Galactose, TMS
- Formula: C21H52O6Si5
- Molecular weight: 541.0615
- IUPAC Standard InChI: InChI=1S/C21H52O6Si5/c1-28(2,3)22-16-17-18(24-29(4,5)6)19(25-30(7,8)9)20(26-31(10,11)12)21(23-17)27-32(13,14)15/h17-21H,16H2,1-15H3/t17?,18-,19?,20?,21?/m0/s1
- IUPAC Standard InChIKey: PPFHNIVPOLWPCF-ANSLWWGBSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- α-D-Mannopyranose, 5TMS derivative
- β-D-Glucopyranose, 5TMS derivative
- α-D-Glactopyranose, 5TMS derivative
- β-Galactopyranose, TMS
- α-D-Glucopyranose, 5TMS derivative
- α-D-Galactose, TMS
- β-Gulopyranose, TMS
- [2H]Mannose, TMS
- A-Psicopyranose, TMS
- A-Sorbopyranose, TMS
- B-Psicopyranose, TMS
- B-Sorbopyranose, TMS
- α-Mannose, TMS
- α-Mannopyranose, TMS
- D(+)-Talose, aldol, TMS
- D-Altrose, aldol, TMS
- α-Allopyranose, TMS
- α-Altropyranose, TMS
- α-Gulopyranose, TMS
- α-Idopyranose, TMS
- α-Talopyranose, TMS
- β-Allopyranose, TMS
- β-Altropyranose, TMS
- β-Idopyranose, TMS
- β-Mannopyranose, TMS
- β-Talopyranose, TMS
- D-Glucopyranose, penta-TMS
- α-Glucopyranoside, TMS
- Glucose, TMS # 2
- β-D-(+)-Mannopyranose, 5TMS derivative
- D-(+)-Galactopyranose, 5TMS derivative (isomer 1)
- D-(+)-Galactopyranose, 5TMS derivative (isomer 2)
- β-D-Allopyranose, 5TMS derivative
- α-D-(+)-Talopyranose, 5TMS derivative
- β-D-(+)-Talopyranose, 5TMS derivative
- α-D-Allopyranose, 5TMS derivative
- Other names: D-Galactose, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1848. | Fu, Iga, et al., 2000 | 30. m/0.25 mm/0.25 μm, He, 100. C @ 1. min, 10. K/min, 290. C @ 8. min |
| Capillary | DB-5 | 1876. | Fu, Iga, et al., 2000 | 30. m/0.25 mm/0.25 μm, He, 100. C @ 1. min, 10. K/min, 290. C @ 8. min |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | OV-101 | 1910. | Binder and Haddon, 1984 | Helium; Column length: 42. m; Column diameter: 0.50 mm; Program: 60 0C (0.5 min) 30 0C/min -> 170 0C 3 0C/min -> 220 0C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Fu, Iga, et al., 2000
Fu, X.; Iga, M.; Kimura, M.; Yamaguchi, S.,
Simplified screening for organic acidemia using GC/MS and dried urine filter paper: a study on neonatal mass screening,
Early Hum. Dev., 2000, 58, 1, 41-55, https://doi.org/10.1016/S0378-3782(00)00053-0
. [all data]
Binder and Haddon, 1984
Binder, R.B.; Haddon, W.F.,
Analysis of O-methylinositols by gas-liquid chromatography-mass spectrometry,
Carbohydrate Research, 1984, 129, 21-32, https://doi.org/10.1016/0008-6215(84)85295-7
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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