Camphene

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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RTX-1RTX-1Mega-5CBP-5
Column length (m) 30.60.60.25.30.
Carrier gas HydrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specifiednot specifiednot specified60 0C 3 0C/min -> 240 0C 10 0C/min -> 280 0C (10 min)
I 938.944.944.954.954.
ReferenceAlbano, Lima, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dell'Agli, Sanna, et al., 2012de Morais, Oliveira, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Polydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groupsHP-5Siloxane, 5 % Ph
Column length (m)   30.25. 
Carrier gas   HeliumHydrogen 
Substrate      
Column diameter (mm)   0.250.32 
Phase thickness (μm)   0.250.52 
Program not specifiednot specified50 0C 4 0C/min -> 200 0C (5 min) 20 0C/min -> 280 0Cnot specifiednot specified
I 954.961.947.954.950.
ReferenceRobinson, Adams, et al., 2012Robinson, Adams, et al., 2012da Silva, de Souza, et al., 2012Velickovic, Ristic, et al., 2012VOC BinBase, 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-55 % Phenyl polydimethyl siloxaneOV-1DB-1 
Column length (m) 30. 30.30. 
Carrier gas Helium HeliumHelium 
Substrate      
Column diameter (mm) 0.25 0.250.25 
Phase thickness (μm) 0.25  0.25 
Program not specifiednot specified40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)50 0C (5 min) 3 0C/min -> 240 0C 15 0C/min -> 300 0C (3 min)not specified
I 953.951.936.953.953.
ReferenceCao, Li, et al., 2011Chaverri, Diaz, et al., 2011Chen and Li, 2011Fathi, Sahari, et al., 2011Karimi, Farmany, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Polydimethyl siloxane, 5 % phenylRTX-1DB-5SLB-5 MS
Column length (m) 30. 60.30.10.
Carrier gas Nitrogen HeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.25 0.220.250.10
Phase thickness (μm) 0.25 0.250.250.10
Program 35 0C (10 min) 3 0C/min -> 205 0C 10 0C/min -> 225 0Cnot specifiednot specified35 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 280 0Cnot specified
I 951.950.943.949.953.
ReferenceLaribi, Kouki, et al., 2011Skogerson, Wohlgemuth, et al., 2011Dib, Djabou, et al., 2010Pontes, Silva, et al., 2010Scandinaro, Tranchida, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1-MSDB-1DB-5DB-15 % Phenyl methyl siloxane
Column length (m) 60.30.30.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specifiednot specified50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)50 0C (2 min) 10 0C/min -> 150 0C 15 0C/min -> 300 0C (10 min)
I 941.959.958.951.957.
ReferenceTakeoka, Hobbs, et al., 2010Xu, Tang, et al., 2010Courtois, Paine, et al., 2009Delort and Jaquier, 2009Huang, Qin, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-5 MSRTX-5RTX-5HP-5 MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeliumNitrogenNitrogenHeliumHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)60 0C 95 min) 110 0C 3 0C/min -> 200 0C 5 0C/min -> 220 0C 95 min)not specified40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)
I 942.949.954.953.938.
ReferenceKapoor, Singh, et al., 2009Leela, Vipin, et al., 2009Leela, Vipin, et al., 2009Mancini, Arnold, et al., 2009Mendes, Trindade, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5HP-5DB-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHeliumHelium Helium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Program 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specifiednot specifiednot specifiednot specified
I 938.950.953.951.951.
ReferenceMendes, Trindade, et al., 2009, 2Porto, Decorti, et al., 2009Porto, Decorti, et al., 2009Riahi, Pourbasheer, et al., 2009Su, Wang, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-1HP-5 MSSLB-5 MSSLB-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Program 50 0C 95 min) 3 0C/min -> 100 0C 4 0C/min -> 160 0C 5 0C/min -> 220 0C (15 min)40 0C 2 0C/min -> 130 0C (5 min) 10 0C/min -> 230 0C (15 min)32 0C (1 min) 50 0C/min -> 115 0C 1.5 0C/min -> 145 0C 12 0C/min -> 240 0C (10 min)50 0C 3 0C/min -> 250 0C (1 min) 10 0C/min -> 300 0C (5 min)not specified
I 951.932.952.953.946.
ReferenceYang, Yang, et al., 2009Yu, Li, et al., 2009Zellner, Amorim, et al., 2009Costa, De Fina, et al., 2008Costa, De Fina, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CB-1CB-1CP Sil 8 CBSLB-5 MS
