Cyclohexanone, 5-methyl-2-(1-methylethyl)-, trans-
- Formula: C10H18O
- Molecular weight: 154.2493
- IUPAC Standard InChI: InChI=1S/C10H18O/c1-7(2)9-5-4-8(3)6-10(9)11/h7-9H,4-6H2,1-3H3/t8-,9+/m0/s1
- IUPAC Standard InChIKey: NFLGAXVYCFJBMK-DTWKUNHWSA-N
- CAS Registry Number: 89-80-5
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: (2R,5S)-2-Isopropyl-5-methylcyclohexanone; p-Menthan-3-one, trans-; p-Menthone; trans-p-Menthan-3-one; trans-Menthan-3-one; Menthone; trans-Menthone; Menthon; 2-Isopropyl-5-methylcyclohexanone, trans; Menthone racemic; Cyclohexanone, 5-methyl-2-(1-methylethyl)-, trans-(.+./.-.)-; Menthan-3-one, trans; DL-Menthone; Menthone G; Neomenthone; trans-p-Menthone; trans-5-Methyl-2-(1-methylethyl)cyclohexanone
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | SE-30 | 100. | 1142.7 | Tudor, 1997 | 40. m/0.35 mm/0.35 μm |
| Capillary | OV-101 | 100. | 1130. | Baaliouamer, Boudarene, et al., 1993 | He; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 100. | 1137. | Baaliouamer, Boudarene, et al., 1993 | He; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 120. | 1138. | Baaliouamer, Boudarene, et al., 1993 | He; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 120. | 1145. | Baaliouamer, Boudarene, et al., 1993 | He; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 80. | 1122. | Baaliouamer, Boudarene, et al., 1993 | He; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 80. | 1129. | Baaliouamer, Boudarene, et al., 1993 | He; Column length: 25. m; Column diameter: 0.20 mm |
Kovats' RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5MS | 1142. | Tepe, Sokmen, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 240. C |
| Capillary | SPB-5 | 1160. | Gauvin, Lecomte, et al., 2004 | 60. m/0.32 mm/1. μm, He, 4. K/min, 200. C @ 30. min; Tstart: 60. C |
| Capillary | BP-1 | 1143. | Srivastava, Ahmad, et al., 2003 | 25. m/0.55 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C |
| Capillary | Cross-Linked Methylsilicone | 1136. | Rajeswara Rao, Kaul, et al., 2002 | 50. m/0.2 mm/0.25 μm, He, 4. K/min; Tstart: 100. C; Tend: 280. C |
| Capillary | BP-1 | 1139. | Rajeswara Rao, 2002 | 25. m/0.5 mm/0.25 μm, N2, 5. K/min, 220. C @ 10. min; Tstart: 60. C |
| Capillary | BP-1 | 1139. | Rao B.R.R., 2002 | 25. m/0.5 mm/0.25 μm, 5. K/min, 220. C @ 10. min; Tstart: 60. C |
| Capillary | BP-1 | 1139. | Rao B.R.R., 2002 | 25. m/0.5 mm/0.25 μm, 5. K/min, 220. C @ 10. min; Tstart: 60. C |
| Capillary | BP-1 | 1137. | Shawl, Srivastava, et al., 2002 | 30. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 13. min; Tstart: 60. C |
| Capillary | BP-1 | 1139. | Jain, Aggarwal, et al., 2001 | 25. m/0.55 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C |
| Capillary | HP-5 | 1154. | Kitic, Palic, et al., 2001 | 25. m/0.32 mm/0.52 μm, H2, 4. K/min; Tstart: 40. C; Tend: 240. C |
| Capillary | BP-1 | 1136. | Rao, Kaul, et al., 2000 | N2, 5. K/min, 220. C @ 10. min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 60. C |
| Capillary | BP-1 | 1136. | Rao, Sastry, et al., 2000 | 25. m/0.50 mm/0.25 μm, N2, 5. K/min, 220. C @ 10. min; Tstart: 60. C |
| Capillary | DB-5 | 1125. | Senatore and de Feo, 1999 | 30. m/0.25 mm/0.33 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min |
| Capillary | DB-5 | 1124. | de Feo, Porta, et al., 1998 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min |
| Capillary | BP-1 | 1137. | Kulkarni, Mallavarapu, et al., 1998 | N2, 5. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 220. C |
| Capillary | DB-5 | 1125. | Senatore, Urrunaga Soria, et al., 1998 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min |
| Capillary | DB-5 | 1125. | Senatore, 1998 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min |
| Capillary | DB-5 | 1124. | Senatore, Urrunaga Soria, et al., 1997 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min |
