Aphyllidine
- Formula: C15H22N2O
- Molecular weight: 246.3480
- IUPAC Standard InChI: InChI=1S/C15H22N2O/c18-15-12-9-11(13-5-2-4-8-17(13)15)10-16-7-3-1-6-14(12)16/h5,11-12,14H,1-4,6-10H2/t11?,12?,14-/m1/s1
- IUPAC Standard InChIKey: UAAWNTMXVSONPU-ORHYLEIMSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 2120. | Beuerle, 2010 | He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 150. C; Tend: 300. C |
| Capillary | DB-5 | 2127. | Przybylak, Ciesiolka, et al., 2005 | He, 180. C @ 2. min, 5. K/min, 300. C @ 10. min; Column length: 30. m; Column diameter: 0.25 mm |
| Capillary | DB-1 | 2145. | Torres, Quintos, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 120. C @ 3. min, 10. K/min, 260. C @ 10. min |
| Capillary | DB-1 | 2125. | Martínez-Herrera, Robledo-Quintos, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 2. K/min, 280. C @ 15. min; Tstart: 150. C |
| Capillary | DB-1 | 2127. | Greinwald, Bachmann, et al., 1995 | He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 150. C; Tend: 300. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 2120. | Wink, Meissner, et al., 1995 | Column length: 30. m; Column diameter: 0.3 mm; Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Beuerle, 2010
Beuerle, T.,
MS and RI data. Personal communication., 2010. [all data]
Przybylak, Ciesiolka, et al., 2005
Przybylak, J.K.; Ciesiolka, D.; Wysocka, W.; García-López, P.M.; Ruiz-López, M.A.; Wysocki, W.; Gulewicz, K.,
Alkaloid profiles of Mexican wild lupin and an effect of alkaloid preparation from Lupinus exaltatus seeds on growth and yield of paprika (Capsicum annuum L.),
Ind. Crops Prod., 2005, 21, 1, 1-7, https://doi.org/10.1016/j.indcrop.2003.12.001
. [all data]
Torres, Quintos, et al., 2002
Torres, K.B.; Quintos, N.R.; Necha, L.L.B.; Wink, M.,
Alkaloid profile of leaves and seeds of Lupinus hintonii C.P. Smith,
Z. Naturforsch., 2002, 57c, 243-247. [all data]
Martínez-Herrera, Robledo-Quintos, et al., 2001
Martínez-Herrera, J.; Robledo-Quintos, N.; Mora-Escobedo, R.; Dávila-Ortiz, G.,
Alkaloid composition of Lupinus campestris from Mexico,
J. Food Biochem., 2001, 25, 2, 117-125, https://doi.org/10.1111/j.1745-4514.2001.tb00728.x
. [all data]
Greinwald, Bachmann, et al., 1995
Greinwald, R.; Bachmann, P.; Lewis, G.; Witte, L.; Czygan, F.-C.,
Alkaloids of the genus Poecilanthe (Leguminosae: Papilionoideae),
Biochem. Syst. Ecol., 1995, 23, 5, 547-553, https://doi.org/10.1016/0305-1978(95)00050-5
. [all data]
Wink, Meissner, et al., 1995
Wink, M.; Meissner, C.; Witte, L.,
Patterns of quinolizidine alkaloids in 56 species of the genus Lupinus,
Phytochemistry, 1995, 38, 1, 139-153, https://doi.org/10.1016/0031-9422(95)91890-D
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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