α-Terpinyl acetate
- Formula: C12H20O2
- Molecular weight: 196.2860
- IUPAC Standard InChIKey: IGODOXYLBBXFDW-LLVKDONJSA-N
- CAS Registry Number: 80-26-2
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: 3-Cyclohexene-1-methanol, α,α,4-trimethyl-, acetate; p-Menth-1-en-8-ol, acetate; α-Terpineol acetate; Terpinyl acetate; 2-(4-Methylcyclohex-3-en-1-yl)propan-2-yl acetate; 1-Methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl acetate; 21090-64-2; 104806-93-1; 10581-37-0; α-Terpenyl acetate; Terpenyl acetate; α-Terpinenyl acetate; Terpineol acetate; terpinenyl acetate; Alpha-Terpenyl acetate; 4-Terpinyl acetate; p-menth-1-en-8-yl acetate
- Permanent link for this species. Use this link for bookmarking this species for future reference.
- Information on this page:
- Other data available:
- Options:
Normal alkane RI, non-polar column, custom temperature program
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | SLB-5 MS | SLB-5 MS | 5 % Phenyl methyl siloxane | HP-5 MS |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | Hydrogen | Helium | Helium | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Program | 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) | not specified | not specified | 50 0C (2 min) 10 0C/min -> 150 0C 15 0C/min -> 300 0C (10 min) | 50 0C (5 min) 6 0C/min -> 125 0C 10 0C/min -> 170 0C |
I | 1334. | 1349. | 1353. | 1352. | 1348. |
Reference | Albano, Lima, et al., 2012 | Mondello, 2012 | Mondello, 2012 | Huang, Qin, et al., 2009 | Keefover-Ring, Thompson, et al., 2009 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | HP-5 | CB-1 | CB-1 | CP Sil 8 CB |
Column length (m) | 30. | 30. | 30. | 30. | 50. |
Carrier gas | Hydrogen | Helium | Helium | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Program | 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) | not specified | 40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min) | not specified | not specified |
I | 1334. | 1351. | 1339. | 1335. | 1349. |
Reference | Mendes, Trindade, et al., 2009 | Isidorov, Lech, et al., 2008 | Kannaste, Vongvanich, et al., 2008 | Kannaste, Vongvanich, et al., 2008 | Kupcinskiene, Stikliene, et al., 2008 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | RTX-5 | RTX-5 | HP-5MS | SPB-5 | HP-5MS |
Column length (m) | 30. | 30. | 30. | 60. | 30. |
Carrier gas | Helium | Helium | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 1. | 0.25 |
Program | 60 0C (5 min) 5 0C/min -> 110 0C 3 0C/min -> 220 0C (5 min) | not specified | 40C(10min) => 3C/min => 200C => 2C/min => 220C | 60C => 1C/min => 180C => 2C/min => 250C (60min) | 40C(10min) => 3C/min => 200C => 2C/min => 220C |
I | 1351. | 1350. | 1350. | 1355. | 1350. |
Reference | Zachariah, Leela, et al., 2008 | Zachariah, Leela, et al., 2008 | Cole, Haber, et al., 2007 | Lucchesi, Smadja, et al., 2007 | Moronkola, Ogunwande, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-5MS | DB-1 | HP-5 | HP-5 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | Hydrogen | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Program | not specified | 40C(10min) => 3C/min => 200C => 2C/min => 220C | 45C => 3C/min => 175C => 15C/min => 300C (10min) | >2.5C/min => 180C => 100C/min => 250C (7.3min) | 60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C |
I | 1350. | 1352. | 1334. | 1363. | 1353. |
