23,24-Dinor-5-cholene-3β,22-diol, di-TMS
- Formula: C31H58O2Si2
- Molecular weight: 518.9620
- IUPAC Standard InChI: InChI=1S/C31H58O2Si2/c1-21(2)29(33-35(9,10)11)22(3)26-14-15-27-25-13-12-23-20-24(32-34(6,7)8)16-18-30(23,4)28(25)17-19-31(26,27)5/h12,21-22,24-29H,13-20H2,1-11H3/t22-,24+,25?,26?,27?,28?,29?,30?,31?/m0/s1
- IUPAC Standard InChIKey: SXEZYKXHWNDRJU-OUHVWKBWSA-N
- Chemical structure:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-1 | 265. | 2975. | Gaskell, Smith, et al., 1975 | N2; Column length: 2. m |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Gaskell, Smith, et al., 1975
Gaskell, S.J.; Smith, A.G.; Brooks, C.J.W.,
Gas chromatography mass spectrometry of trimethylsilyl ethers of sidechain hydroxylated Δ4-3-ketosteroids. Long range trimethylsilyl group migration under electron impact,
Biomed. Mass Spectrom., 1975, 2, 3, 148-155, https://doi.org/10.1002/bms.1200020309
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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