| Capillary | OV-101 | 1148. | von Poser, Menut, et al., 1996 | 25. m/0.25 mm/0.25 μm, N2, 5. K/min; Tstart: 50. C; Tend: 200. C |
| Capillary | DB-5 | 1155. | Loayza, Abujder, et al., 1995 | 40. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m |
Kovats' RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | BP-1 | 1136. | Dwivedi, Khan, et al., 2004 | 25. m/0.25 mm/0.25 μm, N2; Program: 60C => 5C/min => 220C(5min) => 3C/min => 245C(5min) |
| Capillary | HP-5 | 1154. | Shellie and Marriott, 2003 | 30. m/0.25 mm/0.25 μm, He; Program: not specified |
| Capillary | AT-5 | 1168. | Rojas and Usubillaga, 2000 | 60. m/0.25 mm/0.25 μm, He; Program: 60 C (1 min) 4 K/min -> 200 C 10 K/min -> 280 C |
| Capillary | SF-96 | 1158. | Malingré and Maarse, 1974 | Column length: 150. m; Column diameter: 0.75 mm; Program: not specified |
Kovats' RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-Wax | 1492. | Gauvin, Lecomte, et al., 2004 | 50. m/0.2 mm/0.4 μm, He, 4. K/min, 230. C @ 30. min; Tstart: 60. C |
| Capillary | Carbowax 20M | 1454. | Kulkarni, Mallavarapu, et al., 1998 | N2, 5. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 200. C |
| Capillary | Carbowax 20M | 1440. | Gaydou, Randriamiharisoa, et al., 1986 | 50. m/0.3 mm/0.15 μm, H2, 2. K/min; Tstart: 70. C; Tend: 210. C |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5 | 1155. | Benzo, Gilardoni, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 5. K/min, 250. C @ 10. min |
| Capillary | BP-1 | 1133. | Castilho, Liu, et al., 2007 | 50. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C |
| Capillary | HP-5MS | 1154. | Vagionas, Ngassapa, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | HP-5MS | 1150. | Kukic J., Petrovic S., et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | CP Sil 5 CB | 1136. | Ziegenbein, Hanssen, et al., 2006 | H2, 10. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 270. C |
| Capillary | DB-5 | 1163. | Agnihotri, Agarwal, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 90. C @ 2. min, 4. K/min; Tend: 220. C |
| Capillary | DB-1 | 1125. | de Feo, Urrunaga Soria, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min |
| Capillary | HP-5MS | 1154. | Pino, Mesa, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min |
| Capillary | HP-5 | 1153. | Shellie and Marriott, 2003 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 240. C |
| Capillary | DB-5 | 1156. | Tampieri, Galuppi, et al., 2003 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | SPB-5 | 1154. | Pino, Marbot, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min |
| Capillary | DB-5 | 1152. | Nogueira, Bittrich, et al., 2001 | 30. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | CP Sil 5 CB | 1131. | Pino and Marbot, 2001 | 50. m/0.32 mm/0.4 μm, He, 60. C @ 10. min, 3. K/min, 280. C @ 60. min |
| Capillary | BPX-5 | 1176. | Zabaras and Wyllie, 2001 | 50. m/0.22 mm/0.25 μm, H2, 60. C @ 5. min, 4. K/min, 180. C @ 5. min |
| Capillary | BP-1 | 1135. | Baldovini, Ristorcelli, et al., 2000 | 50. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C |
| Capillary | OV-101 | 1127. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 1. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1130. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 1. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1132. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 0. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1139. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 0. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1131. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1131. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1134. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1134. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1135. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 4. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1137. | Baaliouamer, Boudarene, et al., 1993 | He, 60. C @ 8. min, 4. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1131. | Baaliouamer, Boudarene, et al., 1993 | He, 70. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1136. | Baaliouamer, Boudarene, et al., 1993 | He, 70. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1135. | Baaliouamer, Boudarene, et al., 1993 | He, 80. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