Reference | Pontes, de Olivera, et al., 2007 | Takaku, Haber, et al., 2007 | Figueiredo A.C., Barroso J.G., et al., 2006 | Goodner, Mahattanatawee, et al., 2006 | Jordan, Martinez, et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 8 CB | SE-52 | DB-5MS | CP Sil 8 CB | DB-5 |
Column length (m) | 50. | 30. | 30. | 50. | 30. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 0.15 | 0.25 | 0.25 | 0.25 |
Program | 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min) | 45C => 1C/min => 100C => 5C/min => 250C (10min) | 60C => 3C/min => 180C => 250C (2min) | 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min) | 40C(1min) => 9C/min => 130C => 2C/min => 230C |
I | 1349. | 1349. | 1314. | 1350. | 1344. |
Reference | Judzentiene and Buzelyte, 2006 | Tognolini, Barocelli, et al., 2006 | Tuberoso, Barra, et al., 2006 | Butkienë, Nivinskienë, et al., 2005 | Hamm, Bleton, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5MS | CP Sil 8 CB | DB-5 | CP Sil 8 CB | |
Column length (m) | 30. | 50. | 30. | 50. | |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.32 | |
Phase thickness (μm) | 0.25 | 0.25 | 0.1 | 0.25 | |
Program | 40C(5min) => 3C/min => 90C => 10C/min => 280C | 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min) | 35C => 4C/min => 180C => 10C/min => 250C | 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min) | not specified |
I | 1353. | 1349. | 1340. | 1350. | 1337. |
Reference | Novak, Draxler, et al., 2005 | Radudienë, Judpintienë, et al., 2005 | Albuquerque, Souza, et al., 2004 | Butkienë, Nivinskienë, et al., 2004 | El-Shazily, Hafez, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-1 | OV-1 | DB-5 | DB-1 | HP-5 |
Column length (m) | 15. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.317 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Program | 50C(4min) => 4C/min => 90C => 10C/min => 300C(10min) | 45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C | 40C(1min) => 9C/min => 130C => 2C/min => 230C | 45C => 3C/min => 175C => 15C/min => 300C (10min) | 40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C |
I | 1337. | 1336. | 1344. | 1334. | 1333. |
Reference | El-Shazly and Hussein, 2004 | Hafez and Abdel-Salam, 2004 | Hamm, Bleton, et al., 2004 | Miguel, Simões, et al., 2004 | Senatore, Apostolides Arnold, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | DB-5 | SE-30 | SE-30 | DB-1 |
Column length (m) | 30. | 30. | |||
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | |||
Phase thickness (μm) | 0.25 | 0.25 | |||
Program | 60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C | not specified | not specified | not specified | 45C => 3C/min => 175C => 15C/min => 300C (10min) |
I | 1353. | 1350. | 1331. | 1332. | 1334. |
Reference | Sotomayor, Martínez, et al., 2004 | Vilaseca, Guy, et al., 2004 | Vinogradov, 2004 | Vinogradov, 2004 | Faleiro, Miguel, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | HP-5 | SE-54 | DB-1 | DB-5 |
Column length (m) | 30. | 30. | 30. | ||
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | ||
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
Program | 40C (1min) => 9C/min => 130C => 2C/min => 230C | 60C (4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C | not specified | 45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min) | not specified |
I | 1344. | 1353. | 1344. | 1334. | 1348. |
Reference | Hamm, Lesellier, et al., 2003 | Jordán, Martínez, et al., 2003 | Kilic, 2002 | Figueiredo, Miguel, et al., 2001 | Petrakis, Tsitsimpikou, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-1 | DB-1 | CP Sil 5 CB | Methyl Silicone | DB-1 |