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min)not specifiednot specifiednot specified
I 953.956.950.953.953.
ReferenceIsidorov, Lech, et al., 2008Kannaste, Vongvanich, et al., 2008Kannaste, Vongvanich, et al., 2008Kupcinskiene, Stikliene, et al., 2008Lo Presti, Sciarrone, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1Elite-1DB-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHelium Helium
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40 0C (2 min) 3 0C/min -> 180 0C (2 min) 15 0C -> 280 0C45C => 3C/min => 175C => 15C/min => 300C (10min)not specified80 0C (1.5 min) 4 pC/min -> 180 0C 10 0C/min -> 300 0C (10 min)40 0C (2 min) 4 0C/min -> 220 0C 20 0C/min -> 280 0C
I 959.938.954.951.943.
ReferenceNing, Zheng, et al., 2008Nogueira, Marcelo-Curto, et al., 2008Raj, Baby, et al., 2008Silva, Doria, et al., 2008Xie, Sun, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5RTX-55 % Phenyl methyl siloxaneDB-5MSCBP-5
Column length (m) 30.30. 30.30.
Carrier gas HeliumHelium HeHe
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm) 0.250.25 0.250.25
Program 60 0C (5 min) 5 0C/min -> 110 0C 3 0C/min -> 220 0C (5 min)not specifiednot specified60C => 1C/min => 65C => 3C/min => 120C => 5C/min => 180C(5min) => 5C/min => 250C (20min)60C(2min) => 3C/min => 240C => 10C/min => 300C
I 948.954.957.947.950.
ReferenceZachariah, Leela, et al., 2008Zachariah, Leela, et al., 2008Agabriel, Cornu, et al., 2007Barra A., Coroneo V., et al., 2007Cheriti, Saad, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSSPB-1DB-1HP-5MS
Column length (m) 30.30.50.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40C => 3C/min => 100C => 5C/min => 230C(2min)40C(10min) => 3C/min => 200C => 2C/min => 220C70C(3min) => 4C/min => 120C => 8C/min => 250C(5min)45C => 3C/min => 175C => 15C/min => 300C (10min)40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C
I 945.953.945.938.953.
ReferenceChokeprasert P., Charles A.L., et al., 2007Cole, Haber, et al., 2007Díaz-Maroto, Castillo, et al., 2007Ferreira, Meireles de Sousa, et al., 2007Formisano, Mignola, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5DB-1HP-5MSHP-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.20.25
Phase thickness (μm) 0.250.250.250.330.25
Program 60C => 4C/min => 150C => 10C/min => 220C45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)40C(3min) => 8C/min => 160C => 15C/min => 300C (10min)60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)40C(10min) => 3C/min => 200C => 2C/min => 220C
I 948.938.950.954.953.
ReferenceHashemi, Abolghasemi, et al., 2007Kamatou, Viljoen, et al., 2007Liu, Song, et al., 2007Merle, Verdeguer, et al., 2007Moronkola, Ogunwande, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 8 CBDB-15 % Phenyl methylsiloxaneHP-5 MS
Column length (m) 50.50.30. 30.
Carrier gas HeliumHeliumHe Helium
Substrate      
Column diameter (mm) 0.320.320.25 0.25
Phase thickness (μm) 0.250.250.25  
Program 60 0C (1 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 280 0C (3 min)45C => 3C/min => 175C => 15C/min => 300C(10min)not specified40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C
I 954.954.938.959.957.
ReferenceNivinsliene, Butkiene, et al., 2007Radusiene, Judzentiene, et al., 2007Rodrigues, Antunes, et al., 2007Serrano, Cornu, et al., 2007Setzer, Stokes, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5BPX-5SPB-5
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm)  0.250.250.251.
Program 40C(10min) => 3C/min => 200C => 2C/min => 220C40C(3min) => 6C/min => 160C => 10C/min => 300C (10min)35C => 4C/min => 180C => 10C/min => 250C50C => 3C/min => 150C(10min) => 10C/min => 250C60C => 1C/min => 130C => 2C/min => 200C => 4C/min => 250C (40min)
I 956.953.948.944.933.
ReferenceTakaku, Haber, et al., 2007Yu, Huang, et al., 2007Albuquerque, Canuto, et al., 2006Baris, Güllüce, et al., 2006Chemat, Lucchesi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1HP-5MSSPB-5HP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.251.0.25
