Pyreno[4,5-b]thiophene


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Lee's RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5446.9Becker and Colmsjö, 199830. m/0.25 mm/0.25 μm, He, 110. C @ 1. min, 10. K/min, 325. C @ 5. min
CapillarySE-52446.74Kong, Lee, et al., 1982H2, 8. K/min; Column length: 19.6 m; Column diameter: 0.32 mm; Tstart: 40. C; Tend: 280. C
CapillarySE-52446.51Vassilaros, Kong, et al., 198220. m/0.30 mm/0.25 μm, H2, 40. C @ 2. min, 4. K/min; Tend: 265. C

Lee's RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-5438.0Becker and Colmsjö, 199830. m/0.25 mm/0.25 μm, He; Program: 110C(1min) => 40C/min => 160C => 10C/min => 300C925min)
CapillaryDB-5438.5Becker and Colmsjö, 199830. m/0.25 mm/0.25 μm, He; Program: 35C(2min) => 25C/min => 160C => 3C/min => 300C(25min)

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Becker and Colmsjö, 1998
Becker, G.; Colmsjö, A., Gas chromatography-atomic emission detection for quantification of polycyclic aromatic sulfur heterocycles, Anal. Chim. Acta., 1998, 376, 3, 265-272, https://doi.org/10.1016/S0003-2670(98)00546-7 . [all data]

Kong, Lee, et al., 1982
Kong, R.C.; Lee, M.L.; Tominaga, Y.; Pratap, R.; Iwao, M.; Castle, R.N.; Wise, S.A., Capillary Column Gas Chromatographic Resolution of Isomeric Polycylic Aromatic Sulfur Heterocycles in a Coal Liquid, J. Chromatogr. Sci., 1982, 20, 11, 502-510, https://doi.org/10.1093/chromsci/20.11.502 . [all data]

Vassilaros, Kong, et al., 1982
Vassilaros, D.L.; Kong, R.C.; Later, D.W.; Lee, M.L., Linear retention index system for polycyclic aromatic compounds. Critical evaluation and additional indices, J. Chromatogr., 1982, 252, 1-20, https://doi.org/10.1016/S0021-9673(01)88394-1 . [all data]


Notes

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