γ-Terpinene

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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-1RTX-1RTX-1Mega-5
Column length (m) 30.30.60.60.25.
Carrier gas HeliumHydrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.220.25
Phase thickness (μm) 0.250.250.250.250.25
Program 70 0C 5 0C/min -> 120 0C 10 0C/min -> 280 0C (20 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specifiednot specifiednot specified
I 1056.1035.1049.1049.1060.
ReferencePurushothaman and Ravi, 2013Albano, Lima, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dell'Agli, Sanna, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSSLB-5 MSPolydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groupsHP-5 MS
Column length (m) 30.30.  30.
Carrier gas HeliumHelium  Helium
Substrate      
Column diameter (mm) 0.250.25  0.25
Phase thickness (μm) 0.250.25  0.25
Program not specifiednot specifiednot specifiednot specified40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
I 1058.1062.1062.1062.1058.
ReferenceMondello, 2012Mondello, 2012Robinson, Adams, et al., 2012Robinson, Adams, et al., 2012Sharopov, Sulaimonova, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Siloxane, 5 % PhDB-55 % Phenyl polydimethyl siloxaneHP-5 MS
Column length (m) 25. 30. 30.
Carrier gas Hydrogen Helium Helium
Substrate      
Column diameter (mm) 0.32 0.25 0.25
Phase thickness (μm) 0.52 0.25 0.25
Program not specifiednot specifiednot specifiednot specified60 0C (1 min) 10 0C -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)
I 1060.1059.1088.1060.1057.
ReferenceVelickovic, Ristic, et al., 2012VOC BinBase, 2012Cao, Li, et al., 2011Chaverri, Diaz, et al., 2011Chu, Liu, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1 HP-5DB-5HP-5 MS
Column length (m) 30. 30.60. 
Carrier gas Helium NitrogenHelium 
Substrate      
Column diameter (mm) 0.25 0.250.25 
Phase thickness (μm) 0.25 0.251.00 
Program 50 0C (5 min) 3 0C/min -> 240 0C 15 0C/min -> 300 0C (3 min)not specified35 0C (10 min) 3 0C/min -> 205 0C 10 0C/min -> 225 0C40 0C 4 0C/min -> 230 0C 100 0C/min -> 260 0C (11.7 min)not specified
I 1062.1074.1062.1073.1062.
ReferenceFathi, Sahari, et al., 2011Karimi, Farmany, et al., 2011Laribi, Kouki, et al., 2011Miyazaki, Plotto, et al., 2011Payo, Colo, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSPolydimethyl siloxane, 5 % phenylHP-5HP-5 MS
Column length (m)    30.30.
Carrier gas    HeliumHelium
Substrate      
Column diameter (mm)    0.250.25
Phase thickness (μm)    0.250.25
Program not specifiednot specifiednot specified60 0C (1 min) 10 0C/min -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)50 0C (1.5 min) 10 0C/min -> 180 0C (2 min) 6 0C/min -> 280 0C (10 min)
I 1063.1065.1059.1057.1047.
ReferencePayo, Colo, et al., 2011Payo, Colo, et al., 2011Skogerson, Wohlgemuth, et al., 2011Wang, Liu, et al., 2011Wang, Xu, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5RTx-1HP-5 MSHP-5 MS
Column length (m) 30.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.250.32
Phase thickness (μm) 0.250.250.250.250.25
Program 50 0C (2 min) 3 0C/min -> 130 0C (2 min) 5 0C/min -> 270 0Cnot specifiednot specified60 0C (1 min) 10 0C/min -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)not specified
I 1054.1060.1049.1057.1060.
ReferenceBamoniri, Mirjalili, et al., 2010Bi Kouame, Bedi, et al., 2010Dib, Bendahou, et al., 2010Liu, Chu, et al., 2010Pino, Marquez, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SLB-5 MSHP-5 MSDB-1-MSDB-5
Column length (m) 30.10.30.60.30.
