Oxo-β-cyclocitral


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillary
Active phase DB-5 MSDB-5 MSHP-5MS
Column length (m) 30.30.30.
Carrier gas HeliumHeliumHe
Substrate    
Column diameter (mm) 0.250.250.25
Phase thickness (μm) 0.250.250.25
Program 50 0C (2.8 min) 5.5 0C/min -> 140 0C (1 min) 4.5 oC/min -> 220 0C -> 225 0C (2 min) 3.4 0C/min -> 265 0C (5 min)50 0C (2.8 min) 5.5 0C/min -> 140 0C (1 min) 4.5 oC/min -> 220 0C -> 225 0C (2 min) 3.4 0C/min -> 265 0C (5 min)50C(3min) => 3C/min) => 180C => 15C/min => 250C(5min)
I 1299.1304.1226.
ReferenceZhu, Li, et al., 2008Zhu, Li, et al., 2008Kanakis, Daferera, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zhu, Li, et al., 2008
Zhu, M.; Li, E.; He, H., Determination of volatile chemical constitutes in tea by simultaneous distillation extraction, vacuum hydrodistillation and thermal desrption, Chromatographia, 2008, 68, 7/8, 603-610, https://doi.org/10.1365/s10337-008-0732-1 . [all data]

Kanakis, Daferera, et al., 2004
Kanakis, C.D.; Daferera, D.J.; Tarantilis, P.A.; Polissiou, M.G., Qualitative determination of volatile compounds and quantitative evaluation of safranal and 4-hydroxy-2,6,6-trimethyl-1-cyclohexene-1-carboxaldehyde (HTCC) in Greek saffron, J. Agric. Food Chem., 2004, 52, 14, 4515-4521, https://doi.org/10.1021/jf049808j . [all data]


Notes

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