| Capillary | OV-101 | 1139. | Baaliouamer, Boudarene, et al., 1993 | He, 80. C @ 8. min, 2. K/min, 260. C @ 30. min; Column length: 25. m; Column diameter: 0.20 mm |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-52 | 1155. | Bruni, Bianchi, et al., 2007 | 30. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C(10min) |
| Capillary | BPX-5 | 1172. | Cardeal, da Silva, et al., 2006 | 30. m/0.25 mm/0.25 μm; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min) |
| Capillary | CP Sil 5 CB | 1143. | Chanegriha, Baaliouamer, et al., 1998 | Program: not specified |
| Capillary | SE-52 | 1156. | Mondello, Dugo, et al., 1995 | 60. m/0.32 mm/0.40 μm, He; Program: 45 C (6 min) 3 C/min -> 111 0C 2 C/min -> 160 C 3 C/min -> 300 C (15 min) |
Van Den Dool and Kratz RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | BP-20 | 1467. | Castilho, Liu, et al., 2007 | 50. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C |
| Capillary | DB-Wax | 1438. | Varming, Andersen, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 10. min, 6. K/min, 240. C @ 25. min |
| Capillary | FFAP | 1504. | Agnihotri, Agarwal, et al., 2005 | 20. m/0.25 mm/0.25 μm, He, 90. C @ 2. min, 4. K/min; Tend: 220. C |
| Capillary | DB-Wax | 1473. | Choi, 2005 | 60. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min |
| Capillary | DB-Wax | 1474. | Choi, 2003 | 60. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min |
| Capillary | AT-Wax | 1448. | Pino and Marbot, 2001 | 60. m/0.32 mm/0.25 μm, He, 65. C @ 10. min, 2. K/min, 250. C @ 60. min |
| Capillary | BP-20 | 1456. | Baldovini, Ristorcelli, et al., 2000 | 50. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C |
| Capillary | DB-Wax | 1476. | Choi and Sawamura, 2000 | 60. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min |
| Capillary | DB-Wax | 1451. | Möllenbeck, König, et al., 1997 | 25. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 4. K/min; Tend: 240. C |
| Capillary | Carbowax 20M | 1458. | Mondello, Dugo, et al., 1995 | 60. m/0.32 mm/0.425 μm, He, 45. C @ 3. min, 3. K/min, 300. C @ 20. min |
Van Den Dool and Kratz RI, polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | CP-Wax 52CB | 1472. | Romeo, Ziino, et al., 2007 | 60. m/0.25 mm/0.25 μm, He; Program: 45C(5min) => 10C/min => 80C => 2C/min => 240C |
| Capillary | DB-Wax | 1486. | Guillot, Peytavi, et al., 2006 | 30. m/0.25 mm/0.25 μm, He; Program: 60C => 5C/min => 200C => 6C/min => 250C(5min) |
| Capillary | BP-20 | 1478. | Chanegriha, Baaliouamer, et al., 1998 | He; Program: not specified |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Optima-5 | 1145. | Al-Qudah, Muhaidat, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium, 60. C @ 1. min, 3. K/min; Tend: 246. C |
| Capillary | DB-5 | 1141. | Boukhris, Bouaziz, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium, 100. C @ 1. min, 10. K/min, 260. C @ 10. min |
| Capillary | HP-5 MS | 1150. | Kotowska, Zalikowski, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium, 35. C @ 5. min, 3. K/min, 300. C @ 15. min |
| Capillary | HP-5 | 1153. | Bertoli, Lepnardi, et al., 2011 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | VF-5 MS | 1158. | Leffingwell and Alford, 2011 | 60. m/0.32 mm/0.25 μm, Helium, 2. K/min, 260. C @ 28. min; Tstart: 30. C |