Column length (m) | 12. | 30. | 25. | 30. | |
Carrier gas | He | H2 | He | ||
Substrate | |||||
Column diameter (mm) | 0.20 | 0.25 | 0.39 | 0.25 | |
Phase thickness (μm) | 0.33 | 0.25 | 0.25 | ||
Program | 40 0C 6.7 0C/min -> 87 0C (9 min) 10 0C/min -> 187 0C | 40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min) | not specified | not specified | 45C => 3C/min => 175C => 15C/min => 240C (10min) |
I | 1329. | 1334. | 1331. | 1333. | 1334. |
Reference | Betts, 2000 | Dorman, Figueiredo, et al., 2000 | Weyerstahl, Marschall, et al., 1999 | Zenkevich, 1999 | Baratta, Dorman, et al., 1998 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Packed |
---|---|---|---|---|
Active phase | DB-1 | DB-5 | 5 % Phenyl methyl siloxane | OV-101 |
Column length (m) | 30. | 2.5 | ||
Carrier gas | He | N2 | ||
Substrate | Chromosorb G 60-80mesh DMCS | |||
Column diameter (mm) | 0.25 | |||
Phase thickness (μm) | 0.25 | |||
Program | 45C => 3C/min => 175C => 15C/min => 280C | not specified | not specified | not specified |
I | 1334. | 1350. | 1332. | 1337. |
Reference | Gaspar, Palma, et al., 1997 | Isidorov, Zenkevich, et al., 1997 | Sagrero-Nieves and Bartley, 1995 | Swigar and Silverstein, 1981 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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El-Shazily, A.M.; Hafez, S.S.; Wink, M.,
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El-Shazly, A.M.; Hussein, K.T.,
Chemical analysis and biological activities of the essential oil of Teucrium leucocladum Boiss. (Lamiaceae),
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Hafez and Abdel-Salam, 2004
Hafez, S.S.; Abdel-Salam, H.A.,
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Chemical composition of the essential oil of Salvia multicaulis Vahl. var. simplicifolia Boiss. growing wild in Lebanon,
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Sotomayor, Martínez, et al., 2004
Sotomayor, J.A.; Martínez, R.M.; García, A.J.; Jordán, M.J.,
Thymus zygis Subsp. Gracilis: watering level effect on phytomass production and essential oil quality,
J. Agric. Food Chem., 2004, 52, 17, 5418-5424, https://doi.org/10.1021/jf0496245
. [all data]
Vilaseca, Guy, et al., 2004
Vilaseca, A.; Guy, I.; Charles, B.; Guinaudeau, H.; de Arias, A.R.; Fournet, A.,
Chemical composition and insecticidal activity of Hedeoma mandoniana essential oils,
J. Essent. Oil Res., 2004, 16, 4, 380-383, https://doi.org/10.1080/10412905.2004.9698749
. [all data]
Vinogradov, 2004
Vinogradov, B.A.,
Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]
Faleiro, Miguel, et al., 2003
Faleiro, M.L.; Miguel, M.G.; Ladeiro, F.; Venancio, F.; Tavares, R.; Brito, J.C.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.,
Antimicrobial activity of essential oils isolated from Portuguese endemic species of Thymus,
Lett. Appl. Microbiol., 2003, 36, 1, 35-40, https://doi.org/10.1046/j.1472-765X.2003.01259.x
. [all data]
Hamm, Lesellier, et al., 2003
Hamm, S.; Lesellier, E.; Bleton, J.; Tchapla, A.,
Optimization of headspace solid phase microextraction for gas chromatography/mass spectrometry analysis of widely different volatility and polarity terpenoids in olibanum,
J. Chromatogr. A, 2003, 1018, 1, 73-83, https://doi.org/10.1016/j.chroma.2003.08.027
. [all data]
Jordán, Martínez, et al., 2003
Jordán, M.J.; Martínez, R.M.; Cases, M.A.; Sotomayor. J.A.,
Watering level effect on Thymus hyemalis lange essential oil yield and composition,