Program 50C(2min) => 6C/min => 200C => 10C/min => 270C(10min)45C => 3C/min => 175C => 15C/min => 300C (10min)40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C60C => 1C/min => 130C => 2C/min => 200C => 4C/min => 250C(40min)60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
I 955.938.953.933.969.
ReferenceDeng, Xu, et al., 2006Figueiredo A.C., Barroso J.G., et al., 2006Formisano C., Senatore F., et al., 2006Iriti, Colnaghi, et al., 2006Jordan, Martinez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5DB-1SE-52HP-5
Column length (m) 50.30.30.25.30.
Carrier gas HeHeliumHeH2 
Substrate      
Column diameter (mm) 0.320.320.250.320.25
Phase thickness (μm) 0.250.25 0.420.25
Program 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)not specified35C => 4C/min => 180C => 10C/min => 250C60C(8min) => 3C/min => 180C => 20C/min => 250C (10min)not specified
I 954.952.954.943.969.
ReferenceJudzentiene and Buzelyte, 2006Kucuk, Gulec, et al., 2006de Lima, Maia, et al., 2006Lorenzo, Loayza, et al., 2006Martinez, Madrid, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5BPX-5DB-5HP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.100.250.250.250.25
Program 40 0C (1 min) 10 0C/min -> 120 0C 0.5 0C/min -> 150 0C 20 0C/min -> 280 0C (5 min)50C => 3C/min => 150C (10min) => 10C/min => 250C35C => 4C/min => 180C => 10C/min => 250C60C => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)60C(1min) => 1.5C => 185C => 9C/min => 275C (2min)
I 953.944.953.954.953.
ReferenceNavickiene, Morandim, et al., 2006Ozer H., Kilic H., et al., 2006Santos, Nunes, et al., 2006Singh, Marimuthu, et al., 2006Singh G., Maurya S., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-52DB-1DB-1CP Sil 8 CB
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (μm) 0.250.150.250.250.25
Program 60C => 2C/min => 100C => 3C/min => 160C => 5C/min => 280C45C => 1C/min => 100C => 5C/min => 250C (10min)35C => 2C/min => 200C => 5C/min => 240C45C => 3C/min => 175C => 15C/min => 300C(10min)50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)
I 950.954.931.938.954.
ReferenceSrivastava, Mallavarapu, et al., 2006Tognolini, Barocelli, et al., 2006Al-Burtamani, Fatope, et al., 2005Belhattab, Larous, et al., 2005Butkienë, Nivinskienë, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1DB-5BPX-5BPX-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.5
Program 50C => 8C/min => 200C => 10C/min => 270C (5min)45C => 3C/min => 175C => 15C/min => 300C (10min)40C(1min) => 9C/min => 130C => 2C/min => 230C60C(0.2min) => 3K/min => 186C => 10C/min => 240C (5min)60C(1min) => 3.5C/min => 180C => 20C/min => 280C(2min)
I 950.938.949.953.953.
ReferenceDeng, Yao, et al., 2005Faleio, Miguel, et al., 2005Hamm, Bleton, et al., 2005Judzentiene and Mockute, 2005Koutsoudaki, Krsek, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBBPX-5CP Sil 8 CBHP-5DB-5
Column length (m) 50.30.50.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (μm) 0.250.250.25 0.1
Program 60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)50C => 3C/min => 150C(10min) => 10C/min => 250C60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min)65C(1min) => 1C/min => 75C (2min) => 0.5C/min => 81C(2min) => 3C/min => 180C(7min)35C => 4C/min => 180C => 10C/min => 250C
I 953.942.954.953.932.
ReferenceNivinskienë, Butkienë, et al., 2005Özer, Sahín, et al., 2005Radudienë, Judpintienë, et al., 2005Singh, Maurya, et al., 2005Albuquerque, Souza, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBMethyl SiliconeHP-5MS OV-1
Column length (m) 50. 30. 30.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.32 0.25 0.25
Phase thickness (μm) 0.25 0.25 0.25
Program 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)not specified60C => 10C/min => 160C => 12C/min => 300C (5min)not specified45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C
I 954.949.954.935.934.
ReferenceButkienë, Nivinskienë, et al., 2004Couladis, Özcan, et al., 2004Deng, Li, et al., 2004El-Shazily, Hafez, et al., 2004Hafez and Abdel-Salam, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 8 CBDB-5DB-5DB-1
Column length (m) 30.50.30. 30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.320.25 0.25
Phase thickness (μm) 0.25 0.25 0.25
Program 40C(1min) => 9C/min => 130C => 2C/min => 230C60C(2min) => 5C/min => 160C (1min) => 10C/min => 250C (2min)60C(4min) => 6C/min => 240 => 10C/min => 280Cnot specified45C => 3C/min => 175C => 15C/min => 300C (10min)