Carrier gas HydrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.100.250.250.25
Phase thickness (μm) 0.250.100.250.250.25
Program 35 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 280 0Cnot specified50 0C (3 min) 3 0C/min -> 160 0C (10 min) 3 0C/min -> 240 0Cnot specified50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C
I 1060.1058.1060.1048.1062.
ReferencePontes, Silva, et al., 2010Scandinaro, Tranchida, et al., 2010Sharifiar, Yassa, et al., 2010Takeoka, Hobbs, et al., 2010Courtois, Paine, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSOptima-5MS5 % Phenyl methyl siloxaneElite-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)40 0C (3 min) 3 0C/min -> 160 0C (2 min) 8 0C/min -> 220 0C (3 min)40 0C (5 min) 5 0C/min -> 230 0C 30 0C/min -> 280 0C (5 min)50 0C (2 min) 10 0C/min -> 150 0C 15 0C/min -> 300 0C (10 min)60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)
I 1056.1061.1054.1067.1050.
ReferenceDelort and Jaquier, 2009Fan, Lu, et al., 2009HEuskin, Godin, et al., 2009Huang, Qin, et al., 2009Kapoor, Singh, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5DB-1DB-1DB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeliumHeliumHydrogenHydrogenHelium
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.170.250.250.25
Program 50 0C (5 min) 6 0C/min -> 125 0C 10 0C/min -> 170 0C60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified
I 1056.1063.1035.1035.1062.
ReferenceKeefover-Ring, Thompson, et al., 2009Maggi, Bilek, et al., 2009Mendes, Trindade, et al., 2009Mendes, Trindade, et al., 2009, 2Porto, Decorti, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1 HTOV-1HP-5 MSSLB-5 MSSLB-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.10 0.250.250.25
Program 40 0C 2 0C/min -> 100 0C 5 0C/min -> 230 0C (5 min)40 0C 2 0C/min -> 130 0C (5 min) 10 0C/min -> 230 0C (15 min)32 0C (1 min) 50 0C/min -> 115 0C 1.5 0C/min -> 145 0C 12 0C/min -> 240 0C (10 min)50 0C 3 0C/min -> 250 0C (1 min) 10 0C/min -> 300 0C (5 min)not specified
I 1039.1040.1062.1058.1054.
ReferenceYang, Kim, et al., 2009Yu, Li, et al., 2009Zellner, Amorim, et al., 2009Costa, De Fina, et al., 2008Costa, De Fina, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CB-1CB-1CP Sil 8 CBSLB-5 MS
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min)not specifiednot specifiednot specified
I 1061.1043.1051.1060.1058.
ReferenceIsidorov, Lech, et al., 2008Kannaste, Vongvanich, et al., 2008Kannaste, Vongvanich, et al., 2008Kupcinskiene, Stikliene, et al., 2008Lo Presti, Sciarrone, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5BPX-5DB-5 MS
Column length (m) 30.30.30.7.530.
Carrier gas HeHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.250.250.100.25
Phase thickness (μm) 0.250.250.2510.0.25
Program 45C => 3C/min => 175C => 15C/min => 300C (10min)40 0C (3 min) 3 0C/min -> 160 0C (2 min) 8 0C/min -> 220 0C (3 min)not specifiednot specified80 0C (1.5 min) 4 pC/min -> 180 0C 10 0C/min -> 300 0C (10 min)
I 1035.1063.1074.1058.1057.
ReferenceNogueira, Marcelo-Curto, et al., 2008Qiao, Xie, et al., 2008Qiao, Xie, et al., 2008Shellie, 2008Silva, Doria, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5MSHP-5MSHP-5MSDB-1
Column length (m)  30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program not specified60C => 1C/min => 65C => 3C/min => 120C => 5C/min => 180C(5min) => 5C/min => 250C (20min)40C => 3C/min => 100C => 5C/min => 230C(2min)40C(10min) => 3C/min => 200C => 2C/min => 220C45C => 3C/min => 175C => 15C/min => 300C (10min)
I 1065.1056.1057.1060.1035.
