trans-β-Ionone

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5RTX-1DB-5MSZB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.320.220.250.32
Phase thickness (μm) 0.250.50.250.250.5
Tstart (C) 60.40.60.40.40.
Tend (C) 280.265.230.285.265.
Heat rate (K/min) 3.7.2.4.37.
Initial hold (min)      
Final hold (min)  5.35. 5.
I 1489.1496.1463.1485.1494.
ReferenceKundakovic, Fokialakis, et al., 2007Mahattanatawee K., Perez-Cacho P.R., et al., 2007Paolini, Muselli, et al., 2007Radulovic, Misic, et al., 2007Ruiz Perez-Cacho, Mahattanatawee, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5Mega 5MSHP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.220.240.260.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 5.    
Final hold (min)      
I 1484.1482.1485.1485.1491.
ReferenceSaroglou, Marin, et al., 2007Vagionas, Ngassapa, et al., 2007Bastos, Ishimoto, et al., 2006Condurso, Verzera, et al., 2006Javidnia, Miri, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.40.
Tend (C) 280.280.280.285.300.
Heat rate (K/min) 3.3.4.4.34.
Initial hold (min)   5. 5.
Final hold (min)      
I 1484.1475.1482.1484.1482.
ReferenceKukic J., Petrovic S., et al., 2006Pavlovic, Tzakou, et al., 2006Saroglou, Dorizas, et al., 2006Vujisic L., Vuckovic I., et al., 2006Vundac, Pfeifhofer, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5ZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 40.50.50.50.40.
Tend (C) 230.250.250.250.265.
Heat rate (K/min) 6.4.4.4.7.
Initial hold (min) 1.5.5.5. 
Final hold (min)  15.15.15.5.
I 1500.1486.1486.1486.1484.
ReferenceZeller and Rychlik, 2006Mahattanatawee, Goodner, et al., 2005Mahattanatawee, Goodner, et al., 2005Mahattanatawee, Goodner, et al., 2005Mahattanatawee, Rouseff, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5MSHP-5MSHP-5MSHP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.80.80.80.
Tend (C) 230.250.290.290.290.
Heat rate (K/min) 2.4.2.4.6.
Initial hold (min)  2.   
Final hold (min) 35.20.   
I 1462.1488.1483.91488.91493.
ReferencePaolini, Costa, et al., 2005Pino, Mesa, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5MSZB-5HP-5MS
Column length (m) 30.30.30.0.30.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.250.250.220.320.25
Phase thickness (μm) 0.250.250.250.50.25
Tstart (C) 60.50.60.40.60.
Tend (C) 280.290.290.265.280.
Heat rate (K/min) 3.4.20.7.4.
Initial hold (min)   1. 5.
Final hold (min)   10.5. 
I 1482.1483.1488.1491.1489.
ReferenceAligiannis, Kalpoutzakis, et al., 2004Flach A., Dondon R.C., et al., 2004Garland, Menary, et al., 2004Gocmen, Gurbuz, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5MSHP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 260.260.280.220.220.
Heat rate (K/min) 3.3.4.5.5.
Initial hold (min)   2.10.10.
Final hold (min)      
I 1485.1486.1485.1485.1485.
ReferenceJavidnia, Miri, et al., 2004Javidnia, Miri, et al., 2004, 2Mardarowicz, Wianowska, et al., 2004Angelini, Carpanese, et al., 2003Campeol, Flamini, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5DB-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 35.60.60.60.40.
Tend (C) 225.240.240.280.265.
Heat rate (K/min) 4.3.3.3.7.
Initial hold (min) 5.    
Final hold (min) 20.   5.
I 1460.1485.1486.1485.1494.
ReferenceChisholm, Jell, et al., 2003Flamini, Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003Fokialakis, Melliou, et al., 2003Högnadóttir and Rouseff, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5CP Sil 5 CBHP-1HP-5
Column length (m) 25.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm)  0.250.250.330.25
Tstart (C) 60.60.60.40.60.
Tend (C) 260.280.280.260.280.
Heat rate (K/min) 4.3.3.2.4.
Initial hold (min)   10.5.5.
Final hold (min)   60.20. 
I 1488.1485.1470.1483.1484.
ReferenceJavidnia, Miri, et al., 2003Ngassapa, Runyoro, et al., 2003Pino, Almora, et al., 2003Senatore, Rigano, et al., 2003Skaltsa, Demetzos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5DB-5SPB-1
Column length (m) 30.30.30.25.37.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.35.60.70.100.
Tend (C) 280.200.280.260.250.
Heat rate (K/min) 3.10.3.4.8.
Initial hold (min) 5.5.   
Final hold (min)  30.   
I 1485.1482.1480.1485.1470.
