3-Hexen-1-ol, (Z)-
- Formula: C6H12O
- Molecular weight: 100.1589
- IUPAC Standard InChI: InChI=1S/C6H12O/c1-2-3-4-5-6-7/h3-4,7H,2,5-6H2,1H3/b4-3-
- IUPAC Standard InChIKey: UFLHIIWVXFIJGU-ARJAWSKDSA-N
- CAS Registry Number: 928-96-1
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Species with the same structure:
- Isotopologues:
- Stereoisomers:
- Other names: (Z)-Hex-3-en-1-ol; cis-3-Hexen-1-ol; cis-3-Hexene-1-ol; cis-3-Hexenol; Blatteralkohol (German); Leaf alcohol; Z-3-Hexenol; 3-(Z)-Hexenol; Blatteralkohol; 3-Hexen-1-ol, cis-; 3-Hexenol, cis-; 3-(Z)-Hexen-1-ol; c-3-Hexen-1-ol; cis-Hex-3-en-1ol; cis-Hex-3-enol; Hex-3( Z)-en-1-ol; Hex-3(Z)-enol; (Z)-Hex-3-ene-1-ol; (Z)Hex-3-enol; (Z)-3-Hexen-1-ol; 3-Hexen-1-ol, (3Z)-; β,γ-Hexenol; HEXEN-30L-1; 3-Hexen-1-ol; (3Z)-3-Hexen-1-ol; cis-3-1-Hexenol
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Normal alkane RI, polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-FFAP | DB-Wax | BP-20 | TC-Wax | CP Wax 52 CB |
| Column length (m) | 30. | 30. | 60. | 30. | |
| Carrier gas | Helium | Helium | Nitrogen | Helium | Helium |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.32 | |
| Phase thickness (μm) | 0.25 | 0.25 | 0.50 | ||
| Tstart (C) | 50. | 40. | 60. | 40. | 40. |
| Tend (C) | 250. | 210. | 200. | 230. | 230. |
| Heat rate (K/min) | 4. | 3. | 5. | 3. | 4. |
| Initial hold (min) | 4. | 3. | 2. | ||
| Final hold (min) | 5. | 15. | |||
| I | 1389. | 1378. | 1370. | 1393. | 1386. |
| Reference | Osorio, Carriazo, et al., 2011 | Kumazawa, Sakai, et al., 2010 | Mishra, Chaudhary, et al., 2010 | Miyazawa, Fujita, et al., 2010 | Birtic, Ginies, et al., 2009 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | HP-Innowax | DB-Wax | HP-20M | HP-20M |
| Column length (m) | 30. | 30. | 30. | 50. | 50. |
| Carrier gas | Hydrogen | Nitrogen | Helium | Helium | Helium |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.52 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 30. | 35. | 40. | 70. | 70. |
| Tend (C) | 230. | 205. | 230. | 180. | 180. |
| Heat rate (K/min) | 8. | 3. | 3. | 4. | 4. |
| Initial hold (min) | 5. | 10. | 2. | 4. | 4. |
| Final hold (min) | 10. | 10. | 5. | ||
| I | 1379. | 1370. | 1386. | 1347. | 1350. |
| Reference | Karlsson, Birgersson, et al., 2009 | Wannes, Mhamdi, et al., 2009 | Zhao, Xu, et al., 2009 | Blazevic and Mastelic, 2008 | Blazevic and Mastelic, 2008 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-20M | DB-Wax | RTX-Wax | HP-Innowax | DB-Wax |
| Column length (m) | 50. | 30. | 60. | 50. | 30. |
| Carrier gas | Helium | He | He | Helium | He |
| Substrate | |||||
| Column diameter (mm) | 0.20 | 0.25 | 0.22 | 0.20 | 0.32 |
| Phase thickness (μm) | 0.20 | 0.25 | 0.25 | 0.20 | 0.5 |
| Tstart (C) | 60. | 30. | 60. | 45. | 40. |
| Tend (C) | 220. | 210. | 230. | 190. | 240. |
| Heat rate (K/min) | 2. | 5. | 2. | 4. | 5. |
| Initial hold (min) | 2. | ||||
| Final hold (min) | 20. | 35. | 50. | ||
| I | 1346. | 1385. | 1377. | 1388. | 1395. |
| Reference | Breme, Langle, et al., 2008 | Kumazawa, Itobe, et al., 2008 | Paolini, Tomi, et al., 2008 | Soria, Sanz, et al., 2008 | Dury-Brun, Fournier, et al., 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-20M | TC-FFAP | CP-Wax 52CB | BP-20 | BP-20 |