ReferenceAgabriel, Cornu, et al., 2007Barra A., Coroneo V., et al., 2007Chokeprasert P., Charles A.L., et al., 2007Cole, Haber, et al., 2007Ferreira, Meireles de Sousa, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-5DB-5 MSDB-1HP-5
Column length (m) 30.30.30.30. 
Carrier gas HeHeHeliumH2 
Substrate      
Column diameter (mm) 0.250.320.250.25 
Phase thickness (μm) 0.250.250.250.25 
Program 40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C60C => 4C/min => 150C => 10C/min => 220C60 0C 3 0C/min -> 210 0C 5 0C/min -> 250 0C45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified
I 1057.1057.1062.1035.1058.
ReferenceFormisano, Mignola, et al., 2007Hashemi, Abolghasemi, et al., 2007Haznagy-Radnai, Szigle, et al., 2007Kamatou, Viljoen, et al., 2007Liolios, Laouer, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-1HP-5 MSHP-5MSDB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.20.250.250.32
Phase thickness (μm) 0.250.330.250.250.25
Program 40C(3min) => 8C/min => 160C => 15C/min => 300C (10min)60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40C(10min) => 3C/min => 200C => 2C/min => 220C60 0C (1 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C
I 1060.1060.1060.1059.1060.
ReferenceLiu, Song, et al., 2007Merle, Verdeguer, et al., 2007Moriarity, Bansal, et al., 2007Moronkola, Ogunwande, et al., 2007Nivinsliene, Butkiene, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-SilDB-1BPX-55 % Phenyl methylsiloxaneHP-5 MS
Column length (m) 30.30.30. 30.
Carrier gas HeliumHeHe Helium
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (μm) 0.250.250.25  
Program 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C45C => 3C/min => 175C => 15C/min => 300C(10min)50C => 3C/min => 150C(10min) => 10C/min => 250Cnot specified40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C
I 1040.1035.1070.1067.1062.
ReferenceProffit, 2007Rodrigues, Antunes, et al., 2007Salamci, Kordali, et al., 2007Serrano, Cornu, et al., 2007Setzer, Stokes, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBPX-5SPB-5DB-1HP-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm)  0.251.0.250.25
Program 40C(10min) => 3C/min => 200C => 2C/min => 220C50C => 3C/min => 150C(10min) => 10C/min => 250C60C => 1C/min => 130C => 2C/min => 200C => 4C/min => 250C (40min)45C => 3C/min => 175C => 15C/min => 300C (10min)>2.5C/min => 180C => 100C/min => 250C (7.3min)
I 1064.1069.1050.1035.1058.
ReferenceTakaku, Haber, et al., 2007Baris, Güllüce, et al., 2006Chemat, Lucchesi, et al., 2006Figueiredo A.C., Barroso J.G., et al., 2006Goodner, Mahattanatawee, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-5CP Sil 8 CBDB-1SE-52
Column length (m) 30.60.50.30.25.
Carrier gas  HeHeHeH2
Substrate      
Column diameter (mm) 0.250.320.320.250.32
Phase thickness (μm) 0.251.0.25 0.42
Program >2.5C/min => 180C => 100C/min => 250C (7.3min)60C => 1C/min => 130C => 2C/min => 200C => 4C/min => 250C(40min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)35C => 4C/min => 180C => 10C/min => 250C60C(8min) => 3C/min => 180C => 20C/min => 250C (10min)
I 1058.1050.1060.1062.1054.
ReferenceGoodner, Mahattanatawee, et al., 2006Iriti, Colnaghi, et al., 2006Judzentiene and Buzelyte, 2006de Lima, Maia, et al., 2006Lorenzo, Loayza, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5BPX-5HP-5 MSDB-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHe HeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.100.250.250.250.25
Program 40 0C (1 min) 10 0C/min -> 120 0C 0.5 0C/min -> 150 0C 20 0C/min -> 280 0C (5 min)50C => 3C/min => 150C (10min) => 10C/min => 250C40 0C (3 min) 2 0C/min -> 150 0C 20 0C/min -> 220 0C (5 min)35C => 4C/min => 180C => 10C/min => 250C40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
I 1062.1068.1036.1060.1055.
