Carvone

Formula: C₁₀H₁₄O
Molecular weight: 150.2176
IUPAC Standard InChI: InChI=1S/C10H14O/c1-7(2)9-5-4-8(3)10(11)6-9/h4,9H,1,5-6H2,2-3H3
IUPAC Standard InChIKey: ULDHMXUKGWMISQ-UHFFFAOYSA-N
CAS Registry Number: 99-49-0
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
- D-Carvone
- (-)-Carvone
Other names: 2-Cyclohexen-1-one, 2-methyl-5-(1-methylethenyl)-; p-Mentha-6,8-dien-2-one; Carvol; Karvon; 1-Carvone; δ(6,8)-(9)-Terpadienone-2; 2-Methyl-5-isopropenyl-2-cyclohexen-1-one; NCI-C55867; 2-Methyl-5-isopropenyl-2-cyclohexenone; 6,8(9)-p-Menthadien-2-one; 2-Methyl-5-(1-methylethenyl)-2-cyclohexene-1-one; DL-Carvone; (.+/-.)-Carvone; 2-Methyl-5-(1-methylethenyl)-2-cyclohexen-1-one; Limonen-6-one; NSC 6275; cis-Dihydrocarvone; Dihydrocarvone; (Z)-dihydrocarvone; (-)-carvone; (Z)-Carvone; (E)-Carvone; R-(-)-carvone; (R)-Carvone; t-carvone; 1(6),8-p-Menthadien-2-one; trans-Carvone; d-p-mentha-1(6),8-dien-2-one
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Normal alkane RI, non-polar column, temperature ramp

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Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	RTX-1	RTX-1	HP-5 MS	HP-5 MS
Column length (m)	60.	60.	60.	25.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.30	0.25
T_start (C)	40.	60.	60.	40.	50.
T_end (C)	250.	230.	230.	260.	250.
Heat rate (K/min)	3.	2.	2.	10.	7.
Initial hold (min)	1.			2.	1.
Final hold (min)	20.	5.	5.	20.	5.
I	1212.	1214.	1214.	1284.	1240.
Reference	Sardashti, Valizadeh, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012	Sandoval-Montemayor, Garcia, et al., 2012	Zouari, Ayadi, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5 MS	VF-5 MS	VF-5 MS	DB-1
Column length (m)	30.	30.	60.	60.	50.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	30.	30.	60.
T_end (C)	240.	270.	260.	260.	250.
Heat rate (K/min)	3.	3.	2.	2.	8.
Initial hold (min)
Final hold (min)			28.	28.
I	1243.	1242.	1247.	1249.	1218.
Reference	Bertoli, Lepnardi, et al., 2011	Cui, Yang, et al., 2011	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011	Misharina T., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP-Sil 5 CB	ZB-5	ZB-5	DB-5 MS	HP-5 MS
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	Nitrogen	Nitrogen	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.26	0.25	0.25	0.25	0.25
T_start (C)	45.	40.	40.	40.	70.
T_end (C)	280.	200.	200.	250.	290.
Heat rate (K/min)	3.	5.	5.	5.	5.
Initial hold (min)		5.	5.	15.
Final hold (min)	22.		5.	15.	10.
I	1220.	1198.	1202.	1249.	1249.
Reference	Mothana, Hasson, et al., 2011	Vazques, Aimar, et al., 2011	Vazquez, Demmel, et al., 2011	Mesa-Arango, Betancur-Galvis, et al., 2010	Radulovic, Blagojevic, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5	OV-101	SE-54	DB-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	40.	70.	60.	70.
T_end (C)	290.	250.	220.	260.	240.
Heat rate (K/min)	5.	10.	2.	2.	5.
Initial hold (min)		1.		5.
Final hold (min)	10.	3.		999.
I	1247.	1224.	1228.	1240.	1257.
Reference	Radulovic, Dordevic, et al., 2010	Yang, Zhang, et al., 2010	Benites, Moiteiro, et al., 2009	Dayisoylu and Alma, 2009	Lawal and Oyedelji, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	5 % Phenyl methyl siloxane	DB-5	DB-1 MS	DB-5 MS
Column length (m)	25.	60.	30.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.25
T_start (C)	60.	90.	40.	40.	40.