| Column length (m) | 50. | 60. | 30. | 30. | |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.2 | 0.25 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.2 | 0.25 | 0.5 | 0.25 | 0.25 |
| Tstart (C) | 70. | 60. | 40. | 70. | 70. |
| Tend (C) | 180. | 220. | 220. | 220. | 220. |
| Heat rate (K/min) | 4. | 3. | 4. | 4. | 4. |
| Initial hold (min) | 4. | 8. | 4. | 4. | |
| Final hold (min) | 30. | 20. | 5. | 5. | |
| I | 1350. | 1394. | 1387. | 1393. | 1393. |
| Reference | Jerkovic, Mastelic, et al., 2007 | Kurose, Okamura, et al., 2007 | Povolo, Contarini, et al., 2007 | Rawat, Gulati, et al., 2007 | Rawat, Gulati, et al., 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | TR-WAX | DB-Wax | DB-Wax | BP-20 | DB-Wax |
| Column length (m) | 60. | 30. | 30. | 50. | 60. |
| Carrier gas | H2 | He | Helium | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.22 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.5 |
| Tstart (C) | 40. | 40. | 40. | 60. | 50. |
| Tend (C) | 200. | 230. | 250. | 220. | 230. |
| Heat rate (K/min) | 3. | 4. | 3. | 2. | 3. |
| Initial hold (min) | 10. | 2. | 2. | ||
| Final hold (min) | 10. | 5. | 20. | 20. | 20. |
| I | 1385. | 1372. | 1351. | 1381. | 1381. |
| Reference | Tena N., Lazzez A., et al., 2007 | Xu, Fan, et al., 2007 | Berlinet, Brat, et al., 2006 | Boti, Yao, et al., 2006 | Cai, Lin, et al., 2006 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-20M | DB-Wax Etr | DB-Wax | HP-Innowax | TR-WAX |
| Column length (m) | 50. | 60. | 15. | 30. | 60. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.2 | 0.25 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.1 | 0.25 | 0.25 | 0.5 | 0.25 |
| Tstart (C) | 60. | 40. | 40. | 40. | 40. |
| Tend (C) | 220. | 230. | 230. | 200. | 200. |
| Heat rate (K/min) | 2. | 2. | 6. | 2. | 3. |
| Initial hold (min) | 5. | 3. | 10. | ||
| Final hold (min) | 30. | 100. | 20. | 15. | |
| I | 1347. | 1390. | 1383. | 1367. | 1396. |
| Reference | Filippi, Lanfranchi, et al., 2006 | Ibarz, Ferreira, et al., 2006 | Kishimoto, Wanikawa, et al., 2006 | Komes, Ulrich, et al., 2006 | Salas J.J., Garcia-Gonzalez D.L., et al., 2006 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-Innowax | Supelcowax-10 | Carbowax 20M | Carbowax 20M | Supelcowax |
| Column length (m) | 60. | 30. | 60. | 50. | 60. |
| Carrier gas | He | He | N2 | Helium | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.2 |
| Phase thickness (μm) | 0.5 | 0.25 | 0.25 | 0.25 | 0.2 |
| Tstart (C) | 60. | 50. | 40. | 40. | 60. |
| Tend (C) | 220. | 220. | 190. | 190. | 230. |
| Heat rate (K/min) | 2. | 4. | 10. | 4. | 4. |
| Initial hold (min) | 1. | 2. | 2. | 30. | |
| Final hold (min) | 10. | 10. | 15. | 30. | |
| I | 1388. | 1386. | 1351. | 1388. | 1345. |
| Reference | Senger-Emonnot, Rochard, et al., 2006 | Wong, Lim, et al., 2006 | Babu and Kaul, 2005 | de la Fuente, Martinez-Castro, et al., 2005 | Gauvin and Smadja, 2005 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Innowax | DB-Wax | DB-Wax | TR-WAX | PEG-20M |
| Column length (m) | 60. | 30. | 60. | 60. | 30. |
| Carrier gas | He | He | Nitrogen | H2 | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.50 | 0.25 | |
| Tstart (C) | 60. | 50. | 35. | 40. | 60. |
| Tend (C) | 240. | 180. | 235. | 200. | 180. |
| Heat rate (K/min) | 5. | 3. | 2. | 3. | 3. |