I 949.953.953.953.938.
ReferenceHamm, Bleton, et al., 2004Judpentienë and Mockutë, 2004Letchamo, Ward, et al., 2004Lo Cantore, Iacobellis, et al., 2004Miguel, Simões, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase MDN-5HP-5HP-5MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas Helium  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 30 0C (1 min) ballistically -> 60 0C 2 0C/min -> 120 0C 5 0C/min -> 280 0C (5 min)40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C60C(1min) => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)60C(1min) => 0.5C/min => 85C(1min) => 1C/min => 105C (2min) => 10C/min => 275C(2min)60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
I 951.953.953.953.969.
ReferenceMoretti, Madonia, et al., 2004Senatore, Apostolides Arnold, et al., 2004Singh, Marimuthu, et al., 2004Singh, Maurya, et al., 2004Sotomayor, Martínez, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-5SE-30DB-1
Column length (m) 30.30.  30.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.25  0.25
Phase thickness (μm) 0.250.25  0.25
Program 50C (3min) => 3C/min => 150C (10min) => 10C/min => 250C45C => 3C/min => 175C => 15C/min => 300C (15min)not specifiednot specified45C => 3C/min => 175C => 15C/min => 300C (10min)
I 954.938.953.951.938.
ReferenceTepe, Donmez, et al., 2004Touafek, Nacer, et al., 2004Vilaseca, Guy, et al., 2004Vinogradov, 2004Faleiro, Miguel, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5CP-Sil 8CB-MSCP Sil 8 CBCP Sil 8 CB
Column length (m) 30.30.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.25 0.250.25
Program 40C (1min) => 9C/min => 130C => 2C/min => 230C60C (4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C50C(2min) => 3C/min => 180C(1min) => 20C/min => 250C(2min)70C(5min) => 3C/min => 100C (1min) => 25C/min => 250C (10min)60C(1min) => 5C/min => 160C => 10C/min => 250C(5min)
I 949.969.953.953.953.
ReferenceHamm, Lesellier, et al., 2003Jordán, Martínez, et al., 2003Mockute, Bernotiene, et al., 2003Mockute and Judzentiene, 2003Mockute, Nivinskiene, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5AT-5DB-5Methyl Silicone
Column length (m) 30.30.60.30. 
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (μm) 0.10.250.250.25 
Program 35C => 4C/min => 180C => 10C/min => 250C60C(5min) => 1C/min => 140C => 10C/min => 270C(5min)50 0C 5 0C/min -> 135 0C (1 min) 5 0C/min -> 225 0C (5 min) 5 0C/min -> 260 0C60C => 3C/min => 210C => 5C/min => 250C(2min)not specified
I 935.953.953.950.5953.
ReferenceSilva, Matos, et al., 2003Singh, Singh, et al., 2003Usai, Atzei, et al., 2003Veres, Varga, et al., 2003Bakshu and Raju, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54SE-30SE-30CP Sil 8 CBCP Sil 8 CB
Column length (m)  60.60.50.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)  0.250.250.320.32
Phase thickness (μm)      
Program not specified50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0Cnot specified60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (2min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C(2min)
I 947.953.951.953.953.
ReferenceKilic, 2002Li, Wu, et al., 2002Li, Wu, et al., 2002Mockute and Judzentiene, 2002Mockute and Judzentiene, 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5HP-5MSHP-5DB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.10.250.250.25
Program 40C(3min) => 5C/min => 180C => 15C/min => 240C(15min)35C => 4C/min => 180C => 20C/min => 280C40C (10min) => 3C/min => 120C => 10C/min => 250C (5min)not specified45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min)
I 944.953.945.945.938.
ReferenceNogueira and Romano, 2002Viana, Andrade-Neto, et al., 2002Ansorena, Gimeno, et al., 2001Aparicio, Romero, et al., 2001Figueiredo, Miguel, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1DB-5HP-5 MSHP-5OV-101
Column length (m) 25. 30.30.50.
Carrier gas Nitrogen HeliumHeN2
Substrate      
Column diameter (mm) 0.25 0.250.250.25
Phase thickness (μm) 0.25 0.250.25 
Program not specifiednot specifiednot specified50 0C 3 K/min -> 200 0C 8 K/min -> 280 0Cnot specified
I 940.950.954.940.951.