ReferenceDemetzos, Angelopoulou, et al., 2002Karagül-Yüceer, Cadwallader, et al., 2002Kovacevic, Pavlovic, et al., 2002Miri, Ramezani, et al., 2002Misharina, Samusenko, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.500.25
Tstart (C) 60.60.60.60.35.
Tend (C) 280.260.380.280.200.
Heat rate (K/min) 3.3.3.3.10.
Initial hold (min) 5.   5.
Final hold (min)  10.  30.
I 1483.1484.1477.1486.1488.
ReferenceAligiannis, Kalpoutzakis, et al., 2001Couladis, Baziou, et al., 2001Couladis, Tsortanidou, et al., 2001Couladis, Tzakou, et al., 2001Karagül-Yüceer, Drake, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBHP-5HP-5MSDB-1
Column length (m) 30.50.30.30.30.
Carrier gas  HeHeHeH2
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (μm) 0.250.4 0.250.25
Tstart (C) 40.60.50.60.40.
Tend (C) 240.280.200.280.245.
Heat rate (K/min) 7.3.4.4.3.
Initial hold (min)  10.1.5.3.
Final hold (min) 5.60.  20.
I 1473.1470.1493.1484.1442.
ReferenceLin and Rouseff, 2001Pino and Marbot, 2001Shalit, Katzir, et al., 2001Skaltsa, Mavrommati, et al., 2001Brat, Brillouet, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5CP Sil 5 CBSE-54
Column length (m) 30.30.30.25.25.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.31
Phase thickness (μm) 0.250.250.25  
Tstart (C) 50.50.50.60.35.
Tend (C) 280.280.280.260.250.
Heat rate (K/min) 4.4.4.5.4.
Initial hold (min) 5.5.5. 3.
Final hold (min)      
I 1482.1482.1485.1467.1494.
ReferenceLazari, Skaltsa, et al., 2000Lazari, Skaltsa, et al., 2000, 2Lazari, Skaltsa, et al., 1999Weyerstahl, Marschall, et al., 1999Li, Wang, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54Methyl SiliconeOV-101OV-101HP-101
Column length (m) 25.25.15.15.50.
Carrier gas H2He  N2
Substrate      
Column diameter (mm) 0.310.20.320.320.25
Phase thickness (μm)  0.3   
Tstart (C) 35.40.35.35.70.
Tend (C) 250.200.250.250.200.
Heat rate (K/min) 4.2.6.6.3.
Initial hold (min) 3. 3.3. 
Final hold (min)      
I 1495.1479.1453.1460.1484.
ReferenceLi, Wang, et al., 1998Píry, Príbela, et al., 1995Chisholm, Guiher, et al., 1994Chisholm, Guiher, et al., 1994Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101OV-101DB-1DB-1
Column length (m) 30.50.50.30.30.
Carrier gas HeN2N2  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)      
Tstart (C) 50.80.80.50.50.
Tend (C) 250.200.200.300.300.
Heat rate (K/min) 4.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1482.1464.1470.1452.91458.4
ReferenceGómez, Ledbetter, et al., 1993Yang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Chang, Sheng, et al., 1989Chang, Sheng, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-150SPB-1SPB-1OV-101OV-101
Column length (m) 30.60.60.26.26.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.530.250.250.260.26
Phase thickness (μm) 1.20.250.250.30.3
Tstart (C) 30.35.35.100.60.
Tend (C) 220.235.235.240.240.
Heat rate (K/min) 3.2.2.2.2.
Initial hold (min)  10.10.  
Final hold (min)  40.40.  
I 1469.1460.1460.1459.61457.5
ReferenceSagrero-Nieves, de Pooter, et al., 1989Huang, Bruechert, et al., 1987Huang, Bruechert, et al., 1987Wang and Sun, 1987Wang and Sun, 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 26.21.521.526.524.
Carrier gas      
Substrate      
Column diameter (mm) 0.260.270.270.250.26
Phase thickness (μm) 0.32.0.140.140.5
Tstart (C) 60.60.60.70.80.
Tend (C) 240.240.240.240.240.
Heat rate (K/min) 8.6.6.9.6.
Initial hold (min)    4.08 
Final hold (min)      
I 1470.01480.41461.31468.31472.65
ReferenceWang and Sun, 1987Wang and Sun, 1987Wang and Sun, 1987Wang and Sun, 1987, 2Wang, Zhong, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kundakovic, Fokialakis, et al., 2007
Kundakovic, T.; Fokialakis, N.; Kovacevic, N.; Chinou, I., Essential oil composition of Achillea lingulata and A. umbellata, Flavour Fragr. J., 2007, 22, 3, 184-187, https://doi.org/10.1002/ffj.1778 . [all data]

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Condurso, C.; Verzera, A.; Romeo, V.; Ziino, M.; Trozzi, A.; Ragusa, S., The leaf volatile constituents of Isatis tinctoria by solid-phase microextraction and gas chromatography/mass spectrometry, Planta Medica, 2006, 72, 10, 924-928, https://doi.org/10.1055/s-2006-946679 . [all data]

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Kukic J., Petrovic S., et al., 2006
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References