| Capillary | VF-5 MS | 1160. | Leffingwell and Alford, 2011 | 60. m/0.32 mm/0.25 μm, Helium, 2. K/min, 260. C @ 28. min; Tstart: 30. C |
| Capillary | HP-5 MS | 1158. | Radulovic, Blagojevic, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C |
| Capillary | HP-5 MS | 1159. | Radulovic, Dordevic, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C |
| Capillary | DB-5 | 1153. | Alim, Goze, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | OV-101 | 1136. | Benites, Moiteiro, et al., 2009 | 50. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 70. C; Tend: 220. C |
| Capillary | 5 % Phenyl methyl siloxane | 1153. | Retta, Gattuso, et al., 2009 | 60. m/0.25 mm/0.25 μm, Helium, 3. K/min, 225. C @ 3. min; Tstart: 90. C |
| Capillary | DB-5 MS | 1161. | Su, Wang, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium, 40. C @ 2. min, 4. K/min, 250. C @ 2. min |
| Capillary | HP-5 MS | 1155. | Zhao, Zeng, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium, 4. K/min; Tstart: 50. C; Tend: 280. C |
| Capillary | ZB-1 | 1125. | Mierendorff, Stahl-Biskup, et al., 2008 | 30. m/0.25 mm/0.25 μm, Nitrogen, 3. K/min; Tstart: 45. C; Tend: 230. C |
| Capillary | DB-5 | 1166. | Baranauskiene R., Bylaite E., et al., 2007 | 50. m/0.32 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min, 280. C @ 10. min |
| Capillary | CP Sil 5 CB | 1139. | Baran, von Reuss, et al., 2007 | 30. m/0.32 mm/0.25 μm, N2, 4. K/min; Tstart: 60. C; Tend: 300. C |
| Capillary | HP-5MS | 1156. | Bozin B., Mlmica-Dukic N., et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | DB-5 | 1127. | Coelho, Grosso, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 70. C @ 5. min, 3. K/min, 310. C @ 20. min |
| Capillary | CP Sil 5 CB | 1145. | Hnawia, Cabalion, et al., 2007 | 30. m/0.25 mm/0.25 μm, N2, 5. K/min; Tstart: 50. C; Tend: 200. C |
| Capillary | HP-5 MS | 1153. | Vagionas, Graikou, et al., 2007 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | HP-5MS | 1156.6 | Zizovic, Stamenic, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 40. C; Tend: 260. C |
| Capillary | HP-5MS | 1157. | Bozin, Mimicá-Dukic, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | DB-5 | 1156. | Morteza-Semnani, Akbarzadeh, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 220. C |
| Capillary | DB-5 | 1154. | Morteza-Semnani K., Akbarzadeh M., et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 220. C |
| Capillary | DB-1 | 1143. | Tohar, Mohd, et al., 2006 | 30. m/0.32 mm/0.25 μm, 60. C @ 3. min, 3. K/min, 230. C @ 10. min |
| Capillary | Methyl Silicone | 1167. | Tonzibo, Coffy, et al., 2006 | 25. m/0.3 mm/0.15 μm, N2, 50. C @ 5. min, 2. K/min; Tend: 210. C |
| Capillary | DB-5 | 1127. | Yadegarinia, Gachkar, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 40. C; Tend: 250. C |
| Capillary | HP-5 | 1153. | Duarte, Figueira, et al., 2005 | 25. m/0.2 mm/0.33 μm, He, 3. K/min, 240. C @ 7. min; Tstart: 60. C |
| Capillary | HP-5 | 1149.8 | Leffingwell and Alford, 2005 | 60. m/0.32 mm/0.25 μm, He, 30. C @ 2. min, 2. K/min, 260. C @ 28. min |
| Capillary | DB-1 | 1152. | Salehi, Sonboli, et al., 2005 | 60. m/0.25 mm/0.25 μm, He, 5. K/min, 250. C @ 10. min; Tstart: 60. C |
| Capillary | DB-5 | 1154. | Sefidkon and Jamzad, 2005 | He, 4. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 40. C; Tend: 240. C |
| Capillary | HP-5MS | 1156. | Slavkovska, Couladis, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | RTX-1 | 1137. | Sonboli, Salehi, et al., 2005 | 60. m/0.25 mm/0.25 μm, He, 5. K/min, 25. C @ 10. min; Tstart: 60. C |
| Capillary | HP-5MS | 1176. | Tepe B., Sokmen M., et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 3. K/min; Tend: 240. C |
| Capillary | HP-5 | 1139. | Aghel, Yamini, et al., 2004 | 30. m/0.25 mm/0.32 μm, He, 60. C @ 3. min, 5. K/min; Tend: 250. C |
| Capillary | DB-1 | 1149. | Choi, 2004 | 60. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min |
