Acetylglycine, bis-TMS
- Formula: C10H23NO3Si2
- Molecular weight: 261.4655
- IUPAC Standard InChI: InChI=1S/C10H23NO3Si2/c1-9(13-15(2,3)4)11-8-10(12)14-16(5,6)7/h8H2,1-7H3
- IUPAC Standard InChIKey: MEERPCCZBNRYNP-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Acetic acid, acetylamino, bis-TMS; N-ACETYLGLYCINE TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 1359. | Tsai, Oliphant, et al., 1985 | He; Program: not specified |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5MS | 1389. | Lee, Yanamandra, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 70. C @ 3. min, 4. K/min, 280. C @ 3. min |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1372. | Kawana, Nakagawa, et al., 2008 | 30. m/0.25 mm/0.25 μm; Program: Total analysis run time was optimized to be 15 min |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Tsai, Oliphant, et al., 1985
Tsai, M.Y.; Oliphant, C.; Josephson, M.W.,
Identification of Metabolites Diagnostic for Organic Acidurias by Simultaneous Dual-Column Capillary Gas Chromatography,
J. Chromatogr., 1985, 341, 1-10, https://doi.org/10.1016/S0378-4347(00)84004-9
. [all data]
Lee, Yanamandra, et al., 2002
Lee, B.Y.; Yanamandra, K.; Thurmon, T.F.,
Quantitative estimation of organic analytes with a capillary column,
Am. Clin. Lab., 2002, May, 30-34. [all data]
Kawana, Nakagawa, et al., 2008
Kawana, S.; Nakagawa, K.; Hesegawa, Y.; Kobayashi, H.; Yamaguchi, S.,
Improvement of sample throghput using gas chromatography-mass spectrometry for biochemical diagnosis of organic acid disorders,
Clin. Chim. Acta, 2008, 392, 1-2, 34-40, https://doi.org/10.1016/j.cca.2008.02.025
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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