ReferenceLy, Yamauchi, et al., 2001Petrakis, Tsitsimpikou, et al., 2001Shang, Hu, et al., 2001Usubillaga, Aparicio, et al., 2001Yang, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1AT-5DB-1
Column length (m) 30.30.30.60.30.
Carrier gas HeH2H2 He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40C => 2C/min => 60C => 4C/min => 260C40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)60C(1min) => 4C/min => 200C=10C/min => 280C(20min)45C => 3C/min => 170C => 15C/min => 300C(10min)
I 953.938.938.957.6938.
ReferenceAndrade, Maia, et al., 2000Dorman, Figueiredo, et al., 2000da Silva, Pedro, et al., 2000Velásquez, Toro, et al., 2000Pedro, da Silva, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBDB-1OV-1DB-5
Column length (m) 30.25.30.50.30.
Carrier gas He HeHeN2
Substrate      
Column diameter (mm) 0.250.390.250.320.25
Phase thickness (μm) 0.25 0.250.250.25
Program 45C => 3C/min => 175C => 15C/min => 300C(10min)not specified45C => 3C/min => 175C => 15C/min => 240C (10min)1)50C(1min) => 4C/min => 180C => 2C/min => 250C(10min) 2)50C(1min) => 6C/min => 200C => 12C/min => 250C(5min)45C(5min) => 2C/min => 200C => 5C/min => 250C
I 938.950.938.940.953.
ReferenceSantos, Figueiredo, et al., 1999Weyerstahl, Marschall, et al., 1999Baratta, Dorman, et al., 1998Kökdil, 1998Sanda, Koba, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBDB-5DB-5DB-1
Column length (m) 30.25.30.15.30.
Carrier gas H2N2HeHeHe
Substrate      
Column diameter (mm) 0.25 0.250.250.25
Phase thickness (μm) 0.250.390.250.250.25
Program 45C => 3C/min => 175C => 15C => 240C(10min)not specified60C => 3C/min => 240C => 30C/min => 300C40C(5min) => 5C/min => 120C(10min) => 4C/min => 250C(4min) => 5C/min => 280C45C => 3C/min => 175C => 15C/min => 280C
I 938.951.948.951.938.
Referenceda Silva, Figueiredo, et al., 1998Weyerstahl, Marschall, et al., 1998Yusuf, Begum, et al., 1998Anitescu, Doneanu, et al., 1997Gaspar, Palma, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-SulfurCP Sil 5 CBCP Sil 5 CBDB-1
Column length (m)  30.25.30.30.
Carrier gas  HeN2N2H2
Substrate      
Column diameter (mm)  0.32 0.250.25
Phase thickness (μm)  4.  0.25
Program not specifiednot specifiednot specifiednot specified45 0C 3 0C/min -> 175 0C 15 0C/min -> 240 0C (10 min)
I 953.946.950.951.938.
ReferenceIsidorov, Zenkevich, et al., 1997Mariaca, Berger, et al., 1997Weyerstahl, Marschall, et al., 1997Weyerstahl, Marschall, et al., 1997, 2Barroso, Figueiredo, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1Methyl SiliconeMethyl SiliconeDB-1DB-1
Column length (m) 24.  60.30.
Carrier gas     He
Substrate      
Column diameter (mm) 0.32  0.320.25
Phase thickness (μm) 0.25  0.251.
Program 60C(2min) => 4C/min => 120C => 2C/min => 220C (20min)not specifiednot specifiednot specified40C (4min) => 10C/min => 200C => 50C/min => 250C
I 944.944.931.940.954.
ReferenceDung, Thanh, et al., 1996Zenkevich, 1996Xu, Chu, et al., 1995Ciccioli, Cecinato, et al., 1994Schuberth, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5OV-101OV-101
Column length (m) 60.30.30.  
Carrier gas      
Substrate      
Column diameter (mm) 0.320.320.32  
Phase thickness (μm) 0.251.1.  
Program 3 min at 5 C; 5 - 50 C at 3 deg/min; 50 - 220 C at 5 deg/min0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)not specifiednot specified
I 940.927.932.940.940.
ReferenceCiccioli, Brancaleoni, et al., 1993Storer, Elmore, et al., 1993Storer, Elmore, et al., 1993De Pooter, Vermeesch, et al., 1989De Pooter, Vermeesch, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPacked
Active phase DB-1OV-1OV-101OV-101
Column length (m)  35. 2.5
Carrier gas    N2
Substrate    Chromosorb G 60-80mesh DMCS
Column diameter (mm)  0.50  
Phase thickness (μm)  1.5  
Program not specifiednot specifiednot specifiednot specified
I 948.941.954.948.
ReferenceMacLeod and Snyder, 1988De Pooter and Schamp, 1987Shibamoto, 1987Swigar and Silverstein, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Albano, Lima, et al., 2012
Albano, S.M.; Lima, A.S.; Miguel, M.G.; Pedro, L.G.; Barroso, J.G.; Figueiredo, A.C., Antioxidant, anti-5-lipoxygenase and antiacetylcholinesterase activities of essential oils and decoction water of some aromatic plants, Rec. Nat. Prod., 2012, 6, 1, 35-48. [all data]

