11-Ketoandrosterone MO TMS
- Formula: C24H42N2O3Si
- Molecular weight: 434.6874
- IUPAC Standard InChI: InChI=1S/C24H42N2O3Si/c1-23-13-12-17(29-30(5,6)7)14-16(23)8-9-18-19-10-11-21(26-28-4)24(19,2)15-20(22(18)23)25-27-3/h16-19,22H,8-15H2,1-7H3/t16-,17+,18?,19?,22?,23-,24-/m1/s1
- IUPAC Standard InChIKey: CZAVIQKBQLKTIH-FRBBNXGPSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-101 | 2627. | Hurter and van Ree, 1979 | Gas-Chrom P (80-100 mesh), 1. K/min; Column length: 3.6 m; Tstart: 180. C |
| Packed | SE-30 | 2630. | Hurter and van Ree, 1979 | Gas-Chrom P (80-100 mesh), 1. K/min; Column length: 3.6 m; Tstart: 180. C |
| Packed | OV-1 | 2600. | Luyten and Rutten, 1974 | He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C |
| Capillary | SE-30 | 2633. | Luyten and Rutten, 1974 | He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 200. C |
| Packed | SE-30 | 2600. | Luyten and Rutten, 1974 | He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Hurter and van Ree, 1979
Hurter, P.; van Ree, T.,
Programmed-Temperature Gas Chromatography on Mixed Phases. Separation of Steroid Derivatives on Binary Mixtures,
J. Chromatogr., 1979, 169, 93-100, https://doi.org/10.1016/0021-9673(75)85034-5
. [all data]
Luyten and Rutten, 1974
Luyten, J.A.; Rutten, G.A.F.M.,
Analysis of Steroids by High-Resolution Gas-Liquid Chromatography. II. Application to Urinary Samples,
J. Chromatogr., 1974, 91, 393-406, https://doi.org/10.1016/S0021-9673(01)97918-X
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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