standard InChI: InChI=1S/C10H21NOSi/c1-13(2,3)12-10-8-11-6-4-9(10)5-7-11/h9-10H,4-8H2,1-3H3
- IUPAC Standard InChIKey: QYBKWHMRDRKMQN-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 3-Quinuclidinol, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-54 | 1268. | Kostiainen, 2000 | 25. m/0.32 mm/0.25 μm, He, 40. C @ 1. min, 10. K/min, 280. C @ 10. min |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-54 | 1265. | Budiman, 2007 | 30. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 10. K/min, 280. C @ 5. min |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-54 | 1268. | Budiman, 2007 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
| Capillary | 5 % Phenyl methyl siloxane | 1268. | OPCW, 1997 | Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Kostiainen, 2000
Kostiainen, O.,
Gas Chromatography in Screening of Chemicals Related to the Chemical Weapons Convention
in Encyclopedia of Analytical Chemistry, Meyers, R.A., ed(s)., John Wiley Sons Ltd, Chichester, 2000, 963-979. [all data]
Budiman, 2007
Budiman, H.,
Analysis and identification spiking chemical compounds related to chemical weapon convention in unknown water samples using gas chromatography and gas chromatography electron ionization mass spectrometry,
Indo. J. Chem., 2007, 7, 3, 297-302. [all data]
OPCW, 1997
OPCW,
Conference of the States Parties C-I/DEC.64 (22 May 1997), 1997, retrieved from http://www.opcw.org/html/global/cseries/csp1/CIDEC64.html. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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