1-Octacosanol, TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-53148.García, Sáenz, et al., 199725. m/0.25 mm/0.23 μm, He, 230. C @ 6. min, 4. K/min; Tend: 300. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryVF-5MS3136.3Zheng and White, 200830. m/0.25 mm/0.25 μm, He; Program: not specified

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-5 Sil MS3139.Lytovchenko, Beleggia, et al., 200930. m/0.25 mm/0.25 μm, Helium, 70. C @ 5. min, 5. K/min, 310. C @ 1. min
CapillarySE-303154.Fels, Dehennin, et al., 197520. m/0.25 mm/0.33 μm, 1.3 K/min; Tstart: 200. C; Tend: 250. C
CapillarySE-303155.Fels, Dehennin, et al., 197520. m/0.25 mm/0.33 μm, 200. C @ 10. min, 2.2 K/min; Tend: 250. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

García, Sáenz, et al., 1997
García, M.D.; Sáenz, M.T.; Ahumada, M.D.; Cert, A., Isolation of three triterpenes and several aliphatic alcohols from Crataegus monogyna Jacq., J. Chromatogr. A, 1997, 767, 1-2, 340-342, https://doi.org/10.1016/S0021-9673(96)01091-6 . [all data]

Zheng and White, 2008
Zheng, Y.; White, E., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2008. [all data]

Lytovchenko, Beleggia, et al., 2009
Lytovchenko, A.; Beleggia, R.; Schauer, N.; Isaacson, T.; Leuendorf, J.E.; Hellmann, H.; Rose, J.K.C.; Fernie, A.R., Application of GC-MS fpr the detection of lipophilic compounds in diverse plant tissues, Plant Methods, 2009, 5, 4, 1-11. [all data]

Fels, Dehennin, et al., 1975
Fels, J.P.; Dehennin, L.; Scholler, R., Determination of estrogenes by gas-liquid chromatography with an open tubular column, J. Steroid Biochem., 1975, 6, 7, 1201-1203, https://doi.org/10.1016/0022-4731(75)90103-X . [all data]


Notes

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