1-Methyladamantane

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryPackedCapillaryCapillaryCapillary
Active phase SE-30SE-30SqualaneSE-30SE-30
Column length (m) 50.1.100.  
Carrier gas He He  
Substrate  CHromaton N-AW   
Column diameter (mm) 0.2 0.25  
Phase thickness (μm)      
Temperature (C) 190.150.110.110.120.
I 1171.1140.1115.31118.1124.
ReferenceSarkisova and Pimerzin, 2005Yashkin, Kurbatova, et al., 2001Bender, Said, et al., 1986Bogoslovsky, Anvaer, et al., 1978Bogoslovsky, Anvaer, et al., 1978
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30SE-30SqualaneSqualane
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Temperature (C) 130.140.145.100.110.
I 1128.1134.1137.1110.1116.
ReferenceBogoslovsky, Anvaer, et al., 1978Bogoslovsky, Anvaer, et al., 1978Bogoslovsky, Anvaer, et al., 1978Bogoslovsky, Anvaer, et al., 1978Bogoslovsky, Anvaer, et al., 1978
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedPackedPacked
Active phase SqualaneSqualaneSE-30SE-30SE-30
Column length (m)   6.16.16.1
Carrier gas   N2N2N2
Substrate   Chrom WChrom WChrom W
Column diameter (mm)      
Phase thickness (μm)      
Temperature (C) 125.140.120.130.140.
I 1125.1135.1124.1128.1134.
ReferenceBogoslovsky, Anvaer, et al., 1978Bogoslovsky, Anvaer, et al., 1978Mitra, Mohan, et al., 1974Mitra, Mohan, et al., 1974Mitra, Mohan, et al., 1974
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneApiezon LSqualaneSqualane
Column length (m) 50.50.50.50.50.
Carrier gas H2H2N2N2N2
Substrate      
Column diameter (mm) 0.20.20.20.20.2
Phase thickness (μm)      
Temperature (C) 100.100.140.110.125.
I 1110.1162.1179.1116.1125.
ReferenceMitra, Mohan, et al., 1974, 2Mitra, Mohan, et al., 1974, 2Hála, Eyem, et al., 1970Hála, Eyem, et al., 1970Hála, Eyem, et al., 1970
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSE-30SE-30SE-30SE-30
Column length (m) 50.50.50.50.50.
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm) 0.20.270.270.270.27
Phase thickness (μm)      
Temperature (C) 140.145.160.175.190.
I 1135.1137.1151.1162.1171.
ReferenceHála, Eyem, et al., 1970Burkhard, Vais, et al., 1969Burkhard, Vais, et al., 1969Burkhard, Vais, et al., 1969Burkhard, Vais, et al., 1969
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sarkisova and Pimerzin, 2005
Sarkisova, V.S.; Pimerzin, A.A., Gas chromatographic characteristics and boiling points of diadamantanes, Pet. Chem. USSR (Engl. Transl.), 2005, 45, 1, 63-66. [all data]

Yashkin, Kurbatova, et al., 2001
Yashkin, S.N.; Kurbatova, S.V.; Buryak, A.K., Gas chromatography of halogenated adamantanes, Russ. Chem. Bull. (Engl. Transl.), 2001, 50, 5, 828-832, https://doi.org/10.1023/A:1011350908009 . [all data]

Bender, Said, et al., 1986
Bender, A.O.; Said, E.Z.; Abdulsada, A.K., Gas chromatographic identification of adamantanes in some Iraqi crude oils, Analyst, 1986, 111, 5, 575-576, https://doi.org/10.1039/an9861100575 . [all data]

Bogoslovsky, Anvaer, et al., 1978
Bogoslovsky, Yu.N.; Anvaer, B.I.; Vigdergauz, M.S., Chromatographic constants in gas chromatography (in Russian), Standards Publ. House, Moscow, 1978, 192. [all data]

Mitra, Mohan, et al., 1974
Mitra, G.D.; Mohan, G.; Sinha, A., Advances in the utilization of the retention index system for characterizing hydrocarbons in complex mixtures by gas chromatography, J. Chromatogr., 1974, 99, 215-230, https://doi.org/10.1016/S0021-9673(00)90857-4 . [all data]

Mitra, Mohan, et al., 1974, 2
Mitra, G.D.; Mohan, G.; Sinha, A., Gas chromatographic analysis of complex hydrocarbon mixtures, J. Chromatogr. A, 1974, 91, 633-648, https://doi.org/10.1016/S0021-9673(01)97944-0 . [all data]

Hála, Eyem, et al., 1970
Hála, S.; Eyem, J.; Burkhard, J.; Landa, S., Retention indices of adamantanes, J. Chromatogr. Sci., 1970, 8, 4, 203-209, https://doi.org/10.1093/chromsci/8.4.203 . [all data]

Burkhard, Vais, et al., 1969
Burkhard, J.; Vais, J.; Vodicka, L.; Landa, S., Adamantane and its derivatives. XVI. The gas chromatographic characterization of adamantane derivatives, J. Chromatogr., 1969, 42, 207-218, https://doi.org/10.1016/S0021-9673(01)80617-8 . [all data]


Notes

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