T_end (C)	240.	225.	230.	250.	250.
Heat rate (K/min)	3.	3.	2.	6.	4.
Initial hold (min)				1.	2.
Final hold (min)	7.	3.		4.	2.
I	1241.	1244.	1246.	1214.	1254.
Reference	Maridass, 2009	Retta, Gattuso, et al., 2009	Scrivanti, Anton, et al., 2009	Seo, Kim, et al., 2009	Su, Wang, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5	SLB-5 MS	DB-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	N2	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	60.	50.	50.
T_end (C)	280.	280.	220.	250.	300.
Heat rate (K/min)	4.	9.	5.	3.	5.
Initial hold (min)		3.	10.	2.	5.
Final hold (min)		3.		10.	5.
I	1246.	1245.	1244.	1244.	1239.
Reference	Zhao, Zeng, et al., 2009	Aicha, Ines, et al., 2008	Flamini, Tebano, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Noudogbessi, Yedomonhan, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Elite-1	HP-5 MS	HP-5 MS	OV-1	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	65.	50.
T_end (C)	246.	250.	240.	260.	230.
Heat rate (K/min)	3.	2.	3.	6.	3.
Initial hold (min)		8.			10.
Final hold (min)		15.			10.
I	1240.	1236.	1250.	1228.	1242.
Reference	Raj, Baby, et al., 2008	Sahraoui, Vian, et al., 2008	Sarikurkcu, Tepe, et al., 2008	Wang, Yi, et al., 2008	Adams, Beauchamp, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	HP-5MS	HP-5MS	DBP-5
Column length (m)	50.	30.	30.	30.	25.
Carrier gas	Nitrogen	N2	He	He	Helium
Substrate
Column diameter (mm)	0.20	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.32	0.25	0.25	0.25	0.22
T_start (C)	60.	60.	60.	60.	40.
T_end (C)	220.	300.	250.	250.	250.
Heat rate (K/min)	5.	4.	2.	2.	3.
Initial hold (min)	3.		8.	8.	1.
Final hold (min)	5.		15.	15.	10.
I	1242.	1218.	1269.	1242.	1215.
Reference	Amiri, 2007	Baran, von Reuss, et al., 2007	Ferhat, Meklati, et al., 2007	Ferhat, Tigrine-Kordjani, et al., 2007	Heravi and Sereshti, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	SE-30	HP-5	Methyl Silicone	HP-5
Column length (m)	30.	30.	30.	50.	25.
Carrier gas	N2	He	He	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25		0.52
T_start (C)	50.	40.	40.	50.	40.
T_end (C)	200.	250.	250.	240.	280.
Heat rate (K/min)	5.	5.	5.	3.	4.
Initial hold (min)		5.	5.
Final hold (min)		10.	10.
I	1230.	1242.	1241.	1243.	1243.
Reference	Hnawia, Cabalion, et al., 2007	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007	Ozcan and Chalchat, 2007	Pavlovic, Petrovic, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DBP-5	DB-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	Helium	He	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22
T_start (C)	40.	50.	40.	60.	60.
T_end (C)	260.	240.	250.	200.	200.
Heat rate (K/min)	4.	4.	3.	2.	2.
Initial hold (min)			1.
Final hold (min)			10.	20.	20.
I	1240.	1193.	1215.	1232.	1242.
Reference	Ristic, Krivokuca-Dokic, et al., 2007	Sefidkon, Abbasi, et al., 2007	Sereshti and Samadi, 2007	Tiwary, Nail, et al., 2007	Tiwary, Nail, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He		N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	50.	50.
T_end (C)	280.	250.	240.	280.	280.
Heat rate (K/min)	3.	3.	5.	9.	9.
Initial hold (min)		5.	3.	3.	3.
Final hold (min)		10.	10.	3.	3.
I	1243.	1279.	1251.	1195.	1203.
Reference	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Wenguang, Wenlai, et al., 2007	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	ZB-5	BP-1	HP-5	HP-1
Column length (m)	30.	30.	50.	30.	50.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.32	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	260.	300.	220.	246.	250.
