Pyrimidine, 5-methyl-2,4-bis[(trimethylsilyl)oxy]-

• Formula: C₁₁H₂₂N₂O₂Si₂
• Molecular weight: 270.4756
• IUPAC Standard InChI: InChI=1S/C11H22N2O2Si2/c1-9-8-12-11(15-17(5,6)7)13-10(9)14-16(2,3)4/h8H,1-7H3 Copy

  
• IUPAC Standard InChIKey: DRNUNECHVNIYHQ-UHFFFAOYSA-N Copy
• CAS Registry Number: 7288-28-0
• Chemical structure:
  This structure is also available as a 2d Mol file or as a computed 3d SD file
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• Other names: Pyrimidine, 5-methyl-2,4-bis(trimethylsiloxy)-; Bis(O-trimethylsilyl)thymine; 2,4-Bis(trimethylsilyl)thymine; 5-Methyl-2,4-bis(trimethylsiloxy)pyrimidine; 5-Methyl-2,4-bis[(trimethylsilyl)oxy]pyrimidine; Pyrimidine, 2,4-dihydroxy-5-methyl, bis-TMS; Thymine, bis-TMS; Thymine, TMS; Pyrimidine, 2,4-dihydroxy-5-methyl, TMS; 2,4-Di-O-(trimethylsilyl)thymine
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• Information on this page:
  • Gas Chromatography
  • References
  • Notes
• Other data available:
  • Mass spectrum (electron ionization)
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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Kovats' RI, non-polar column, custom temperature program

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Normal alkane RI, non-polar column, temperature ramp

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References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Miller, Pacáková, et al., 1976
Miller, V.; Pacáková, V.; Smolková, E., Gas-liquid chromatographic analysis of trimethylsilyl derivatives of pyrimidine and purine bases and nucleosides, J. Chromatogr., 1976, 119, 355-367, https://doi.org/10.1016/S0021-9673(00)86799-0 . [all data]

Pacakova, Miller, et al., 1971
Pacakova, V.; Miller, V.; Cernohorsky, I.J., Gas-Liquid Chromatography of Some Pyrimidine Derivatives, Anal. Biochemistry, 1971, 42, 2, 549-554, https://doi.org/10.1016/0003-2697(71)90071-6 . [all data]

Yamaji, Kimura, et al., 1978
Yamaji, A.; Kimura, S.; Kawasaki, H.; Yuki, H., Gas chromatographic analysis of pyrimidine and purine bases by retention indices, Yakugaku Zasshi, 1978, 98, 1, 1536-1541. [all data]

Butts, 1972
Butts, W.C., Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds, Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3 . [all data]

Lee, Yanamandra, et al., 2002
Lee, B.Y.; Yanamandra, K.; Thurmon, T.F., Quantitative estimation of organic analytes with a capillary column, Am. Clin. Lab., 2002, May, 30-34. [all data]

Notes

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• Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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