| Initial hold (min) | 4. | 10. | 10. | ||
| Final hold (min) | 30. | 40. | 30. | 30. | |
| I | 1393. | 1381. | 1410. | 1396. | 1386. |
| Reference | Joichi, Yomogida, et al., 2005 | Lee, Umano, et al., 2005 | Qian and Wang, 2005 | Salas, Sánchez, et al., 2005 | Yao, Guo, et al., 2005 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | DB-Wax | DB-Wax | DB-Wax |
| Column length (m) | 60. | 60. | 30. | 60. | 60. |
| Carrier gas | N2 | H2 | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.5 | 0.25 | 0.5 | ||
| Tstart (C) | 35. | 70. | 40. | 60. | 60. |
| Tend (C) | 240. | 230. | 200. | 220. | 220. |
| Heat rate (K/min) | 4. | 2. | 4. | 2. | 2. |
| Initial hold (min) | 5. | 2. | 5. | 4. | 4. |
| Final hold (min) | 10. | 20. | |||
| I | 1418. | 1368. | 1407. | 1385. | 1385. |
| Reference | Chida, Sone, et al., 2004 | Choi, 2004 | Culleré, Escudero, et al., 2004 | Jiang and Kubota, 2004 | Jiang and Kubota, 2004 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | PEG-20M | DB-Wax | HP-Innowax | DB-Wax |
| Column length (m) | 60. | 50. | 60. | 50. | 30. |
| Carrier gas | He | He | He | H2 | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.20 | 0.32 | 0.2 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.20 | 0.25 | 0.2 | 0.5 |
| Tstart (C) | 40. | 40. | 35. | 45. | 50. |
| Tend (C) | 220. | 180. | 220. | 190. | 200. |
| Heat rate (K/min) | 3. | 3. | 3. | 4. | 3. |
| Initial hold (min) | 5. | 5. | 2. | 10. | |
| Final hold (min) | 30. | 50. | 10. | ||
| I | 1382. | 1381. | 1388. | 1391. | 1391. |
| Reference | López, Ezpeleta, et al., 2004 | Narain, Almeida, et al., 2004 | Palá-Paúl, Brophy, et al., 2004 | Soria, Gonzalez, et al., 2004 | Alves and Franco, 2003 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | TC-Wax | Supelcowax-10 | Supelcowax-10 |
| Column length (m) | 60. | 30. | 60. | 30. | 30. |
| Carrier gas | H2 | H2 | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.5 | 0.25 | 0.25 | |
| Tstart (C) | 40. | 40. | 80. | 40. | 40. |
| Tend (C) | 230. | 200. | 240. | 200. | 200. |
| Heat rate (K/min) | 4. | 4. | 3. | 3. | 3. |
| Initial hold (min) | 5. | 5. | 10. | 10. | |
| Final hold (min) | 25. | ||||
| I | 1385. | 1405. | 1383. | 1385. | 1380. |
| Reference | Dregus and Engel, 2003 | López, Ortín, et al., 2003 | Miyazawa, Teranishi, et al., 2003 | Vichi, Castellote, et al., 2003 | Vichi, Pizzale, et al., 2003 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Supelcowax-10 | BP-20 | DB-Wax | DB-Wax | DB-Wax |
| Column length (m) | 30. | 50. | 60. | 60. | 30. |
| Carrier gas | He | H2 | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 40. | 45. | 40. | 60. | 40. |
| Tend (C) | 200. | 230. | 220. | 180. | 210. |
| Heat rate (K/min) | 3. | 3. | 3. | 3. | 5. |
| Initial hold (min) | 10. | 1. | 10. | 4. | |
| Final hold (min) | 10. | 10. | |||
| I | 1378. | 1356. | 1384. | 1390. | 1387. |
| Reference | Vichi, Pizzale, et al., 2003, 2 | Darriet, Pons, et al., 2002 | Hayata, Sakamoto, et al., 2002 | Ito, Sugimoto, et al., 2002 | Kumazawa and Masuda, 2002 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | TC-WAX FFS | TC-Wax | DB-Wax | DB-Wax |
| Column length (m) | 60. | 60. | 60. | 60. | 30. |
| Carrier gas | He | He | He | He | H2 |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.5 | |