Bendiabdellah, El Amine Dib, et al., 2012
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de Morais, Oliveira, et al., 2012
de Morais, S.R.; Oliveira, T.L.S.; BAra, M.T.F.; da Conceicao, E.C.; Rezende, M.H.; Ferri, P.H.; de Paula, J.R., Chemical constituents of essential oil from Lippia sidoides Cham. (Verbenaceae) leaves cultivated in Hidrolandia, Goias, Brasil, Int. J. Anal. Chem., 2012, 2012, 1-4, https://doi.org/10.1155/2012/363919 . [all data]

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da Silva, de Souza, et al., 2012
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Velickovic, Ristic, et al., 2012
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Chaverri, Diaz, et al., 2011
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Fathi, Sahari, et al., 2011
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Karimi, Farmany, et al., 2011
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Laribi, Kouki, et al., 2011
Laribi, B.; Kouki, K.; Sahli, A.; Mougou, A.; Marzouk, B., Essential oil fatty acids composition of a Tunisian caraway (Carum carvi L.) seed ecotype cultivated under water deficit, Adv. Environ. Biol., 2011, 1-15, retrieved from http://www.thefreelibrary.com//print/PrintArticle.aspx?id=253057768. [all data]

Skogerson, Wohlgemuth, et al., 2011
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Xu, Tang, et al., 2010
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Huang, Qin, et al., 2009
Huang, B.; Qin, L.; Chu, Q.; Zhang, Q.; Gao, L.; Zheng, H., Comparison of headspace SPME with hydrodistillation and SFE for analysis of the volatile components of the roots of Valeriana officinalis var. latifolia, Chromatographia, 2009, 69, 5/6, 489-496, https://doi.org/10.1365/s10337-008-0921-y . [all data]