| Capillary | DB-5 | 1152. | Kalvandi, Sefidkon, et al., 2004 | 60. m/0.25 mm/0.25 μm, He, 40. C @ 4. min, 4. K/min; Tend: 280. C |
| Capillary | DB-5 | 1152. | Miyazawa, Fuhita, et al., 2004 | Helium, 2. K/min, 240. C @ 999. min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C |
| Capillary | DB-5 | 1152. | Miyazawa, Fujita, et al., 2004 | Helium, 2. K/min, 240. C @ 999. min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 60. C |
| Capillary | DB-1 | 1125. | Park, Lee, et al., 2004 | 60. m/0.32 mm/0.25 μm, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min |
| Capillary | DB-1 | 1126. | Park, Lee, et al., 2004 | 60. m/0.32 mm/0.25 μm, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min |
| Capillary | DB-1 | 1127. | Park, Lee, et al., 2004 | 60. m/0.32 mm/0.25 μm, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min |
| Capillary | DB-1 | 1130. | Park, Lee, et al., 2004 | 60. m/0.32 mm/0.25 μm, He, 35. C @ 4. min, 2. K/min, 230. C @ 25. min |
| Capillary | HP-1 | 1125. | Senatore, Napolitano, et al., 2004 | 30. m/0.25 mm/0.33 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min |
| Capillary | BPX-5 | 1175. | Vilaseca, Guy, et al., 2004 | 25. m/0.22 mm/1. μm, He, 60. C @ 5. min, 3. K/min, 250. C @ 10. min |
| Capillary | DB-5 | 1165. | Edris and Farrag, 2003 | He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 220. C |
| Capillary | ZB-1 | 1125. | Mierendorff, Stahl-Biskup, et al., 2003 | 30. m/0.25 mm/0.25 μm, N2, 3. K/min; Tstart: 45. C; Tend: 230. C |
| Capillary | DB-5 | 1154. | Pino, Marbot, et al., 2003 | 30. m/0.25 mm/0.25 μm, H2, 60. C @ 10. min, 4. K/min, 280. C @ 40. min |
| Capillary | DB-5 | 1126. | Phatak and Heble, 2002 | 30. m/0.25 mm/0.25 μm, He, 70. C @ 3. min, 3. K/min, 250. C @ 2. min |
| Capillary | BP-1 | 1136. | Gupta, Mallavarapu, et al., 2001 | 30. m/0.25 mm/0.25 μm, N2, 5. K/min; Tstart: 60. C; Tend: 220. C |
| Capillary | SPB-1 | 1125. | Kamath, Asha, et al., 2001 | 30. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 180. C @ 1. min |
| Capillary | OV-101 | 1135. | Orav and Kann, 2001 | He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 50. C; Tend: 250. C |
| Capillary | HP-5 | 1144. | Lis-Balchin and Roth, 2000 | He, 9. K/min, 200. C @ 10. min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 80. C |
| Capillary | HP-1 | 1125. | Lopes, Koketsu, et al., 1999 | 25. m/0.32 mm/0.17 μm, H2, 40. C @ 5. min, 3. K/min; Tend: 260. C |
| Capillary | OV-101 | 1141. | Menon, Chacko, et al., 1999 | N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C |
| Capillary | OV-1 | 1142. | Oberhofer, Nikiforov, et al., 1999 | 25. m/0.25 mm/0.25 μm, H2, 40. C @ 5. min, 3. K/min, 220. C @ 5. min |
| Capillary | BP-1 | 1141. | Rao, Bhattacharya, et al., 1999 | N2, 5. K/min, 220. C @ 10. min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 60. C |
| Capillary | DB-5 | 1129. | Reverchon, Porta, et al., 1997 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 2. K/min; Tend: 250. C |
| Capillary | DB-1 | 1149. | Sagrero-Nieves and Bartley, 1996 | 60. m/0.32 mm/0.50 μm, He, 50. C @ 1. min, 8. K/min, 250. C @ 6. min |
| Capillary | OV-101 | 1134. | De Pooter and Schamp, 1986 | 30. m/0.5 mm/0.8 μm, He, 2. K/min; Tstart: 40. C; Tend: 220. C |
| Capillary | OV-101 | 1132. | De Pooter and Schamp, 1986 | 30. m/0.5 mm/0.8 μm, He, 2. K/min; Tstart: 40. C; Tend: 220. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 1120. | Albano, Lima, et al., 2012 | 30. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) |
| Capillary | HP-5 MS | 1154. | Kotowska, Zalikowski, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
| Capillary | Polydimethyl siloxane with 5 % Ph groups | 1154. | Robinson, Adams, et al., 2012 | Program: not specified |
