Silane, chlorotrimethyl-
- Formula: C3H9ClSi
- Molecular weight: 108.642
- IUPAC Standard InChIKey: IJOOHPMOJXWVHK-UHFFFAOYSA-N
- CAS Registry Number: 75-77-4
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Chlorotrimethylsilane; Trimethylchlorosilane; Trimethylsilyl chloride; (CH3)3SiCl; Monochlorotrimethylsilicon; Silane, trimethylchloro-; Silicane, chlorotrimethyl-; TL 1163; UN 1298; Silylium, trimethyl-, chloride; Monochlorotrimethylsilane; NSC 15750; Trimethylsilane chloride; KA 31; TSL 8031
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
Column type | Active phase | Temperature (C) | I | Reference | Comment |
---|---|---|---|---|---|
Packed | SE-30 | 100. | 555. | Kirichenko, Markov, et al., 1975 | Ar; Column length: 1. m |
Packed | SE-30 | 70. | 552. | Kirichenko, Markov, et al., 1975 | Ar; Column length: 1. m |
Packed | Polymethylsiloxane, (PMS-20000) | 50. | 552.4 | Ainshtein and Shulyatieva, 1972 | He, Chromosorb W; Column length: 2. m |
Packed | SE-30 | 40. | 553. | Garzó, Fekete, et al., 1967 | N2, Chromosorb W; Column length: 2. m |
Normal alkane RI, non-polar column, temperature ramp
Column type | Active phase | I | Reference | Comment |
---|---|---|---|---|
Capillary | OV-101 | 560. | Zenkevich, 2005 | 25. m/0.20 mm/0.10 μm, N2/He, 6. K/min; Tstart: 50. C; Tend: 250. C |
Normal alkane RI, non-polar column, custom temperature program
Column type | Active phase | I | Reference | Comment |
---|---|---|---|---|
Capillary | Polydimethyl siloxanes | 560. | Zenkevich, 2001 | Program: not specified |
Capillary | Methyl Silicone | 560. | Zenkevich, 2001, 2 | Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Kirichenko, Markov, et al., 1975
Kirichenko, É.A.; Markov, B.A.; Kochetov, V.A.; Kuznetsova, T.I.,
Chromatographic retention indices of alkylchlorosilanes,
Zh. Anal. Khim., 1975, 30, 6, 1038-1040. [all data]
Ainshtein and Shulyatieva, 1972
Ainshtein, A.A.; Shulyatieva, T.I.,
Retention indices of alkyl- and arylchlorosilanes,
Zh. Anal. Khim., 1972, 27, 816-821. [all data]
Garzó, Fekete, et al., 1967
Garzó, G.; Fekete, J.; Blazsó, M.,
Determination of the gas chromatographic retention indices of various organometallic compounds,
Acta Chim. Acad. Sci. Hung., 1967, 51, 4, 359-369. [all data]
Zenkevich, 2005
Zenkevich, I.G.,
Experimentally measured retention indices., 2005. [all data]
Zenkevich, 2001
Zenkevich, I.G.,
Encyclopedia of Chromatography. Derivatization of Hydroxy Compounds for GC Analysis, Marcel Dekker, Inc., New York - Basel, 2001, 237. [all data]
Zenkevich, 2001, 2
Zenkevich, I.G.,
Comparative Characterization of Conditions for Unambuguous Chromatographic Identification of Organic Compounds,
Zh. Anal. Khim., 2001, 56, 9, 915-924. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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