| Tstart (C) | 40. | 60. | 40. | 40. | 40. |
| Tend (C) | 210. | 240. | 230. | 200. | 200. |
| Heat rate (K/min) | 5. | 3. | 3. | 2. | 4. |
| Initial hold (min) | 10. | 2. | 5. | ||
| Final hold (min) | 10. | 60. | |||
| I | 1387. | 1378. | 1371. | 1376. | 1401. |
| Reference | Kumazawa and Masuda, 2002 | Miyazawa, Maehara, et al., 2002 | Suhardi, Suzuki, et al., 2002 | Umano, Hagi, et al., 2002 | Aznar, López, et al., 2001 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | DB-Wax | DB-Wax | Carbowax 20M |
| Column length (m) | 30. | 60. | 60. | 30. | 50. |
| Carrier gas | H2 | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.22 |
| Phase thickness (μm) | 0.5 | 0.1 | 0.25 | ||
| Tstart (C) | 40. | 60. | 40. | 40. | 60. |
| Tend (C) | 200. | 220. | 220. | 180. | 220. |
| Heat rate (K/min) | 4. | 2. | 2. | 2. | 2. |
| Initial hold (min) | 5. | 4. | 5. | ||
| Final hold (min) | 60. | 20. | |||
| I | 1401. | 1411. | 1418. | 1385. | 1350. |
| Reference | Ferreira, Aznar, et al., 2001 | Jiang, Kojima, et al., 2001 | Jiang and Kubota, 2001 | Kato and Shibamoto, 2001 | Vernin, Lageot, et al., 2001 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | CP-Wax 52CB | DB-Wax | Supelcowax-10 |
| Column length (m) | 30. | 60. | 50. | 30. | 30. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.30 | 0.32 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 50. | 30. | 40. | 50. | 70. |
| Tend (C) | 220. | 170. | 220. | 210. | 240. |
| Heat rate (K/min) | 4. | 2. | 3. | 2. | 5. |
| Initial hold (min) | 3. | 4. | 5. | 2. | 8. |
| Final hold (min) | 30. | 20. | |||
| I | 1389. | 1380. | 1351. | 1425. | 1376. |
| Reference | Weckerle, Bastl-Borrmann, et al., 2001 | Buttery, Light, et al., 2000 | Chagonda, Makanda, et al., 2000 | Ebeler, Terrien, et al., 2000 | Kim, Kim, et al., 2000 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Supelcowax-10 | DB-Wax | DB-Wax | DB-Wax | DB-Wax |
| Column length (m) | 60. | 30. | 30. | 30. | 25. |
| Carrier gas | He | H2 | H2 | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.5 | 0.5 | 0.25 | 0.25 |
| Tstart (C) | 60. | 60. | 60. | 50. | 50. |
| Tend (C) | 280. | 245. | 245. | 180. | 200. |
| Heat rate (K/min) | 4. | 3. | 3. | 3. | 4. |
| Initial hold (min) | 3. | 3. | 4. | ||
| Final hold (min) | 20. | 20. | 40. | 10. | |
| I | 1355. | 1400. | 1400. | 1358. | 1370. |
| Reference | Korány, Mednyánszky, et al., 2000 | Kotseridis and Baumes, 2000 | Kotseridis and Baumes, 2000 | Lee and Shibamoto, 2000 | Morales, Duque, et al., 2000 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | DB-Wax | DB-Wax | DB-Wax |
| Column length (m) | 25. | 25. | 25. | 30. | 30. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 50. | 50. | 50. | 50. | 50. |
| Tend (C) | 200. | 200. | 200. | 240. | 240. |
| Heat rate (K/min) | 4. | 4. | 4. | 4. | 4. |
| Initial hold (min) | 4. | 4. | 4. | 3. | 3. |
| Final hold (min) | 10. | 10. | 10. | 10. | 10. |
| I | 1371. | 1377. | 1377. | 1376. | 1377. |
| Reference | Morales, Duque, et al., 2000 | Morales, Duque, et al., 2000 | Morales, Duque, et al., 2000 | Parada, Duque, et al., 2000 | Parada, Duque, et al., 2000 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | Carbowax 20M | DB-Wax | DB-Wax | Supelcowax-10 |
| Column length (m) | 60. | 60. | 60. | 60. | 60. |