| Capillary | Polydimethyl siloxane with 5 % Ph groups | 1165. | Robinson, Adams, et al., 2012 | Program: not specified |
| Capillary | HP-5 MS | 1153. | Sharopov, Sulaimonova, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C |
| Capillary | DB-1 | 1143. | Delort and Jaquier, 2009 | 60. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min) |
| Capillary | RTX-5 MS | 1153. | Mebazaa, Mahmoudi, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (5 min) 2 0C/min -> 100 0C (5 min) 5 0C/min -> 300 0C |
| Capillary | RTX-5 MS | 1154. | Mebazaa, Mahmoudi, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
| Capillary | DB-5 MS | 1155. | Su, Wang, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
| Capillary | SPB-1 | 1147. | Díaz-Maroto, Castillo, et al., 2007 | 50. m/0.25 mm/0.25 μm; Program: 70C(3min) => 4C/min => 120C => 8C/min => 250C(5min) |
| Capillary | HP-5 MS | 1138. | Formisano, Rigano, et al., 2007 | 30. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (5 min) 2 0C/min -> 250 0C (15 min) 10 0C/min -> 270 0C |
| Capillary | HP-5MS | 1138. | Senatore, Apostolides Arnold, et al., 2006 | 30. m/0.25 mm/0.25 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C |
| Capillary | SE-52 | 1153. | Tognolini, Barocelli, et al., 2006 | 30. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min) |
| Capillary | HP-5MS | 1153. | Sahin, Gulluce, et al., 2004 | 30. m/0.25 mm/0.25 μm, He; Program: 50C(3min) => 3C/min => 150C(10min) => 10C/min => 250C |
| Capillary | DB-5 | 1154. | Vilaseca, Guy, et al., 2004 | Program: not specified |
| Capillary | SE-30 | 1143. | Vinogradov, 2004 | Program: not specified |
| Capillary | Methyl Silicone | 1141. | Bakshu and Raju, 2002 | Program: not specified |
| Capillary | DB-1 | 1120. | Baratta, Dorman, et al., 1998 | 30. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 240C (10min) |
| Capillary | DB-5 | 1154. | Isidorov, Zenkevich, et al., 1997 | Program: not specified |
| Capillary | Polydimethyl siloxanes | 1139. | Zenkevich, 1997 | Program: not specified |
| Capillary | OV-101 | 1142. | Shibamoto, 1987 | Column length: 60. m; Column diameter: 0.25 mm; Program: not specified |
| Capillary | OV-101 | 1143. | Shibamoto, 1987 | Program: not specified |
| Packed | OV-101 | 1140. | Swigar and Silverstein, 1981 | N2, Chromosorb G 60-80mesh DMCS; Column length: 2.5 m; Program: not specified |
Normal alkane RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-Innowax | 1475. | Formisano, Rigano, et al., 2007 | 30. m/0.25 mm/0.25 μm, Helium, 40. C @ 5. min, 2. K/min; Tend: 250. C |
| Capillary | Carbowax | 1450. | Singh, Kumar, et al., 2007 | 60. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 40. C; Tend: 180. C |
| Capillary | DB-Wax | 1473. | Choi, 2006 | 60. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min |
| Capillary | Carbowax 20M | 1444. | Babu and Kaul, 2005 | 60. m/0.25 mm/0.25 μm, N2, 40. C @ 2. min, 10. K/min, 190. C @ 15. min |
| Capillary | CP-Wax | 1448. | Ka, Choi, et al., 2005 | 30. m/0.32 mm/0.25 μm, He, 40. C @ 2. min, 5. K/min; Tend: 180. C |
| Capillary | PE-Wax | 1455. | Ram, Kumar, et al., 2005 | 50. m/0.32 mm/0.25 μm, H2, 4. K/min, 220. C @ 2. min; Tstart: 60. C |
| Capillary | DB-Wax | 1445. | Salehi, Sonboli, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 4. K/min, 250. C @ 10. min; Tstart: 40. C |
| Capillary | DB-Wax | 1476. | Choi, 2004 | 60. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min |
| Capillary | DB-Wax | 1475. | Tu, Thanh, et al., 2002 | 60. m/0.25 mm/0.25 μm, N2, 2. K/min; Tstart: 70. C; Tend: 230. C |
| Capillary | PEG-20M | 1464. | Orav and Kann, 2001 | He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 70. C; Tend: 220. C |
| Capillary | HP Innowax FSP | 1474. | Kaya, Baser, et al., 1999 | 60. m/0.25 mm/0.25 μm, He, 60. C @ 10. min, 220. C @ 10. min |
| Capillary | Innowax | 1474. | Kaya, Baser, et al., 1999, 2 | 60. m/0.25 mm/0.25 μm, He, 60. C @ 10. min; Tend: 220. C |
