2,4-Dimethyl-1,3-dithiolane
- Formula: C5H10S2
- Molecular weight: 134.263
- IUPAC Standard InChI: InChI=1S/C5H10S2/c1-4-3-6-5(2)7-4/h4-5H,3H2,1-2H3
- IUPAC Standard InChIKey: FSCICYWMDXUMTJ-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 2,4-Dimethyl-1,3-dithiolan
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | OV-101 | 130. | 1032. | Misharina and Golovnya, 1994 | He; Column length: 50. m; Column diameter: 0.32 mm |
| Capillary | OV-101 | 150. | 1044. | Misharina and Golovnya, 1994 | He; Column length: 50. m; Column diameter: 0.32 mm |
| Capillary | SE-52 | 130. | 1060. | Misharina and Golovnya, 1994 | 60. m/0.32 mm/2. μm, He |
| Capillary | SE-52 | 150. | 1078. | Misharina and Golovnya, 1994 | 60. m/0.32 mm/2. μm, He |
| Capillary | OV-101 | 130. | 1032. | Misharina, Golovnya, et al., 1993 | 50. m/0.32 mm/0.5 μm, He |
| Packed | Apiezon M | 130. | 1060. | Garbuzov, Misharina, et al., 1985 | He or N2, Chromosorb W, AW-DMCS; Column length: 2.1 m |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | OV-101 | 1012. | Misharina and Golovnya, 1994 | He, 50. C @ 0. min, 4. K/min; Column length: 50. m; Column diameter: 0.32 mm; Tend: 200. C |
| Capillary | SE-52 | 1050. | Misharina and Golovnya, 1994 | 60. m/0.32 mm/2. μm, He, 50. C @ 0. min, 4. K/min; Tend: 200. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Methyl Silicone | 1032. | Misharina, 1995 | Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Misharina and Golovnya, 1994
Misharina, T.A.; Golovnya, R.V.,
Spectral and gas-chromatographic characterization of 4-methyl-2-alkyl substituted 1,3-oxothiolanes and 1,3-dithiolanes,
Zh. Anal. Khim., 1994, 49, 4, 395-401. [all data]
Misharina, Golovnya, et al., 1993
Misharina, T.A.; Golovnya, R.V.; Beletsky, I.V.,
Sorption properties of heterocyclic compounds differing by heteroatom in capillary gas chromatography,
Russ. Chem. Bull. (Engl. Transl.), 1993, 42, 7, 1167-1170, https://doi.org/10.1007/BF00701998
. [all data]
Garbuzov, Misharina, et al., 1985
Garbuzov, V.G.; Misharina, T.A.; Aerov, A.F.; Golovnya, R.V.,
Gas chromatographic retention indices for sulphur(II)-containing organic substances,
J. Anal. Chem. USSR (Engl. Transl.), 1985, 40, 4, 576-586. [all data]
Misharina, 1995
Misharina, T.A.,
Sorption regularities of sulfur- and oxygen-containing compounds in chromatography and their application in identification of volatile organic compounds, Diss. degree of Dr. Sci. (Chemistry), 1995, 52. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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