4-Chlorodehydromethyltestosterone, per-TMS
- Formula: C26H43ClO2Si2
- Molecular weight: 479.242
- IUPAC Standard InChI: InChI=1S/C26H43ClO2Si2/c1-24-15-14-22(28-30(4,5)6)23(27)21(24)11-10-18-19(24)12-16-25(2)20(18)13-17-26(25,3)29-31(7,8)9/h11,14-15,18-20H,10,12-13,16-17H2,1-9H3
- IUPAC Standard InChIKey: GBKVYVYEVCEEMU-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Species with the same structure:
- Stereoisomers:
- Other names: 4-Chloro-1,2-dehydro-17α-methyltestosterone, bis-TMS
- Information on this page:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-1 | 2931. | Schänzer, Horning, et al., 1995 | 17. m/0.2 mm/0.11 μm, He, 5. K/min; Tstart: 180. C; Tend: 320. C |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-54 | 2993. | Schänzer, Opfermann, et al., 1992 | 5. K/min; Column length: 17. m; Phase thickness: 0.33 μm; Tstart: 200. C; Tend: 320. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Schänzer, Horning, et al., 1995
Schänzer, W.; Horning, S.; Donike, M.,
Metabolism of anabolic steroids in humans: Synthesis of 6β-hydroxy metabolites of 4-chloro-1,2-dehydro-17α -methyltestosterone, fluoxymesterone, and metandienone,
Steroids, 1995, 60, 4, 353-366, https://doi.org/10.1016/0039-128X(95)00008-E
. [all data]
Schänzer, Opfermann, et al., 1992
Schänzer, W.; Opfermann, G.; Donike, M.,
17-Epimerization of 17α-methyl anabolic steroids in humans: metabolism and synthesis of 17α-hydroxy-17β-methyl steroids,
Steroids, 1992, 57, 11, 537-550, https://doi.org/10.1016/0039-128X(92)90023-3
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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