Heat rate (K/min)	4.	2.	2.	3.	2.
Initial hold (min)	5.
Final hold (min)			20.		40.
I	1240.	1193.	1213.	1242.	1212.
Reference	Askari and Sefidkon, 2006	Biondi, Sari, et al., 2006	Boti, Muselli, et al., 2006	Coronel, Cerda-Garcia-Rojas, et al., 2006	Filippi, Lanfranchi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	CP Sil 5 CB	CP Sil 5 CB	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	N2	N2	Nitrogen
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	50.
T_end (C)	260.	260.	300.	200.	280.
Heat rate (K/min)	3.	5.	4.	5.	5.
Initial hold (min)		2.
Final hold (min)		13.			5.
I	1246.	1243.	1220.	1223.	1242.
Reference	Javidnia, Miri, et al., 2006	Kucuk, Gulec, et al., 2006	Lis and Milczarek, 2006	Martin, Joseph, et al., 2006	Marzouk, Mansour, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DB-5	DB-5	NB-30
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.52	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	50.
T_end (C)	280.	220.	260.	220.	250.
Heat rate (K/min)	5.	4.	4.	4.	2.
Initial hold (min)			4.	5.
Final hold (min)	5.
I	1242.	1195.	1196.	1245.	1222.
Reference	Marzouk, Neffati, et al., 2006	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani, Saeedi, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Orav, Raal, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SPB-5	DB-5	DB-5	DB-5
Column length (m)	30.		30.	50.	25.
Carrier gas	He	He	He
Substrate
Column diameter (mm)	0.25		0.25	0.3	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.15
T_start (C)	40.	50.	40.	60.	40.
T_end (C)	240.	250.	250.	240.	220.
Heat rate (K/min)	4.	5.	4.	2.	3.
Initial hold (min)		3.			5.
Final hold (min)		15.
I	1241.	1242.	1214.	1246.	1243.
Reference	Sefidkon and Jamzad, 2006	Stojanovic, Palic, et al., 2006	Yadegarinia, Gachkar, et al., 2006	Chagonda and Chalchat, 2005	Chagonda and Chalchat, 2005, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	HP-5	DB-1	HP-5	HP-5
Column length (m)	60.	25.	60.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.3	0.2	0.25	0.25	0.25
Phase thickness (μm)		0.33	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	50.
T_end (C)	240.	240.	250.	300.	300.
Heat rate (K/min)	3.	3.	5.	5.	5.
Initial hold (min)				5.	5.
Final hold (min)		7.		5.	5.
I	1243.	1240.	1223.	1265.	1205.
Reference	Chalchat and Özcan, 2005	Duarte, Figueira, et al., 2005	Fakhari, Salehi, et al., 2005	Figuérédo, Cabassu, et al., 2005	Figuérédo, Cabassu, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	DB-1	DB-5	HP-5	DB-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	50.	60.	30.	60.
T_end (C)	280.	265.	240.	260.	220.
Heat rate (K/min)	6.	2.5	3.	2.	4.
Initial hold (min)	2.	1.		2.	5.
Final hold (min)	10.	30.		28.
I	1231.	1206.	1244.	1250.5	1243.
Reference	Jirovetz, Buchbauer, et al., 2005	Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005	Khayyat and Karimi, 2005	Leffingwell and Alford, 2005	Morteza-Semnani, Akbarzadeh, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5MS	DB-1	DB-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25
T_start (C)	40.	60.	60.	60.	40.
T_end (C)	250.	240.	275.	250.	240.
Heat rate (K/min)	5.	5.	4.	5.	4.
Initial hold (min)	0.5
Final hold (min)	2.			10.
I	1254.	1242.	1248.	1246.	1241.
Reference	Özel, Gögüs, et al., 2005	Saeidnia, Gohari, et al., 2005	Sajjadi and Ghannadi, 2005	Salehi, Sonboli, et al., 2005	Sefidkon and Jamzad, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5MS	PE-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	275.	240.	230.	230.	280.
Heat rate (K/min)	15.	3.	5.	3.	3.
