1-(5'-Chloro-2'-methylaminobenzoyl)-cyclohex-1-ene


Gas Chromatography

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

View large format table.

Column type Active phase Temperature (C) I Reference Comment
CapillaryDB-1250.2189.Japp, Garthwaite, et al., 198830. m/0.53 mm/1.5 μm, N2
CapillaryDB-1250.2232.Japp, Garthwaite, et al., 198830. m/0.53 mm/1.5 μm, N2
CapillaryBP-1250.2203.Japp, Garthwaite, et al., 198825. m/0.22 mm/0.25 μm, N2
CapillaryBP-1250.2247.Japp, Garthwaite, et al., 198825. m/0.22 mm/0.25 μm, N2

Kovats' RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryCross-Linked Methylsilicone2220.Maurer and Pfleger, 198712. m/0.2 mm/0.33 μm, He, 100. C @ 3. min, 30. K/min, 310. C @ 5. min

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Japp, Garthwaite, et al., 1988
Japp, M.; Garthwaite, K.; Geeson, A.V.; Osselton, M.D., Collection of Analytical Data for Benzodiazepines and Benzophenones, J. Chromatogr., 1988, 439, 2, 317-339, https://doi.org/10.1016/S0021-9673(01)83844-9 . [all data]

Maurer and Pfleger, 1987
Maurer, H.; Pfleger, K., Identification and differentiation of benzodiazepines and their metabolites in urine by computerized gas chromatography-mass spectrometry, J. Chromatogr., 1987, 422, 85-101, https://doi.org/10.1016/0378-4347(87)80442-5 . [all data]


Notes

Go To: Top, Gas Chromatography, References