m-Synephrine, N-DTFMB-TMS
- Formula: C24H31F6NO3Si2
- Molecular weight: 551.6693
- IUPAC Standard InChI: InChI=1S/C24H31F6NO3Si2/c1-31(22(32)17-11-18(23(25,26)27)14-19(12-17)24(28,29)30)15-21(34-36(5,6)7)16-9-8-10-20(13-16)33-35(2,3)4/h8-14,21H,15H2,1-7H3
- IUPAC Standard InChIKey: YNNAAKHUVJFAQK-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: m-Synephrine, DTFMB-TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-1 | 2220. | Shafi, Midgley, et al., 1989 | He, 100. C @ 1. min, 10. K/min; Column length: 12.5 m; Column diameter: 0.20 mm; Tend: 300. C |
| Capillary | Methyl Silicone | 2220. | Midgley, MacLachlan, et al., 1988 | He, 100. C @ 1. min, 20. K/min; Column length: 12.5 m; Column diameter: 0.20 mm; Tend: 280. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Shafi, Midgley, et al., 1989
Shafi, N.; Midgley, J.M.; Watson, D.G.; Smail, G.A.; Strang, R.; MacFarlane, R.G.,
Analysis of biogenic amines in the brain of the American Cockroach (Periplaneta Americana) by gas chromatography-negative ion chemical ionisation mass spectrometry,
J. Chromatogr., 1989, 490, 9-19, https://doi.org/10.1016/S0378-4347(00)82756-5
. [all data]
Midgley, MacLachlan, et al., 1988
Midgley, J.M.; MacLachlan, J.; Watson, D.G.,
An extraction-derivatization method suitable for the analysis of biogenic amines by gas chromatography negative ion mass spectrometry,
Biomed. Environ. Mass Spectrom., 1988, 15, 10, 535-539, https://doi.org/10.1002/bms.1200151005
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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