ReferenceNavickiene, Morandim, et al., 2006Ozer H., Kilic H., et al., 2006Pyun and Shin, 2006Santos, Nunes, et al., 2006Schmidt, Noletto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5MSDB-5SE-52
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.250.250.250.15
Program 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C60C => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)60C(1min) => 1.5C => 185C => 9C/min => 275C (2min)60C => 2C/min => 100C => 3C/min => 160C => 5C/min => 280C45C => 1C/min => 100C => 5C/min => 250C (10min)
I 1053.1062.1064.1064.1060.
ReferenceSchmidt, Noletto, et al., 2006Singh, Marimuthu, et al., 2006Singh G., Maurya S., et al., 2006Srivastava, Mallavarapu, et al., 2006Tognolini, Barocelli, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSDB-1CP Sil 8 CBBP-5
Column length (m) 30.30.30.50.25.
Carrier gas He HeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.250.50
Program 60C => 3C/min => 180C => 250C (2min)70C(2min) => 10C/min => 150C(15min) => 5C/min => 240C45C => 3C/min => 175C => 15C/min => 300C(10min)50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)60 0C 6 0C/min -> 210 0C 10 0C/min -> 290 0C (10 min)
I 1056.1061.1035.1060.1063.
ReferenceTuberoso, Barra, et al., 2006Bagci and Baser, 2005Belhattab, Larous, et al., 2005Butkienë, Nivinskienë, et al., 2005Eyres, Dufour, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5BP-5BP-5BP-5DB-1
Column length (m) 25.25.25.25.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (μm) 0.500.500.500.500.25
Program not specified60 0C 6 0C/min -> 210 0C 10 0C/min -> 290 0C (10 min)60 0C 6 0C/min -> 210 0C 10 0C/min -> 290 0C (10 min)60 0C 6 0C/min -> 210 0C 10 0C/min -> 290 0C (10 min)45C => 3C/min => 175C => 15C/min => 300C (10min)
I 1061.1058.1061.1064.1035.
ReferenceEyres, Dufour, et al., 2005Eyres, Dufour, et al., 2005Eyres, Dufour, et al., 2005Eyres, Dufour, et al., 2005Faleio, Miguel, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5CP-Sil5 CB MSBPX-5CP Sil 8 CB
Column length (m) 30.30.50.30.50.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.250.251.20.250.25
Program 45C => 3C/min => 175C => 15C/min => 300C (10min)40C(1min) => 9C/min => 130C => 2C/min => 230C36C(2min) => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)60C(0.2min) => 3K/min => 186C => 10C/min => 240C (5min)60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)
I 1035.1054.1056.1062.1062.
ReferenceFigueiredo, Sim-Sim, et al., 2005Hamm, Bleton, et al., 2005Iraqi, Vermeulen, et al., 2005Judzentiene and Mockute, 2005Nivinskienë, Butkienë, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1BPX-5Polydimethyl siloxane with 5 % Ph groupsCP Sil 8 CB
Column length (m) 30. 30. 50.
Carrier gas   He He
Substrate      
Column diameter (mm) 0.25 0.25 0.32
Phase thickness (μm) 0.25 0.25 0.25
Program 40C(5min) => 3C/min => 90C => 10C/min => 280Cnot specified50C => 3C/min => 150C(10min) => 10C/min => 250Cnot specified60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min)
I 1061.1061.1068.1061.1061.
ReferenceNovak, Draxler, et al., 2005Omidbaigi and Bastan, 2005Özer, Sahín, et al., 2005Pino, Marbot, et al., 2005Radudienë, Judpintienë, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-5CP Sil 8 CBDB-1
Column length (m) 30.30.30.50.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm)  0.250.10.25 
Program 65C(1min) => 1C/min => 75C (2min) => 0.5C/min => 81C(2min) => 3C/min => 180C(7min)45C => 3C/min => 175C => 15C/min => 300C (15min)35C => 4C/min => 180C => 10C/min => 250C50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)35C => 4C/min => 180C => 10C/min => 250C
I 1064.1035.1051.1060.1062.
