1-(5'-Chloro-2'-methylaminobenzoyl)-cyclohex-1-ene
- Formula: C14H16ClNO
- Molecular weight: 249.736
- IUPAC Standard InChI: InChI=1S/C14H16ClNO/c1-16-13-8-7-11(15)9-12(13)14(17)10-5-3-2-4-6-10/h5,7-9,16H,2-4,6H2,1H3
- IUPAC Standard InChIKey: CZSVMGRCLAQSME-UHFFFAOYSA-N
- CAS Registry Number: 97994-57-5
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 1-Cyclohexenyl 5-chloro-2-methylaminophenyl ketone; Tetrazepam, isomer 1, hydrolysis; Tetrazepam, isomer 2, hydrolysis
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | DB-1 | 250. | 2189. | Japp, Garthwaite, et al., 1988 | 30. m/0.53 mm/1.5 μm, N2 |
| Capillary | DB-1 | 250. | 2232. | Japp, Garthwaite, et al., 1988 | 30. m/0.53 mm/1.5 μm, N2 |
| Capillary | BP-1 | 250. | 2203. | Japp, Garthwaite, et al., 1988 | 25. m/0.22 mm/0.25 μm, N2 |
| Capillary | BP-1 | 250. | 2247. | Japp, Garthwaite, et al., 1988 | 25. m/0.22 mm/0.25 μm, N2 |
Kovats' RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Cross-Linked Methylsilicone | 2220. | Maurer and Pfleger, 1987 | 12. m/0.2 mm/0.33 μm, He, 100. C @ 3. min, 30. K/min, 310. C @ 5. min |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Japp, Garthwaite, et al., 1988
Japp, M.; Garthwaite, K.; Geeson, A.V.; Osselton, M.D.,
Collection of Analytical Data for Benzodiazepines and Benzophenones,
J. Chromatogr., 1988, 439, 2, 317-339, https://doi.org/10.1016/S0021-9673(01)83844-9
. [all data]
Maurer and Pfleger, 1987
Maurer, H.; Pfleger, K.,
Identification and differentiation of benzodiazepines and their metabolites in urine by computerized gas chromatography-mass spectrometry,
J. Chromatogr., 1987, 422, 85-101, https://doi.org/10.1016/0378-4347(87)80442-5
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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