3B,16A-Dihydroxy-5-androsten-17-one, MO TMS
- Formula: C26H49NO3Si2
- Molecular weight: 479.8432
- IUPAC Standard InChI: InChI=1S/C26H49NO3Si2/c1-25-14-12-19(29-31(4,5)6)16-18(25)10-11-20-21(25)13-15-26(2)22(20)17-23(24(26)27-28-3)30-32(7,8)9/h18-23H,10-17H2,1-9H3/t18-,19+,20?,21?,22?,23-,25+,26+/m0/s1
- IUPAC Standard InChIKey: TVJNIUFLVUUMNG-YYXCNFCFSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 2732. | Luyten and Rutten, 1974 | He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C |
| Capillary | OV-1 | 2768. | Luyten and Rutten, 1974 | He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 220. C |
| Capillary | SE-30 | 2774. | Luyten and Rutten, 1974 | He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 200. C |
| Packed | SE-30 | 2743. | Luyten and Rutten, 1974 | He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Luyten and Rutten, 1974
Luyten, J.A.; Rutten, G.A.F.M.,
Analysis of Steroids by High-Resolution Gas-Liquid Chromatography. II. Application to Urinary Samples,
J. Chromatogr., 1974, 91, 393-406, https://doi.org/10.1016/S0021-9673(01)97918-X
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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