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Mendes, Trindade, et al., 2009, 2
Mendes, M.D.; Trindade, H.; Figueiredo, A.C.; Barroso, J.G.; Fontinha, S.S.; Pedro, L.G., Volatile and molecular characterization of two Portuguese endemic species: Angelica lignescens and Melanoselinium decipiens, Biochen. Systematics Ecol., 2009, 37, 2, 98-105, https://doi.org/10.1016/j.bse.2008.12.006 . [all data]

Porto, Decorti, et al., 2009
Porto, C.Da.; Decorti, D.; Kikic, I., Flavour compounds of Lavandula angustifolia L. to use in food manufacturing: comparison of three different extraction methods, Food Chem., 2009, 112, 4, 1072-1078, https://doi.org/10.1016/j.foodchem.2008.07.015 . [all data]

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Su, Wang, et al., 2009
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Yang, Yang, et al., 2009
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Yu, Li, et al., 2009
Yu, L.-F.; Li, X.-R.; Liu, S.-Y.; Xu, G.-W.; Liang, Y.-Z., Comparative analysis of essential components between the herbal pair Radix Saposhnikoviae-Rhizoma seu Radix Notopterygii and its single herbs by GC-MS combined with a chemometric resolution method, Anal. Methods, 2009, 1, 1, 45-51, https://doi.org/10.1039/b9ay00044e . [all data]

Zellner, Amorim, et al., 2009
Zellner, B.D.; Amorim, A.C.L.; de Miranda A.L.P.; Alves, R.J.V.; Barbosa, J.P.; da Costa, G.L.; Rezende, C.M., Screening of the odor-activity and bioactiovity of the essential oils of leaves and flowers of Hyptis Passerina Mart. from the Brazilian Cerrado, J. Braz. Chem. Soc., 2009, 20, 2, 322-332, https://doi.org/10.1590/S0103-50532009000200018 . [all data]

Costa, De Fina, et al., 2008
Costa, R.; De Fina, M.R.; Valentino, M.R.; Rustaiyan, A.; Dugo, P.; Dugo, G.; Mondello, L., An investigation on the volatile composition of some Artemisia species from Iran, Flavour Fragr. J., 2008, 24, 2, 75-82, https://doi.org/10.1002/ffj.1919 . [all data]

