alanine, N(O,S)-isoBOC TBDMS
- Formula: C14H29NO4Si
- Molecular weight: 303.4699
- IUPAC Standard InChI: InChI=1S/C14H29NO4Si/c1-10(2)9-18-13(17)15-11(3)12(16)19-20(7,8)14(4,5)6/h10-11H,9H2,1-8H3,(H,15,17)
- IUPAC Standard InChIKey: XFEYVCZFKABRCV-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Ala, N-isoBOC TBDMS; Ala isoBOC TBDMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1702.7 | Oh, Mabry, et al., 1995 | 30. m/0.25 mm/0.25 μm, N2, 150. C @ 2. min, 3. K/min; Tend: 280. C |
| Capillary | DB-5 | 1703. | Oh, Kim, et al., 1994 | 30. m/0.25 mm/0.25 μm, 150. C @ 2. min, 3. K/min; Tend: 280. C |
| Capillary | DB-5 | 1702. | Kim, Kim, et al., 1992 | 30. m/0.25 mm/0.24 μm, 150. C @ 2. min, 3. K/min; Tend: 280. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Oh, Mabry, et al., 1995
Oh, C.-H.; Mabry, T.J.; Kim, K.-R.; Kim, J.-H.,
GC-MS Analysis of nonprotein amino acids in Gymnocladus dioicus as N(O,S)-Isobutyloxycarbonyl silyl derivatives,
J. Chromatogr. Sci., 1995, 33, 7, 399-404, https://doi.org/10.1093/chromsci/33.7.399
. [all data]
Oh, Kim, et al., 1994
Oh, C.-H.; Kim, J.-H.; Kim, K.-R.; Brownson, D.M.; Mabry, T.J.,
Simultaneous gas chromatographic analysis of non-protein and protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives,
J. Chromatogr. A, 1994, 669, 1-2, 125-137, https://doi.org/10.1016/0021-9673(94)80344-7
. [all data]
Kim, Kim, et al., 1992
Kim, K.-R.; Kim, J.-H.; Oh, C.-H.; Mabry, T.J.,
Capillary gas chromatography of protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives in aqueous samples,
J. Chromatogr., 1992, 605, 2, 241-249, https://doi.org/10.1016/0021-9673(92)85242-L
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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