L-Alanine, N-(tert-butyldimethylsilyl)-, tert-butyldimethylsilyl ester

• Formula: C₁₅H₃₅NO₂Si₂
• Molecular weight: 317.6149
• IUPAC Standard InChI: InChI=1S/C15H35NO2Si2/c1-12(16-19(8,9)14(2,3)4)13(17)18-20(10,11)15(5,6)7/h12,16H,1-11H3/t12-/m1/s1 Copy

  
• IUPAC Standard InChIKey: NZMBBDALTGCDPQ-GFCCVEGCSA-N Copy
• CAS Registry Number: 92751-15-0
• Chemical structure:
  This structure is also available as a 2d Mol file
• Other names: tert-Butyl(dimethyl)silyl 2-([tert-butyl(dimethyl)silyl]amino)propanoate; Alanine diTBDMS; Ala, O,N-bis-DMTBS; Ala, TBDMS; L-Alanine, 2TBDMS derivative; tert-Butyl(dimethyl)silyl 2-([tert-butyl(dimethyl)silyl]amino)propanoate, (S)-; Ala, N,O-di-TBDMS; Alanine, N,O-bis-TBDMS; Alanine, TBDMS
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• Information on this page:
  • Mass spectrum (electron ionization)
  • Gas Chromatography
  • References
  • Notes
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Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Normal alkane RI, non-polar column, temperature ramp

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References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ohie, Fu, et al., 2000
Ohie, T.; Fu, X.; Iga, M.; Kimura, M.; Yamaguchi, S., Gas chromatography-mass spectrometry with tert .-butyldimethylsilyl derivatization: use of the simplified sample preparations and the automated data system to screen for organic acidemias, J. Chromatogr. B, 2000, 746, 1, 63-73, https://doi.org/10.1016/S0378-4347(00)00105-5 . [all data]

Tret'yakov, 2007
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]

Peng, Yang, et al., 1991
Peng, C.T.; Yang, Z.C.; Maltby, D., Prediction of retention indexes. III. Silylated derivatives of polar compounds, J. Chromatogr., 1991, 586, 1, 113-129, https://doi.org/10.1016/0021-9673(91)80029-G . [all data]

Tsunoda, 1993
Tsunoda, N., Simultaneous determination of the herbicides glyphosate, glufosinate and bialaphos and their metabolites by capillary gas chromatography-ion-trap mass spectrometry, J. Chromatogr., 1993, 637, 2, 167-173, https://doi.org/10.1016/0021-9673(93)83209-B . [all data]

Notes

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• Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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