| Carrier gas | He | He | He | He | H2 |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.5 | 0.25 | 0.25 | 0.5 |
| Tstart (C) | 40. | 40. | 60. | 40. | 35. |
| Tend (C) | 200. | 190. | 240. | 200. | 250. |
| Heat rate (K/min) | 2. | 2. | 4. | 2. | 5. |
| Initial hold (min) | 2. | 5. | 2. | 5. | |
| Final hold (min) | 20. | ||||
| I | 1386. | 1389. | 1379. | 1386. | 1404. |
| Reference | Umano, Hagi, et al., 2000 | Lopez, Ferreira, et al., 1999 | Ngassoum, Yonkeu, et al., 1999 | Umano, Nakahara, et al., 1999 | Campeanu, Burcea, et al., 1998 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Carbowax 20M | Carbowax 20M | Supelcowax-10 | DB-Wax | DB-Wax |
| Column length (m) | 60. | 60. | 30. | 30. | 30. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.5 | 0.5 | 0.25 | 0.25 | |
| Tstart (C) | 40. | 40. | 60. | 50. | 50. |
| Tend (C) | 190. | 190. | 240. | 240. | 240. |
| Heat rate (K/min) | 2. | 2. | 4. | 4. | 4. |
| Initial hold (min) | 5. | 5. | 3. | 3. | |
| Final hold (min) | 10. | 10. | |||
| I | 1389. | 1389. | 1390. | 1376. | 1378. |
| Reference | Ferreira, Ardanuy, et al., 1998 | Ferreira, Lopez, et al., 1998 | Lamarque, Maestri, et al., 1998 | Parada and Duque, 1998 | Parada and Duque, 1998 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | CBP-20 | DB-Wax | HP-Innowax | DB-Wax | DB-Wax |
| Column length (m) | 25. | 60. | 60. | 60. | 30. |
| Carrier gas | H2 | He | He | ||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.5 | 0.25 | ||
| Tstart (C) | 35. | 50. | 50. | 50. | 20. |
| Tend (C) | 200. | 230. | 180. | 200. | 200. |
| Heat rate (K/min) | 5. | 2. | 1.5 | 3. | 4. |
| Initial hold (min) | 5. | 4. | |||
| Final hold (min) | 40. | 10. | |||
| I | 1371. | 1385. | 1398. | 1393. | 1342. |
| Reference | Quiroz A. and Niemeyer H.M., 1998 | Ravichandran and Parthiban, 1998 | Ulrich, Hoberg, et al., 1997 | Wada and Shibamoto, 1997 | Morales, Albarracín, et al., 1996 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | PEG-20M | TC-Wax | Supelcowax-10 | Supelcowax-10 |
| Column length (m) | 30. | 50. | 60. | 60. | 90. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
| Tstart (C) | 50. | 70. | 80. | 40. | 35. |
| Tend (C) | 200. | 250. | 240. | 200. | 220. |
| Heat rate (K/min) | 4. | 2. | 3. | 3. | 2. |
| Initial hold (min) | 4. | 5. | 3. | 20. | |
| Final hold (min) | 10. | 30. | 30. | ||
| I | 1355. | 1379. | 1383. | 1392. | 1369. |
| Reference | Morales, Albarracín, et al., 1996 | Orav, Kailas, et al., 1996 | Shuichi, Masazumi, et al., 1996 | Wong and Lai, 1996 | Girard and Lau, 1995 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Carbowax 20M | DB-Wax | DB-Wax | DB-Wax | PEG-20M |
| Column length (m) | 60. | 60. | 60. | 60. | 50. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.15 | |||
| Tstart (C) | 60. | 60. | 60. | 50. | 60. |
| Tend (C) | 180. | 180. | 180. | 180. | 180. |
| Heat rate (K/min) | 2. | 2. | 2. | 2.5 | 2. |
| Initial hold (min) | 4. | 4. | 4. | 5. | 4. |
| Final hold (min) | |||||
| I | 1361. | 1374. | 1378. | 1368. | 1361. |
| Reference | Kawakami, Ganguly, et al., 1995 | Kobayashi, Tsuda, et al., 1995 | Kobayashi, Tsuda, et al., 1995 | Stashenko, Torres, et al., 1995 | Togari, Kobayashi, et al., 1995 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | PEG-20M | Carbowax 20M | CP-Wax 52CB | Carbowax 20M | DB-Wax |