Isidorov, Lech, et al., 2008
Isidorov, V.A.; Lech, P.; Zolciak, A.; Rusak, N.; Szczepaniak, L., Gas Chromatographic - nass spectrometric investigation of metabolites from the needles and roots of pine seedlings at early stages of pathogenic fungi Armillaria ostoyae attack, Trees, 2008, 22, 4, 531-542, https://doi.org/10.1007/s00468-008-0213-z . [all data]

Kannaste, Vongvanich, et al., 2008
Kannaste, A.; Vongvanich, N.; Borg-Karlson, A.-K., Infestation by a Nalepella species induces emissions of alpha- and beta-farnesenes, (-)-linalool and aromatic compounds in Norway spruce clones of different susceptibility to the large pine weevil, Anthropod-Plant Interactions, 2008, 2, 1, 31-41, https://doi.org/10.1007/s11829-008-9029-4 . [all data]

Kupcinskiene, Stikliene, et al., 2008
Kupcinskiene, E.; Stikliene, A.; Judzentiene, A., The essential oil guatitative composition in the needles of Pinus sylvestris L. growing along industrial transects, Environ. Pollution, 2008, 155, 3, 481-491, https://doi.org/10.1016/j.envpol.2008.02.001 . [all data]

Lo Presti, Sciarrone, et al., 2008
Lo Presti, M.; Sciarrone, D.; Crupi, M.C.; Costa, R.; Ragusa, S.; Dugo, G.; Mondello, L., Evaliation of the volatile and chiral composition in Pistacia lentiscus L. essential oil, Flavour Fragr. J., 2008, 23, 4, 249-257, https://doi.org/10.1002/ffj.1878 . [all data]

Ning, Zheng, et al., 2008
Ning, H.; Zheng, F.; Sun, B.; Xie, J.; Liu, Y., Solvent-free microwave extraction of essential oil from Zanthoxylum bungeanum Maxim., Food Environ. Ind. (Chinese), 2008, 34, 5, 179-184. [all data]

Nogueira, Marcelo-Curto, et al., 2008
Nogueira, T.; Marcelo-Curto, M.J.; Cristina Figueiredo, A.; Barroso, J.G.; Pedro, L.G.; Rubiolo, P.; Bicchi, C., Chemotaxonomy of Hypericum genus from Portugal: Geographical distribution and essential oils composition of Hypericum perfoliatum, Hypericum humifusum, Hypericum linarifolium and Hypericum pulchrum, Biochem. Syst. Ecol., 2008, 36, 1, 40-50, https://doi.org/10.1016/j.bse.2007.07.004 . [all data]

Raj, Baby, et al., 2008
Raj, G.; Baby, S.; Dan, M.; Thaha, A.R.M.; Sethuraman, M.G.; George, V., Volatile constituents from the rhisomes of Curcuma haritha Mangaly and Sabu from Sauthern India, Flavour Fragr. J., 2008, 23, 5, 348-352, https://doi.org/10.1002/ffj.1891 . [all data]

Silva, Doria, et al., 2008
Silva, W.L.; Doria, G.A.A.; Maia, R.T.; Nunes, R.S.; Carvalho, G.A.; Blank, A.F.; Alves, P.B.; Marcal, R.M.; Cavalcanti, S.C.H., Effects of essential oils on Aedes aegypti larvae: alternatives to environmentally safe insecticides, Bioresource Technol., 2008, 99, 8, 3251-3255, https://doi.org/10.1016/j.biortech.2007.05.064 . [all data]

Xie, Sun, et al., 2008
Xie, J.; Sun, B.; Zheng, F.; Wang, S., Volatile flavor constituents in roasted pork of mini-pig, Food Chem., 2008, 109, 3, 506-514, https://doi.org/10.1016/j.foodchem.2007.12.074 . [all data]

Zachariah, Leela, et al., 2008
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Agabriel, Cornu, et al., 2007
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Notes

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