ReferenceSingh, Maurya, et al., 2005Touafek, Nacer, et al., 2005Albuquerque, Souza, et al., 2004Butkienë, Nivinskienë, et al., 2004Cavalcanti, de Morais, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeHP-5MS OV-1OV-1
Column length (m)  30. 15.30.
Carrier gas  He HeHe
Substrate      
Column diameter (mm)  0.25 0.3170.25
Phase thickness (μm)  0.25  0.25
Program not specified60C => 10C/min => 160C => 12C/min => 300C (5min)not specified50C(4min) => 4C/min => 90C => 10C/min => 300C(10min)45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C
I 1059.1064.1048.1048.1048.
ReferenceCouladis, Özcan, et al., 2004Deng, Li, et al., 2004El-Shazily, Hafez, et al., 2004El-Shazly and Hussein, 2004Hafez and Abdel-Salam, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CBDB-5DB-5DB-1
Column length (m) 50.50.30. 30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.320.320.25 0.25
Phase thickness (μm)  0.250.25 0.25
Program 60C(2min) => 5C/min => 160C (1min) => 10C/min => 250C (2min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)60C(4min) => 6C/min => 240 => 10C/min => 280Cnot specified45C => 3C/min => 175C => 15C/min => 300C (10min)
I 1062.1062.1060.1068.1035.
ReferenceJudpentienë and Mockutë, 2004Judpentienë and Mockutë, 2004, 2Letchamo, Ward, et al., 2004Lo Cantore, Iacobellis, et al., 2004Miguel, Simões, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CBMDN-5HP-5MSHP-5MS
Column length (m) 50.50.30.30.30.
Carrier gas HeHeHeliumHe 
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program 50 0C (2 min) 3 0C/min -> 180 0C (1 min) 20 0C/min -> 250 0C (2 min)50C(2min) => 3C/min => 180C(1min) => 20C/min => 250C (2min)30 0C (1 min) ballistically -> 60 0C 2 0C/min -> 120 0C 5 0C/min -> 280 0C (5 min)50C(3min) => 3C/min => 150C(10min) => 10C/min => 250C60C(1min) => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)
I 1062.1062.1055.1060.1064.
ReferenceMockutë, Bernotienë, et al., 2004Mockutë, Judbentienë, et al., 2004Moretti, Madonia, et al., 2004Sahin, Gulluce, et al., 2004Singh, Marimuthu, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-1DB-5SE-30
Column length (m) 30.30.30.  
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.250.25  
Phase thickness (μm) 0.250.250.25  
Program 60C(1min) => 0.5C/min => 85C(1min) => 1C/min => 105C (2min) => 10C/min => 275C(2min)50C (3min) => 3C/min => 150C (10min) => 10C/min => 250C45C => 3C/min => 175C => 15C/min => 300C (15min)not specifiednot specified
I 1064.1060.1035.1062.1050.
ReferenceSingh, Maurya, et al., 2004Tepe, Donmez, et al., 2004Touafek, Nacer, et al., 2004Vilaseca, Guy, et al., 2004Vinogradov, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30Methyl SiliconeHP-5DB-5CP-Sil 8CB-MS
Column length (m)   30.30.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)   0.250.250.32
Phase thickness (μm)   0.250.25 
Program not specified60 0C 3 0C/min -> 200 0C 15 0C/min -> 250 0C (5 min)50C(3min) => 3C/min => 150C(10min) => 10 C/min => 250C40C (1min) => 9C/min => 130C => 2C/min => 230C50C(2min) => 3C/min => 180C(1min) => 20C/min => 250C(2min)
I 1047.1062.1060.1054.1062.
