5B-Androstan-3A,16B,17B-triol, tris-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-302798.Ludwig-Köhn, Sziedat, et al., 1980He, 2. K/min; Column length: 20. m; Tstart: 150. C; Tend: 295. C
PackedSE-302803.Grote and Spiteller, 1977Chromosorb W AW DMCS, 1. K/min; Column length: 1.5 m; Tstart: 200. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-1012807.Pfeifer and Spiteller, 1981H2, 2. K/min; Column length: 50. m; Column diameter: 0.30 mm; Tstart: 150. C; Tend: 300. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ludwig-Köhn, Sziedat, et al., 1980
Ludwig-Köhn, H.; Sziedat, A.; Spiteller, G.; Matthaei, D.; Henning, H.V.; Scheler, F., Occurrence of highly oxygen-substituted androgens in hemofiltrates of uremic patients, Biomed. Mass Spectrom., 1980, 7, 7, 284-287, https://doi.org/10.1002/bms.1200070704 . [all data]

Grote and Spiteller, 1977
Grote, H.; Spiteller, G., Location of Functional Groups with the Aid of Mass Spectrometry. XVI-Mass Spectra of Trimethylsilylated Androstan-3,16,17β-triols, Biomed. Mass Spectrom., 1977, 4, 4, 216-219, https://doi.org/10.1002/bms.1200040405 . [all data]

Pfeifer and Spiteller, 1981
Pfeifer, P.; Spiteller, G., Steroid Profiles of Healthy Individuals, J. Chromatogr., 1981, 223, 1, 21-32, https://doi.org/10.1016/S0378-4347(00)80064-X . [all data]


Notes

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