| Column length (m) | 50. | 50. | 50. | 50. | 60. |
| Carrier gas | He | He | H2 | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.15 | 0.22 | |||
| Tstart (C) | 60. | 60. | 50. | 60. | 50. |
| Tend (C) | 180. | 180. | 200. | 180. | 230. |
| Heat rate (K/min) | 2. | 2. | 2. | 2. | 4. |
| Initial hold (min) | 4. | 4. | 5. | 4. | |
| Final hold (min) | 10. | ||||
| I | 1361. | 1361. | 1392.5 | 1361. | 1378. |
| Reference | Togari, Kobayashi, et al., 1995 | Kawakami, Kobayashi, et al., 1993 | Chyau, Chen, et al., 1992 | Kawakami and Kobayashi, 1991 | Binder, Benson, et al., 1990 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | Supelcowax-10 | DB-Wax | DB-Wax |
| Column length (m) | 60. | 60. | 60. | 60. | 60. |
| Carrier gas | He | ||||
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.32 | 0.32 |
| Phase thickness (μm) | |||||
| Tstart (C) | 50. | 50. | 60. | 50. | 50. |
| Tend (C) | 230. | 230. | 220. | 230. | 250. |
| Heat rate (K/min) | 4. | 4. | 2. | 4. | 4. |
| Initial hold (min) | 1. | 0.1 | 0.1 | ||
| Final hold (min) | 10. | 10. | 10. | 5. | |
| I | 1378. | 1378. | 1402. | 1377. | 1376. |
| Reference | Binder, Turner, et al., 1990 | Binder, Turner, et al., 1990, 2 | Loughrin, Hamilton-Kemp, et al., 1990 | Binder, Flath, et al., 1989 | Binder and Flath, 1989 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | DB-Wax | DB-Wax | Supelcowax-10 |
| Column length (m) | 60. | 60. | 60. | 60. | 60. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.32 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 30. | 30. | 30. | 30. | 60. |
| Tend (C) | 180. | 180. | 180. | 180. | 220. |
| Heat rate (K/min) | 2. | 2. | 2. | 2. | 2. |
| Initial hold (min) | 4. | 4. | 4. | 4. | 1. |
| Final hold (min) | 30. | ||||
| I | 1378. | 1378. | 1382. | 1382. | 1401. |
| Reference | Takeoka and Butter, 1989 | Takeoka and Butter, 1989 | Takeoka and Butter, 1989 | Takeoka and Butter, 1989 | Andersen, Hamilton-Kemp, et al., 1988 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | Supelcowax-10 | Carbowax 20M | Carbowax 20M | Carbowax 20M |
| Column length (m) | 60. | 60. | 50. | 50. | 50. |
| Carrier gas | He | N2 | N2 | N2 | |
| Substrate | |||||
| Column diameter (mm) | 0.322 | 0.32 | 0.22 | 0.22 | 0.22 |
| Phase thickness (μm) | 0.25 | ||||
| Tstart (C) | 50. | 60. | 80. | 80. | 80. |
| Tend (C) | 230. | 220. | 200. | 200. | 200. |
| Heat rate (K/min) | 4. | 3. | 3. | 3. | 3. |
| Initial hold (min) | 1. | ||||
| Final hold (min) | |||||
| I | 1381. | 1396. | 1358. | 1360. | 1358. |
| Reference | Engel, Flath, et al., 1988 | Hamilton-Kemp, Andersen, et al., 1988 | Mihara, Tateba, et al., 1988 | Mihara, Tateba, et al., 1988 | Mihara, Tateba, et al., 1988 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Carbowax 20M | DB-Wax | DB-Wax | Carbowax 20M | Carbowax 20M |
| Column length (m) | 50. | 60. | 60. | 150. | 50. |
| Carrier gas | N2 | H2 | H2 | N2 | |
| Substrate | |||||
| Column diameter (mm) | 0.22 | 0.25 | 0.25 | 0.66 | 0.22 |
| Phase thickness (μm) | 0.25 | 0.25 | |||
| Tstart (C) | 80. | 30. | 30. | 60. | 80. |
| Tend (C) | 200. | 180. | 180. | 170. | 200. |
| Heat rate (K/min) | 3. | 2. | 2. | 1. | 3. |
| Initial hold (min) | 2. | 2. | 40. | ||
| Final hold (min) | |||||