ReferenceVinogradov, 2004Demyttenaere, Morina, et al., 2003Güllüce, Sökmen, et al., 2003Hamm, Lesellier, et al., 2003Mockute, Bernotiene, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CBDB-1HP-5AT-5
Column length (m) 50.50.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.250.250.10.250.25
Program 70C(5min) => 3C/min => 100C (1min) => 25C/min => 250C (10min)60C(1min) => 5C/min => 160C => 10C/min => 250C(5min)35C => 4C/min => 180C => 10C/min => 250C60C(5min) => 1C/min => 140C => 10C/min => 270C(5min)50 0C 5 0C/min -> 135 0C (1 min) 5 0C/min -> 225 0C (5 min) 5 0C/min -> 260 0C
I 1062.1062.1038.1064.1062.
ReferenceMockute and Judzentiene, 2003Mockute, Nivinskiene, et al., 2003Silva, Matos, et al., 2003Singh, Singh, et al., 2003Usai, Atzei, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSSE-30SE-30CP Sil 8 CB
Column length (m) 30.25.60.60.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.25   
Program 60C => 3C/min => 210C => 5C/min => 250C(2min)40C(2min) => 8C/min => 160C => 15C/min => 250C(3min)50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0Cnot specified60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (2min)
I 1059.01062.1056.1056.1062.
ReferenceVeres, Varga, et al., 2003Demyttenaere, Moriña, et al., 2002Li, Wu, et al., 2002Li, Wu, et al., 2002Mockute and Judzentiene, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-1DB-5HP-5MSHP-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm)  0.250.10.250.25
Program 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C(2min)40C(3min) => 5C/min => 180C => 15C/min => 240C(15min)35C => 4C/min => 180C => 20C/min => 280C40C (10min) => 3C/min => 120C => 10C/min => 250C (5min)not specified
I 1062.1068.1062.1058.1055.
ReferenceMockute and Judzentiene, 2002, 2Nogueira and Romano, 2002Viana, Andrade-Neto, et al., 2002Ansorena, Gimeno, et al., 2001Aparicio, Romero, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5CBP-1DB-5HP-5 MS
Column length (m) 30.30.25. 30.
Carrier gas  HeNitrogen Helium
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (μm) 0.25 0.25 0.25
Program 45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min)not specifiednot specifiednot specifiednot specified
I 1035.1062.1047.1060.1053.
ReferenceFigueiredo, Miguel, et al., 2001Isidorov, Zenkevich, et al., 2001Ly, Yamauchi, et al., 2001Petrakis, Tsitsimpikou, et al., 2001Shang, Hu, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5OV-101DB-5HP-1DB-1
Column length (m) 30.50.30.12.30.
Carrier gas HeN2HeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm) 0.25 0.250.330.25
Program 50 0C 3 K/min -> 200 0C 8 K/min -> 280 0Cnot specified40C => 2C/min => 60C => 4C/min => 260C40 0C 6.7 0C/min -> 87 0C (9 min) 10 0C/min -> 187 0C40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)
I 1055.1053.1065.1036.1035.
ReferenceUsubillaga, Aparicio, et al., 2001Yang, 2001Andrade, Maia, et al., 2000Betts, 2000Dorman, Figueiredo, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1DB-1DB-1DB-1DB-1
Column length (m)  30.30.30.30.
Carrier gas  HeHeHeH2
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program not specifiednot specifiednot specifiednot specified40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)
I 1045.1044.1049.1049.1035.
ReferenceJuliani, Biurrun, et al., 2000Kéita, Vincent, et al., 2000Kéita, Vincent, et al., 2000Kéita, Vincent, et al., 2000da Silva, Pedro, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-30DB-1CP Sil 5 CBDB-1
Column length (m) 30.30.30.25.60.
Carrier gas HeHeliumHe N2
Substrate      
Column diameter (mm) 0.250.250.250.390.32
Phase thickness (μm) 0.250.200.25 0.25
Program 45C => 3C/min => 170C => 15C/min => 300C(10min)not specified45C => 3C/min => 175C => 15C/min => 300C(10min)not specified40 0C (10 min) 40 - 80 0C at 2 0C/min 80 - 200 0C at 5 0C/min 200 0C (10 min)
I 1035.1057.1035.1054.1063.
