13,17-Dimethylheptatriacontane
- Formula: C39H80
- Molecular weight: 549.0525
- IUPAC Standard InChI: InChI=1S/C39H80/c1-5-7-9-11-13-15-17-18-19-20-21-22-23-24-26-28-30-32-35-39(4)37-33-36-38(3)34-31-29-27-25-16-14-12-10-8-6-2/h38-39H,5-37H2,1-4H3
- IUPAC Standard InChIKey: KVVOPMLJQVAOCC-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Heptatriacontane, 13,17-dimethyl
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | Methyl Silicone | 225. | 3752. | Pomonis, Hakk, et al., 1989 | He; Column length: 12.5 m |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Ultra-1 | 3758. | Nelson, Adams, et al., 2003 | 150. C @ 4. min, 4. K/min, 320. C @ 30. min; Column length: 12. m; Column diameter: 0.2 mm |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 3755. | Bernier, Carlson, et al., 1998 | 30. m/0.32 mm/0.25 μm; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Ultra-1 | 3758. | Nelson and Charlet, 2003 | He, 4. K/min; Column length: 12.5 m; Column diameter: 0.2 mm; Tstart: 150. C; Tend: 320. C |
| Packed | OV-101 | 3758. | Nelson, de Renobales, et al., 1989 | Helium, Gas-Chrom Q (100-120 mesh), 3. K/min, 320. C @ 25. min; Column length: 3. m; Tstart: 150. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 3755. | Carlson, Geden, et al., 1999 | 30. m/0.32 mm/0.25 μm, He; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C (12 - 42 min) |
| Capillary | CP Sil 5 CB | 3758. | Kenig, Sinninghe Damsté, et al., 1995 | 25. m/0.32 mm/0.2 μm, He; Program: 50C => 20C/min => 130C => 4C/min => 300C (20min) |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Pomonis, Hakk, et al., 1989
Pomonis, J.G.; Hakk, H.; Fatland, C.L.,
Synthetic methyl- and dimethylalkanes. Kovats indices [13C]NMR and mass spectra of some methylpentacosanes and 2,X-dimethylheptacosanes,
J. Chem. Ecol., 1989, 15, 9, 2319-2333. [all data]
Nelson, Adams, et al., 2003
Nelson, D.R.; Adams, T.S.; Fatland, C.L.,
Hydrocarbons in the surface wax of eggs and adults of the Colorado potato beetle, Leptinotarsa decemlineata,
Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 134, 3, 447-466, https://doi.org/10.1016/S1096-4959(02)00262-2
. [all data]
Bernier, Carlson, et al., 1998
Bernier, U.R.; Carlson, D.A.; Geden, C.J.,
Gas chromatography/mass spectrometry analysis of the cuticular hydrocarbons from parasitic wasps of the genus Muscidifurax,
J. Am. Soc. Mass Spectrom., 1998, 9, 4, 320-332, https://doi.org/10.1016/S1044-0305(97)00288-2
. [all data]
Nelson and Charlet, 2003
Nelson, D.R.; Charlet, L.D.,
Cuticular hydrocarbons of the sunflower beetle,Zygogramma exclamationis,
Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 135, 2, 273-284, https://doi.org/10.1016/S1096-4959(03)00080-0
. [all data]
Nelson, de Renobales, et al., 1989
Nelson, D.R.; de Renobales, M.; Dwyer, L.A.; Zamboni, A.C.; Fatland, C.L.; Blomquist, G.J.,
Novel very long-chain methyl branched alcohols and their esters, and methyl branched alkanes in pupae of the gabbage looper, Trichoplusa ni (Hubner),
Insect Biochem., 1989, 19, 2, 197-208, https://doi.org/10.1016/0020-1790(89)90092-9
. [all data]
Carlson, Geden, et al., 1999
Carlson, D.A.; Geden, C.J.; Bernier, U.R.,
Identification of pupal exiviae of Nasania vitripennis and Muscidifurax raptorellus parasitoids using cuticular hydrocarbons,
Biol. Control, 1999, 15, 2, 97-106, https://doi.org/10.1006/bcon.1999.0708
. [all data]
Kenig, Sinninghe Damsté, et al., 1995
Kenig, F.; Sinninghe Damsté, J.S.; Kock-van Dalen, A.C.; Rijpstra, W.I.C.; Huc, A.Y.; de Leeuw, J.W.,
Occurrence and origin of mono-, di-, and trimethylalkanes in modern and holocene cyanobacterial mats from Abu Dhabi, United Arab Emirates,
Geochim. Cosmochim. Acta, 1995, 59, 14, 2999-3015, https://doi.org/10.1016/0016-7037(95)00190-5
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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