J. Agric. Food Chem., 2003, 51, 18, 5420-5427, https://doi.org/10.1021/jf034335m
. [all data]
Kilic, 2002
Kilic, A.,
Volatile compounds of buds, flowers and fruits of bay (Laurus nobilis L.) and their odour contribution,
Proc. ICNP-2002 - Trabzon/Turkiye, 2002, 338-341. [all data]
Figueiredo, Miguel, et al., 2001
Figueiredo, A.C.; Miguel, M.G.; Duarte, A.M.F.; Barroso, J.G.; Pedro, L.G.,
Essential oil composition of Thymus lotocephallus G. López R. Morales, collected during flowering and vegetative phases,
Flavour Fragr. J., 2001, 16, 6, 417-421, https://doi.org/10.1002/ffj.1028
. [all data]
Petrakis, Tsitsimpikou, et al., 2001
Petrakis, P.V.; Tsitsimpikou, C.; Tzakou, O.; Couladis, M.; Vagias, C.; Roussis, V.,
Needle volatiles from five Pinus species growing in Greece,
Flavour Fragr. J., 2001, 16, 4, 249-252, https://doi.org/10.1002/ffj.990
. [all data]
Betts, 2000
Betts, T.J.,
Solid phase microextraction of volatile constituents from individual fresh Eucalyptis leaves of three species,
Planta Medica, 2000, 66, 2, 193-195, https://doi.org/10.1055/s-0029-1243133
. [all data]
Dorman, Figueiredo, et al., 2000
Dorman, H.J.D.; Figueiredo, A.C.; Barroso, J.G.; Deans, S.G.,
In vitro evaluation of antioxidant activity of essential oils and their components,
Flavour Fragr. J., 2000, 15, 1, 12-16, https://doi.org/10.1002/(SICI)1099-1026(200001/02)15:1<12::AID-FFJ858>3.0.CO;2-V
. [all data]
Weyerstahl, Marschall, et al., 1999
Weyerstahl, P.; Marschall, H.; Splittgerber, U.; Son, P.T.; Giang, P.M.; Kaul, V.K.,
Constituents of the essential oil from the fruits of Zanthoxylum rhetsoides Drake from Vietnam and from the aerial parts of Zanthoxylum alatum Roxb. from India,
Flavour Fragr. J., 1999, 14, 4, 225-229, https://doi.org/10.1002/(SICI)1099-1026(199907/08)14:4<225::AID-FFJ818>3.0.CO;2-1
. [all data]
Zenkevich, 1999
Zenkevich, I.G.,
Analytical Parameters of Components of essential Oils for their Gas Chromatographic and Chromato-Mass-Spectral Identification. Acetates of Terpene Alcohols,
Rastitelnye Resursy (Plant Resources), 1999, 35, 1, 30-37. [all data]
Baratta, Dorman, et al., 1998
Baratta, M.T.; Dorman, H.J.; Deans, S.G.; Figueiredo, A.C.; Barroso, J.G.; Ruberto, G.,
Antimicrobial and antioxidant properties of some commercial essential oils,
Flavour Fragr. J., 1998, 13, 4, 235-244, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<235::AID-FFJ733>3.0.CO;2-T
. [all data]
Gaspar, Palma, et al., 1997
Gaspar, H.; Palma, F.M.S.B.; de la Torre, M.C.; Rodríguez, B.; Barroso, J.G.; Figueiredo, A.C.,
Composition of the essential oil of Teucrium haenseleri Boiss.,
Flavour Fragr. J., 1997, 12, 5, 355-357, https://doi.org/10.1002/(SICI)1099-1026(199709/10)12:5<355::AID-FFJ656>3.0.CO;2-B
. [all data]
Isidorov, Zenkevich, et al., 1997
Isidorov, V.; Zenkevich, I.; Sacharevich, T.,
Calculation of Gas Chromatographic Retention Indices for Monoterpenes and Terpenoids from Their Physico-Chemical Constants,
Chem. Anal. (Warsaw), 1997, 42, 627-634. [all data]
Sagrero-Nieves and Bartley, 1995
Sagrero-Nieves, L.; Bartley, J.P.,
Volatile Constituents from the Leaves of Chenopodium ambrosioides L.,
J. Essent. Oil Res., 1995, 7, 2, 221-223, https://doi.org/10.1080/10412905.1995.9698506
. [all data]
Swigar and Silverstein, 1981
Swigar, A.A.; Silverstein, R.M.,
Monoterpenes, Aldrich Chemical Company, Milwaukee, WI, USA, 1981, 130. [all data]
Notes
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