ReferencePedro, da Silva, et al., 1999Prikhod'ko, Klyuev, et al., 1999Santos, Figueiredo, et al., 1999Weyerstahl, Marschall, et al., 1999Yen and Lin, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBOV-1DB-5DB-1
Column length (m) 30.50.50.30.30.
Carrier gas HeHeHeN2H2
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.251.20.250.250.25
Program 45C => 3C/min => 175C => 15C/min => 240C (10min)30C => 55C/min => 85C => 1C/min => 145C => 3C/min => 250C1)50C(1min) => 4C/min => 180C => 2C/min => 250C(10min) 2)50C(1min) => 6C/min => 200C => 12C/min => 250C(5min)45C(5min) => 2C/min => 200C => 5C/min => 250C45C => 3C/min => 175C => 15C => 240C(10min)
I 1035.1058.1055.1068.1035.
ReferenceBaratta, Dorman, et al., 1998Guyot, Bouseta, et al., 1998Kökdil, 1998Sanda, Koba, et al., 1998da Silva, Figueiredo, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1DB-5SPB-Sulfur
Column length (m) 30.30.30. 30.
Carrier gas HeH2He He
Substrate      
Column diameter (mm) 0.250.250.25 0.32
Phase thickness (μm) 0.250.250.25 4.
Program 60C => 3C/min => 240C => 30C/min => 300C45C => 3C/min => 175C => 15C/min => 240C(10min)45C => 3C/min => 175C => 15C/min => 280Cnot specifiednot specified
I 1058.1035.1035.1062.1049.
ReferenceYusuf, Begum, et al., 1998Figueiredo, Barroso, et al., 1997Gaspar, Palma, et al., 1997Isidorov, Zenkevich, et al., 1997Mariaca, Berger, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBMethyl Silicone5 % Phenyl methyl siloxaneDB-5DB-5
Column length (m) 30.  30.30.
Carrier gas N2    
Substrate      
Column diameter (mm) 0.25  0.320.32
Phase thickness (μm)    1.1.
Program not specifiednot specifiednot specified0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)
I 1055.1049.1056.1044.1045.
ReferenceWeyerstahl, Marschall, et al., 1997Zenkevich, 1996Sagrero-Nieves and Bartley, 1995Storer, Elmore, et al., 1993Storer, Elmore, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-54OV-101OV-101DB-1
Column length (m) 30.30.   
Carrier gas  He   
Substrate      
Column diameter (mm) 0.320.32   
Phase thickness (μm) 1.0.3   
Program 0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)35C(2min) => 40C/min => 50C(2min) => 6C/min => 230C(10min)not specifiednot specifiednot specified
I 1049.1062.1047.1047.1053.
ReferenceStorer, Elmore, et al., 1993Blank, Fischer, et al., 1989De Pooter, Vermeesch, et al., 1989De Pooter, Vermeesch, et al., 1989MacLeod and Snyder, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-1OV-101OV-101
Column length (m) 30.30.35.60. 
Carrier gas H2H2   
Substrate      
Column diameter (mm) 0.250.250.500.25 
Phase thickness (μm) 0.250.251.5  
Program 30C (2min) => 2C/min => 150C => 4C/min => 250C30C (2min) => 2C/min => 150C => 4C/min => 250Cnot specifiednot specifiednot specified
I 1043.1048.1047.1057.1057.
ReferenceTakeoka, Flath, et al., 1988Takeoka, Flath, et al., 1988De Pooter and Schamp, 1987Shibamoto, 1987Shibamoto, 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase OV-101
Column length (m) 2.5
Carrier gas N2
Substrate Chromosorb G 60-80mesh DMCS
Column diameter (mm)  
Phase thickness (μm)  
Program not specified
I 1053.
ReferenceSwigar and Silverstein, 1981
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Purushothaman and Ravi, 2013
Purushothaman, D.N.; Ravi, S., GC-MS analusis of essential oil obtained from Heracleum candolleanum (Wight et Arn), J. Pharmacy Res., 2013, 6, 1, 155-157, https://doi.org/10.1016/j.jopr.2012.11.032 . [all data]

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Notes

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