trans-Muurola-4(14),5-diene

Formula: C₁₅H₂₄
Molecular weight: 204.3511
IUPAC Standard InChI: InChI=1S/C15H24/c1-10(2)13-8-6-12(4)14-7-5-11(3)9-15(13)14/h9-10,12-14H,3,5-8H2,1-2,4H3/t12-,13+,14?/m0/s1
IUPAC Standard InChIKey: RNDFUOKDULDZPR-WLDKUNSKSA-N
Chemical structure:
This structure is also available as a 2d Mol file
Stereoisomers:
Other names: trans-Murrola-4(14),5-diene; (E)-Muurola-4(14),5-diene
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Other data available:
- Gas Chromatography
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Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5 MS	HP-5 MS	DB-5	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	60.	60.	60.
T_end (C)	250.	230.	220.	220.	220.
Heat rate (K/min)	3.	3.	4.	4.	5.
Initial hold (min)	2.	10.		5.	10.
Final hold (min)	10.	10.
I	1495.	1491.	1497.	1497.	1499.
Reference	Lo Presti, Sciarrone, et al., 2008	Adams, Beauchamp, et al., 2007	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Pintore G., Chessa M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	DB-5	SPB-5	5 % Phenyl methyl siloxane
Column length (m)	60.	30.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.32	0.25
Phase thickness (μm)	1.	0.25	0.25	1.	0.25
T_start (C)	40.	60.	60.	40.	75.
T_end (C)	230.	240.	240.	230.	200.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)	5.			5.	4.
Final hold (min)	2.				8.
I	1519.	1490.	1489.	1508.	1494.
Reference	Tornambe, Cornu, et al., 2006	Chaverri and Cicció, 2005	Chaverri and Cicció, 2005	Cornu, Kondjoyan, et al., 2005	Cicció and Gómez-Laurito, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary
Active phase	DB-1
Column length (m)	30.
Carrier gas	He
Substrate
Column diameter (mm)	0.2
Phase thickness (μm)
T_start (C)	60.
T_end (C)	240.
Heat rate (K/min)	3.
Initial hold (min)
Final hold (min)
I	1461.5
Reference	Santos, Moreira, et al., 2001
Comment	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Lo Presti, Sciarrone, et al., 2008
Lo Presti, M.; Sciarrone, D.; Crupi, M.C.; Costa, R.; Ragusa, S.; Dugo, G.; Mondello, L., Evaliation of the volatile and chiral composition in Pistacia lentiscus L. essential oil, Flavour Fragr. J., 2008, 23, 4, 249-257, https://doi.org/10.1002/ffj.1878 . [all data]

Adams, Beauchamp, et al., 2007
Adams, R.P.; Beauchamp, P.S.; Dev, V.; Dutz, S.M., New Natural Products Isolated from One-Seeded Juniperus of the Southwestern United States: Isolation and Occurence of 2-Ethenyl-3-methyl Phanol and Its Derivatives, J. Essent. Oil Res., 2007, 19, 2, 146-152, https://doi.org/10.1080/10412905.2007.9699247 . [all data]

Morteza-Semnani, Akbarzadeh, et al., 2006
Morteza-Semnani, K.; Akbarzadeh, M.; Changizi, S., Essential oils composition of Stachys byzantina, S. inflata, S. lavandulifolia and S. laxa from Iran, Flavour Fragr. J., 2006, 21, 2, 300-303, https://doi.org/10.1002/ffj.1594 . [all data]

Morteza-Semnani K., Saeedi M., et al., 2006
Morteza-Semnani K.; Saeedi M.; Changizi S., The essential oil composition of Hypericum scabrum L. from Iran, Flavour Fragr. J., 2006, 21, 3, 513-515, https://doi.org/10.1002/ffj.1614 . [all data]

Pintore G., Chessa M., et al., 2006
Pintore G.; Chessa M.; Manconi P.; Zanetti S.; Deriu A.; Tirillini B., Chemical composition and antimicrobial activities of essential oil of stachys glutinosa L. from Sardinia, Natural Product Communications, 2006, 1, 12, 1133-1136. [all data]

Tornambe, Cornu, et al., 2006
Tornambe, G.; Cornu, A.; Pradel, P.; Kondjoyan, N.; Carnat, A.P.; Petit, M.; Martin, B., Changes in Terpene Content in Milk from Pasture-Fed Cows, J. Dairy Sci., 2006, 89, 6, 2309-2319, https://doi.org/10.3168/jds.S0022-0302(06)72302-5 . [all data]

Chaverri and Cicció, 2005
Chaverri, C.; Cicció, J.F., Essential oil of trees of the genus Ocotea (Lauraceae) in Costa Rica. I. Ocotea brenesii, Rev. Biol. Trop., 2005, 53, 3-4, 431-436, https://doi.org/10.15517/rbt.v53i3-4.14611 . [all data]

Cornu, Kondjoyan, et al., 2005
Cornu, A.; Kondjoyan, N.; Martin, B.; Verdier-Metz, I.; Pradel, P.; Berdague, J.-L.; Coulon, J.-B., Terpene profiles in Cantal and Saint-Nectairetype cheese made from raw or pasteurised milk, J. Sci. Food Agric., 2005, 85, 12, 2040-2046, https://doi.org/10.1002/jsfa.2214 . [all data]

Cicció and Gómez-Laurito, 2002
Cicció, J.F.; Gómez-Laurito, J., Volatile constituents of the leaves of Siparuna thecaphora (Siparunaceae) from Turrialba, Costa Rica, Rev. Biol. Trop., 2002, 50, 3/4, 963-967. [all data]

Santos, Moreira, et al., 2001
Santos, P.R.; Moreira, D.L.; Guimaraes, E.F.; Kaplan, M.A.C., Essential oil analysis of 10 piperaceae species from the Brazilian Atlantic forest, Phytochemistry, 2001, 58, 4, 547-551, https://doi.org/10.1016/S0031-9422(01)00290-4 . [all data]

Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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