Initial hold (min)			2.
Final hold (min)			4.	20.
I	1198.	1242.	1259.	1193.	1244.
Reference	Shams-Ardakani, Ghannadi, et al., 2005	da Silva, Andrade, et al., 2005	Singh, Raina, et al., 2005	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	BP-1	HP-5MS	DB-5	HP-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.32
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	250.	220.	240.	280.	250.
Heat rate (K/min)	5.	5.	3.	3.	5.
Initial hold (min)			3.		3.
Final hold (min)	10.	15.
I	1219.	1227.	1225.	1223.	1237.
Reference	Sonboli, Salehi, et al., 2005	Srivastava, Srivastava, et al., 2005	Tepe B., Sokmen M., et al., 2005	Tzakou and Constantinidis, 2005	Aghel, Yamini, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	BP-1	DB-5	RTX-1	DB-1
Column length (m)	30.	50.	60.	30.	60.
Carrier gas	N2		He	N2	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	40.	60.	35.
T_end (C)	200.	220.	280.	300.	230.
Heat rate (K/min)	5.	2.	4.	4.	2.
Initial hold (min)			4.		4.
Final hold (min)		20.			25.
I	1231.	1215.	1193.	1218.	1208.
Reference	Agnaniet, Menut, et al., 2004	Blanc, Muselli, et al., 2004	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004	Park, Lee, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	NB-30	DB-1
Column length (m)	60.	60.	60.	50.	60.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	35.	35.	50.	70.
T_end (C)	230.	230.	230.	250.	230.
Heat rate (K/min)	2.	2.	2.	2.	2.
Initial hold (min)	4.	4.	4.		2.
Final hold (min)	25.	25.	25.		20.
I	1209.	1209.	1213.	1220.	1222.
Reference	Park, Lee, et al., 2004	Park, Lee, et al., 2004	Park, Lee, et al., 2004	Raal, Arak, et al., 2004	Sawamura, Son, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	HP-5	DB-5
Column length (m)	60.	30.	25.	25.	30.
Carrier gas	Nitrogen		N2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.5	0.52	0.25
T_start (C)	70.	50.	30.	40.	60.
T_end (C)	230.	250.	280.	240.	240.
Heat rate (K/min)	2.	3.	3.	4.	3.
Initial hold (min)	2.	5.
Final hold (min)
I	1222.	1200.	1250.	1242.	1240.
Reference	Sawamura, Sou, et al., 2004	Sefidkon, Jamzad, et al., 2004	Shafi, Nambiar, et al., 2004	Simic, Sokovic, et al., 2004	Tellez, Khan, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BPX-5	DB-5	DB-1	HP-5MS
Column length (m)	30.	25.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	1.	0.25	0.25	0.25
T_start (C)	60.	60.	60.	70.	60.
T_end (C)	240.	250.	240.	230.	280.
Heat rate (K/min)	3.	3.	4.	2.	3.
Initial hold (min)		5.		2.
Final hold (min)		10.		20.
I	1193.	1276.	1242.	1220.	1239.
Reference	Tellez, Khan, et al., 2004	Vilaseca, Guy, et al., 2004	Cabanillas, Lopez, et al., 2003	Choi, 2003	Couladis, Özcan, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	RSL-200	RSL-200	CP Sil 5 CB
Column length (m)	60.	60.	30.	30.	25.
Carrier gas	He	He	H2	H2	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32	0.25
Phase thickness (μm)			0.25	0.25	0.39
T_start (C)	50.	50.	40.	40.	60.
T_end (C)	220.	220.	280.	280.	220.
Heat rate (K/min)	3.	3.	6.	6.	5.
Initial hold (min)			2.	5.
Final hold (min)			10.	5.
I	1262.	1208.	1195.	1228.	1218.
Reference	Edris, Shalaby, et al., 2003	Edris, Shalaby, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2	Khanavi, Hadjiakhoondi, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	OV-101	DB-5	HP-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	Helium	Helium	He	H2	He
Substrate
Column diameter (mm)	0.32	0.32	0.2	0.25	0.25
Phase thickness (μm)			0.5	0.25	0.25
T_start (C)	70.	70.	50.	60.	60.