| I | 1360. | 1385. | 1386. | 1370. | 1358. |
| Reference | Mihara, Tateba, et al., 1988 | Takeoka, Flath, et al., 1988 | Takeoka, Flath, et al., 1988 | Buttery, Ling, et al., 1987 | Mihara, Tateba, et al., 1987 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Carbowax 20M | Carbowax 20M | Carbowax 20M | Carbowax 20M | Carbowax 20M |
| Column length (m) | 50. | 50. | 50. | 50. | 150. |
| Carrier gas | N2 | N2 | N2 | He | |
| Substrate | |||||
| Column diameter (mm) | 0.22 | 0.22 | 0.22 | 0.25 | 0.66 |
| Phase thickness (μm) | |||||
| Tstart (C) | 80. | 80. | 80. | 80. | 60. |
| Tend (C) | 200. | 200. | 200. | 200. | 170. |
| Heat rate (K/min) | 3. | 3. | 3. | 2. | 1. |
| Initial hold (min) | 40. | ||||
| Final hold (min) | |||||
| I | 1360. | 1358. | 1360. | 1354. | 1370. |
| Reference | Mihara, Tateba, et al., 1987 | Mihara, Tateba, et al., 1987 | Mihara, Tateba, et al., 1987 | Shibamoto, 1987 | Buttery, Maddox, et al., 1986 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Carbowax 20M | BP-20 | Carbowax 20M | Carbowax 20M | Carbowax 20M |
| Column length (m) | 150. | 25. | 150. | 150. | 50. |
| Carrier gas | |||||
| Substrate | |||||
| Column diameter (mm) | 0.66 | 0.2 | 0.64 | 0.66 | 0.32 |
| Phase thickness (μm) | |||||
| Tstart (C) | 60. | 70. | 50. | 60. | 70. |
| Tend (C) | 170. | 180. | 170. | 170. | 180. |
| Heat rate (K/min) | 1. | 3. | 1. | 1. | 2. |
| Initial hold (min) | 40. | 5. | 40. | ||
| Final hold (min) | 30. | ||||
| I | 1370. | 1351. | 1370. | 1370. | 1365. |
| Reference | Buttery, Xu, et al., 1985 | MacLeod and Snyder, 1985 | Buttery, Kamm, et al., 1984 | Buttery and Ling, 1984 | Engel and Tressl, 1983 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary |
|---|---|---|---|
| Active phase | Carbowax 20M | Carbowax 20M | Carbowax 20M |
| Column length (m) | 150. | 150. | 150. |
| Carrier gas | |||
| Substrate | |||
| Column diameter (mm) | 0.64 | 0.64 | 0.64 |
| Phase thickness (μm) | |||
| Tstart (C) | 50. | 50. | 50. |
| Tend (C) | 170. | 170. | 170. |
| Heat rate (K/min) | 1. | 1. | 1. |
| Initial hold (min) | 30. | 30. | 30. |
| Final hold (min) | |||
| I | 1370. | 1370. | 1370. |
| Reference | Buttery, Parker, et al., 1981 | Buttery and Kamm, 1980 | Buttery, Ling, et al., 1980 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Green leaf headspace volatiles from Nicotiana tabacum lines of different trichome morphology,
J. Agric. Food Chem., 1988, 36, 2, 295-299, https://doi.org/10.1021/jf00080a014
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Engel, Flath, et al., 1988
Engel, K.-H.; Flath, R.A.; Buttery, R.G.; Mon, T.R.; Ramming, D.W.; Teranishi, R.,
Investigation of volatile constituents in nectarines. 1. Analytical and sensory characterization of aroma components in some nectarine cultivars,
J. Agric. Food Chem., 1988, 36, 3, 549-553, https://doi.org/10.1021/jf00081a036
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Hamilton-Kemp, Andersen, et al., 1988
Hamilton-Kemp, T.R.; Andersen, R.A.; Rodriguez, J.G.; Loughrin, J.H.; Patterson, C.G.,
Strawberry foliage headspace vapor components at periods of susceptability and resistance to Tetranychus urticae Koch,
J. Chem. Ecol., 1988, 14, 3, 789-796, https://doi.org/10.1007/BF01018773
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Mihara, Tateba, et al., 1988
