D-Isoleucine, N(O,S)-ethoxycarbonyl, (S)-(+)-3-methyl-2-butyl ester


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51647.4Lee, Kim, et al., 200130. m/0.25 mm/0.25 μm, He; Program: 60C(1min) => 30C/min => 120C(2min) => 3C/min => 280C
CapillaryDB-51671.1Lee, Kim, et al., 200130. m/0.25 mm/0.25 μm, He; Program: 60C(1min) => 30C/min => 120C(2min) => 3C/min => 280C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lee, Kim, et al., 2001
Lee, J.; Kim, K.-R.; Won, S.; Kim, J.H.; Goto, J., Enantioseparation of chiral amino acids as the N(O,S)-ethoxycarbonylated diastereomeric esters by achiral dual-capillary column gas chromatography, Analyst, 2001, 126, 12, 2128-2133, https://doi.org/10.1039/b106610m . [all data]


Notes

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