T_end (C)	210.	210.	250.	280.	280.
Heat rate (K/min)	2.	2.	2.	4.	3.
Initial hold (min)				10.
Final hold (min)	60.	60.		40.
I	1241.	1197.	1215.	1243.	1229.
Reference	Mookdasanit, Tamura, et al., 2003	Mookdasanit, Tamura, et al., 2003	Orav, Kailas, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	HP-5	DB-1	HP-5	HP-5
Column length (m)	50.	60.	60.	25.	25.
Carrier gas	He		N2	Helium	Helium
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.5	0.25	0.25	0.53	0.53
T_start (C)	50.	40.	70.	40.	40.
T_end (C)	250.	250.	230.	280.	280.
Heat rate (K/min)	2.	5.	2.	4.	4.
Initial hold (min)		15.	2.
Final hold (min)			20.
I	1220.	1245.	1236.	1241.	1242.
Reference	Raal, Arak, et al., 2003	Stashenko, Jaramillo, et al., 2003	Tu, Onishi, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DB-5	HP-5	HP-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	Helium	He	N2	N2	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.53	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	50.	60.
T_end (C)	280.	240.	250.	250.	275.
Heat rate (K/min)	4.	3.	4.	4.	4.
Initial hold (min)				5.
Final hold (min)
I	1243.	1243.	1242.	1243.	1240.
Reference	Velickovic, Ristic, et al., 2003	Zoghbi, Andrade, et al., 2003	Farah, Fechtal, et al., 2002	Farah, Fechtal. M., et al., 2002	Ghannadi, Sajjadi, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RSL-200	SPB-5	HP-5	DB-5
Column length (m)	30.	30.	60.	30.	25.
Carrier gas	H2	H2	He		N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.23
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.15
T_start (C)	40.	40.	50.	60.	50.
T_end (C)	280.	280.	240.	275.	250.
Heat rate (K/min)	6.	6.	5.	4.	3.
Initial hold (min)	5.	2.	3.	4.
Final hold (min)	5.	10.	10.
I	1231.	1231.	1256.	1237.	1233.
Reference	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Smith, et al., 2002	Kim and Lee, 2002	Lockwood, Asghari, et al., 2002	Mahmout, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	CP Sil 5 CB	HP-5	HP-5	HP-1
Column length (m)	30.	25.	30.	30.	50.
Carrier gas	He	He			N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	90.
T_end (C)	240.	220.	240.	240.	220.
Heat rate (K/min)	3.	5.	3.	3.	3.
Initial hold (min)
Final hold (min)
I	1243.	1218.	1253.	1202.	1229.
Reference	Maia, Zoghbi, et al., 2002	Monfared, Davarani, et al., 2002	Novak, Langbehn, et al., 2002	Novak, Langbehn, et al., 2002	Priestap, van Baren, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SE-54	HP-5	HP-5	RSL-200
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	H2	N2	N2	H2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	40.
T_end (C)	280.	240.	220.	220.	280.
Heat rate (K/min)	4.	5.	5.	5.	6.
Initial hold (min)	5.		10.	10.	5.
Final hold (min)					5.
I	1212.	1242.	1245.	1195.	1227.
Reference	Sefidkon, Jalili, et al., 2002	Silva A.D., Patitucci M.L., et al., 2002	Gallori, Flamini, et al., 2001	Gallori, Flamini, et al., 2001	Jirovetz L., Buchbauer G., et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5MS	OV-101	OV-101	SPB-1
Column length (m)	30.	30.	50.	50.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.2	0.32
Phase thickness (μm)	0.25	0.25	0.5		0.25
T_start (C)	60.	60.	50.	50.	50.
T_end (C)	300.	240.	250.	250.	250.
Heat rate (K/min)	4.	3.	2.	2.	2.
Initial hold (min)
Final hold (min)		30.
I	1219.	1217.	1215.	1215.	1187.
Reference	Kalemba, Marschall, et al., 2001	Marongiu, Porcedda, et al., 2001	Orav, Kailas, et al., 2001	Orav and Kann, 2001	Vijayanand, Rao, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	RSL-200	BP-1	HP-5
Column length (m)	50.	50.	60.	25.	30.