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The volatile components of Chinese quince (Pseudocydonia sinensis Schneid)
in Flavors and Fragrances: A World Perspective. Proceedings of the 10th International Congress of Essential Oils, Fragrances and Flavors, Lawrence,B.M.; Mookherjee,B.D.; Willis,B.J., ed(s)., Elsevier, New York, 1988, 537-550. [all data]
Takeoka, Flath, et al., 1988
Takeoka, G.R.; Flath, R.A.; Güntert, M.; Jennings, W.,
Nectarine volatiles: vacuum steam distillation versus headspace sampling,
J. Agric. Food Chem., 1988, 36, 3, 553-560, https://doi.org/10.1021/jf00081a037
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Buttery, Ling, et al., 1987
Buttery, R.G.; Ling, L.C.; Light, D.M.,
Tomato leaf volatile aroma components,
J. Agric. Food Chem., 1987, 35, 6, 1039-1042, https://doi.org/10.1021/jf00078a043
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Mihara, Tateba, et al., 1987
Mihara, S.; Tateba, H.; Nishimura, O.; Machii, Y.; Kishino, K.,
Volatile components of Chinese quince (Pseudocydonia sinensis Schneid),
J. Agric. Food Chem., 1987, 35, 4, 532-537, https://doi.org/10.1021/jf00076a023
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Shibamoto, 1987
Shibamoto, T.,
Retention Indices in Essential Oil Analysis
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Buttery, Maddox, et al., 1986
Buttery, R.G.; Maddox, D.M.; Light, D.M.; Ling, L.C.,
Volatile components of yellow starthistle,
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Buttery, Xu, et al., 1985
Buttery, R.G.; Xu, C.; Ling, L.C.,
Volatile components of wheat leaves (and stems): Possible insect attractants,
J. Agric. Food Chem., 1985, 33, 1, 115-117, https://doi.org/10.1021/jf00061a033
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MacLeod and Snyder, 1985
MacLeod, A.J.; Snyder, C.H.,
Volatile components of two cultivars of mango from Florida,
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Buttery, Kamm, et al., 1984
Buttery, R.G.; Kamm, J.A.; Ling, L.C.,
Volatile components of red clover leaves, flowers, and seed pods: possible insect attractants,
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. [all data]
Buttery and Ling, 1984
Buttery, R.G.; Ling, L.C.,
Corn leaf volatiles: identification using Tenax trapping for possible insect attractants,
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Engel and Tressl, 1983
Engel, K.-H.; Tressl, R.,
Formation of aroma components from nonvolatile precursors in passion fruit,
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. [all data]
Buttery, Parker, et al., 1981
Buttery, R.G.; Parker, F.D.; Teranishi, R.; Mon, T.R.; Ling, L.C.,
Volatile components of alfalfa leaf-cutter bee cells,
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. [all data]
Buttery and Kamm, 1980
Buttery, R.G.; Kamm, J.A.,
Volatile components of alfalfa: possible insect host plant attractants,
J. Agric. Food Chem., 1980, 28, 5, 978-981, https://doi.org/10.1021/jf60231a014
. [all data]
Buttery, Ling, et al., 1980
Buttery, R.G.; Ling, L.C.; Teranishi, R.,
Volatile of corn tassels: possible corn ear worm attractants,
J. Agric. Food Chem., 1980, 28, 4, 771-774, https://doi.org/10.1021/jf60230a020
. [all data]
Notes
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