| Capillary | HP-Innowax | 1474. | Kaya, Baser, et al., 1999, 3 | 60. m/0.25 mm/0.25 μm, He, 60. C @ 10. min; Tend: 220. C |
| Capillary | HP-Innowax | 1474. | Kaya, Baser, et al., 1999, 3 | 60. m/0.25 mm/0.25 μm, He, 60. C @ 10. min; Tend: 220. C |
| Capillary | HP-Innowax | 1474. | Kaya, Baser, et al., 1999, 3 | 60. m/0.25 mm/0.25 μm, He, 60. C @ 10. min; Tend: 220. C |
| Capillary | Carbowax | 1478. | Menon, Chacko, et al., 1999 | N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C |
| Capillary | BP-20 | 1444. | Rao, Bhattacharya, et al., 1999 | N2, 5. K/min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 60. C; Tend: 200. C |
| Capillary | DB-Wax | 1449. | Werkhoff, Güntert, et al., 1998 | 60. m/0.32 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 220. C |
| Capillary | HP-Innowax FSC | 1476. | Baser, Kirimer, et al., 1997 | He, 60. C @ 10. min, 4. K/min, 240. C @ 10. min; Column length: 60. m; Column diameter: 0.25 mm |
| Capillary | DB-Wax | 1478. | Sagrero-Nieves and Bartley, 1996 | 60. m/0.32 mm/0.50 μm, He, 50. C @ 1. min, 8. K/min, 250. C @ 6. min |
| Capillary | TC-Wax | 1468. | Shuichi, Masazumi, et al., 1996 | 80. C @ 5. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 240. C |
| Capillary | Carbowax 20M | 1444. | Shibamoto, 1987 | 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C |
| Packed | Carbowax 20M | 1502. | Stancher and Pertoldi, 1967 | Hydrogen, Gas-Chrom Z (80-100 mesh), 4. K/min; Column length: 2. m; Tstart: 65. C; Tend: 220. C |
Normal alkane RI, polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Innowax FSC | 1475. | Demirci, Temel, et al., 2011 | 60. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C |
| Capillary | DB-FFAP | 1427. | Mebazaa, Mahmoudi, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 2 0C/min -> 100 0C (5 min) 5 0C/min -> 250 0C |
| Capillary | DB-FFAP | 1427. | Mebazaa, Mahmoudi, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
| Capillary | HP-Innowax | 1475. | Senatore, Apostolides Arnold, et al., 2006 | 50. m/0.2 mm/0.2 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C |
| Capillary | Carbowax 20M | 1478. | Vinogradov, 2004 | Program: not specified |
| Capillary | HP-Innowax | 1475. | Baser, Demirci, et al., 2002 | 60. m/0.25 mm/0.25 μm, He; Program: 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C |
| Capillary | Innowax FSC | 1475. | Tabanca N., Demirci F., et al., 2001 | 60. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C |
| Capillary | HP-Innowax | 1475. | Tabanca, Kirimer, et al., 2001 | 60. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C |
| Capillary | Carbowax 20M | 1478. | Shibamoto, 1987 | Program: not specified |
| Capillary | Carbowax 400, Carbowax 20M, Carbowax 1540, Carbowax 4000, Superox 06, PEG 20M, etc. | 1432. | Waggott and Davies, 1984 | Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Lis-Balchin, M.; Roth, G.,
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Flavour Fragr. J., 1999, 14, 5, 293-299, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<293::AID-FFJ829>3.0.CO;2-T
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Volatile components from the leaves of heterotheca inuloides Cass.,
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Vinogradov, 2004
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Kaya, Baser, et al., 1999, 2
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Kaya, Baser, et al., 1999, 3
Kaya, A.; Baser, K.H.C.; Tümen, G.; Koca, F.,
The essential oil of Acinos suaveolens (Sm.) G. Don fil. Acinos arvensis (Lam.) Dandy and Acinos rotundifolius Pers. growing wild in Turkey,
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Waggott and Davies, 1984
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Notes
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