Carrier gas	N2	N2	H2	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.33	0.25
Phase thickness (μm)			0.25	1.0	0.25
T_start (C)	80.	80.	40.	60.	60.
T_end (C)	200.	200.	250.	275.	275.
Heat rate (K/min)	2.	2.	6.	4.	4.
Initial hold (min)
Final hold (min)
I	1220.	1220.	1227.	1195.	1195.
Reference	Yang, 2001	Yang, 2001, 2	Jirovetz, Puschmann, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SPB-5	OV-1	HP-1	HP-1
Column length (m)	30.	50.	50.	25.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.1
T_start (C)	60.	60.	50.	35.	50.
T_end (C)	240.	240.	250.	250.	300.
Heat rate (K/min)	3.	3.	10.	4.	5.
Initial hold (min)			5.		2.
Final hold (min)		20.	20.		3.
I	1243.	1245.	1224.	1208.	1228.
Reference	Tellez, Canel, et al., 1999	Doneanu and Anitescu, 1998	Kökdil, Kurucu, et al., 1998	Ong, Acree, et al., 1998	Boatright and Crum, 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	DB-1	HP-5
Column length (m)		30.	30.	60.
Carrier gas		Helium		He
Substrate
Column diameter (mm)		0.25	0.25	0.32
Phase thickness (μm)		0.25	0.25	0.50
T_start (C)	80.	60.	60.	50.	40.
T_end (C)	220.	240.	300.	250.	210.
Heat rate (K/min)	6.	3.	4.	8.	2.
Initial hold (min)			2.	1.
Final hold (min)			5.	6.
I	1206.	1242.	1239.4	1229.	1242.
Reference	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Gawdzik, Mardarowicz, et al., 1996	Sagrero-Nieves and Bartley, 1996	Collin, Deslauriers, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	Methyl Silicone	Methyl Silicone
Column length (m)				50.	50.
Carrier gas				N2	N2
Substrate
Column diameter (mm)				0.25	0.25
Phase thickness (μm)				0.17	0.17
T_start (C)	40.	40.	40.	80.	80.
T_end (C)	210.	210.	210.	200.	200.
Heat rate (K/min)	2.	2.	2.	2.	3.
Initial hold (min)
Final hold (min)
I	1243.	1191.	1192.	1228.	1224.
Reference	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-101	SE-54	RSL-150
Column length (m)	50.	50.	54.	30.	30.
Carrier gas			He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.26	0.25	0.32
Phase thickness (μm)				0.25	0.20
T_start (C)	80.	80.	50.	60.	30.
T_end (C)	200.	200.	230.	250.	200.
Heat rate (K/min)	2.	2.	3.	2.	3.
Initial hold (min)				5.
Final hold (min)				2.
I	1220.	1224.	1220.	1239.	1216.
Reference	Tamura, Yang, et al., 1993	Tamura, Yang, et al., 1993	Zenkevich and Kulikova, 1993	Kollmannsberger, Nitz, et al., 1992	Ronse and De Pooter, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-101	OV-101	OV-101
Column length (m)	50.	50.	50.	50.	50.
Carrier gas	N2	N2	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)
T_start (C)	80.	80.	80.	80.	80.
T_end (C)	200.	200.	200.	200.	200.
Heat rate (K/min)	2.	2.	2.	2.	2.
Initial hold (min)
Final hold (min)
I	1220.	1224.	1220.	1218.	1224.
Reference	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990	Sugisawa, Yamamoto, et al., 1989	Sugisawa, Yang, et al., 1989	Sugisawa, Yang, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary
Active phase	BP-1
Column length (m)	25.
Carrier gas	Hydrogen
Substrate
Column diameter (mm)	0.20
Phase thickness (μm)
T_start (C)	70.
T_end (C)	180.
Heat rate (K/min)	3.
Initial hold (min)	5.
Final hold (min)
I	1228.
Reference	MacLeod, MacLeod, et al., 1988
Comment	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Kalemba, Marschall, et al., 2001
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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